Chemical exchange and spectral coalescence in low-hydration MCM-41 studied by proton NMR

Microporous and Mesoporous Materials

Volumn 162, Issue , 2012, Pages 136-142

  Niknam, Mohamad ^a   Liang, Jianzhen ^a   Walia, Jaspreet ^a   Peemoeller, Hartwig ^a  

^a UNIVERSITY OF WATERLOO   (Canada)

Author keywords

2D time domain NMR; Chemical exchange; MAS; MCM 41; Spectral coalescence

Indexed keywords

CHEMICAL EXCHANGE; EXCHANGE RATES; HIGH-FIELD; HYDRATION LEVELS; INVERSION RECOVERY; MAS; MAS NMR; MCM-41; NMR RELAXATION; OH GROUP; PROTON NMR; PROTON RESONANCES; SPECTRAL POSITION; SURFACE OH GROUP; TIME DOMAIN NMR; WATER MOLECULE;

EXPERIMENTS; FINANCE; HYDRATION; MAGIC ANGLE SPINNING; MESOPOROUS MATERIALS; PROTONS; SILICA; SURFACE WATERS; SURFACES; TIME DOMAIN ANALYSIS;

COALESCENCE;

EID: 84863836188     PISSN: 13871811     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.micromeso.2012.06.010     Document Type: Article

References (24)

1. C.T. Kresge, M.E. Leonowicz, W.J. Roth, J.C. Vartuli, and J.S. Beck Nature 359 1992 710
2. D. Akporiaye, E.W. Hansen, R. Schmidt, and M. Stocker J. Phys. Chem. 98 1994 1926
3. E.W. Hansen, R. Schmidt, M. Stocker, and D. Akporiaye J. Phys. Chem. 99 1995 4148
4. F. Stallmach, J. Karger, C. Krause, M. Jeschke, and U. Oberhagemann J. Am. Chem. Soc. 122 2000 9237
5. D.W. Hwang, A.K. Sinha, C.-Y. Cheng, T.-Y. Yu, and L.-P. Hwang J. Phys. Chem. B 105 2001 5713
6. D.W. Hwang, C.-C. Chu, A.K. Sinha, and L.-P. Hwang J. Phys. Chem. 126 2007 044702
7. B. Grünberg, T. Emmler, E. Gedat, I. Shenderovich, G.H. Findenegg, H.-H. Limbach, and G. Buntkowsky Chem. Eur. J. 10 2004 5689
8. J. Trebosc, J.W. Wiench, S. Huh, V.S.-Y. Lin, and M. Pruski J. Am. Chem. Soc. 127 2005 3057
9. G. Buntkowsky, H. Breitzke, A. Adamczyk, F. Roelofs, T. Emmler, E. Gedat, B. Grünberg, Y. Xu, H.-H. Limbach, I. Shenderovich, A. Vyalikh, and G. Findenegg Phys. Chem. Chem. Phys. 9 2007 4843
10. F. Mallamace, M. Broccio, C. Corsaro, A. Faraone, L. Liu, C.-Y. Mou, and S.-H. Chen J. Phys.: Condens. Matter 18 2006 S2285
11. F. Mallamace, C. Corsaro, M. Broccio, C. Branca, N. Gonzalez-Segredo, J. Spooren, and S.-H. Shen PNAS 105 2008 12725
12. J. Hassan, E. Reardon, and H. Peemoeller Microporous Mesoporous Mater. 122 2009 121
13. S. Pizzanelli, S. Kababya, V. Frydman, M. Landau, and S. Vega J. Phys. Chem. B 109 2005 8029
14. A. Vyalikh, T. Emmler, B. Grünberg, Y. Xu, I. Shenderovich, G. Findenegg, H.-H. Limbach, and G. Buntkowsky Z. Phys. Chem. 221 2007 155
15. I.-S. Chuang, D.R. Kinney, and G.E. Maciel J. Am. Chem. Soc. 115 1993 8695
16. F. Mansour, R.M. Dimeo, and H. Peemoeller Phys. Rev. B 66 2002 041307
17. H. Peemoeller Bull. Magn. Reson. 11 1989 19
18. D. Marquardt SIAM J. Appl. Math. 11 1963 431
19. R. Kimmich NMR Tomography, Diffusometry, Relaxometry 1997 Springer-Verlag Berlin (Chapter 23, Section 1.3)
20. X.S. Zhao, G.Q. Lu, A.K. Whittaker, G.J. Millar, and H.Y. Zhu J. Phys. Chem. B 101 1997 6525
21. H.T. Edzes, and E.T. Samulski J. Magn. Reson. 31 1978 207
22. J.C. MacTavish, Ph.D. Thesis, University of Waterloo, Waterloo, Ontario, Canada (1988).
23. D.A. Oleskevich, N. Ghahramany, W.P. Weglarz, and H. Peemoeller J. Magn. Reson. 113 1996 1
24. A. Bain Prog. Nucl. Magn. Reson. Spectrosc. 43 2003 63