Rapid isolation of new furostanol saponins from fenugreek seeds based on ultra-performance liquid chromatography coupled with a hybrid quadrupole time-of-flight tandem mass spectrometry

Journal of Separation Science

Volumn 35, Issue 12, 2012, Pages 1538-1550

  Pang, Xu ^a   Kang, Liping ^a,b   Yu, Heshui ^a,b   Zhao, Yang ^a   Xiong, Chengqi ^a   Zhang, Jie ^a   Shan, Junjie ^c   Ma, Baiping ^a  

^a BEIJING INSTITUTE OF RADIATION MEDICINE   (China)

^b TIANJIN UNIVERSITY OF TRADITIONAL CHINESE MEDICINE   (China)

^c BEIJING INSTITUTE OF PHARMACOLOGY AND TOXICOLOGY   (China)

Author keywords

Furostanol saponins; Isolation; Leguminosae; Trigonella foenumgraecum L.; UPLC Q TOF MSE

Indexed keywords

FUROSTANOL SAPONINS; ISOLATION; LEGUMINOSAE; TRIGONELLA FOENUM-GRAECUM; UPLC-Q-TOF MSE;

CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

METABOLITES;

5,25(27)DIEN FUROST 3 BETA, 22ALPHA,26 TRIOL; 5ALPHA FUROST 2ALPHA,3BETA,22',26 TETROL; 5ALPHA FUROST 2ALPHA,3BETA,22ALPHA,26 TETROL; 5ALPHA FUROST 3BETA,22ALPHA,26 TRIOL; 5BETA FUROST 3BETA,22ALPHA,26 TRIOL; FUROST 5 EN 2',3BETA,22',26 TETROL; FUROST 5 EN 3 BETA, 22ALPHA,26 TRIOL; PARVIFLOSIDE; SAPONIN DERIVATIVE; TRIGONEOSIDE XV; TRIGONEOSIDE XVIIB; TRIGONEOSIDE XVIII; UNCLASSIFIED DRUG;

ARTICLE; DRUG IDENTIFICATION; DRUG ISOLATION; FENUGREEK; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; QUADRUPOLE MASS SPECTROMETRY; TIME OF FLIGHT MASS SPECTROMETRY; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; PLANT EXTRACTS; SAPONINS; SEEDS; TANDEM MASS SPECTROMETRY; TRIGONELLA;

FABACEAE; TRIGONELLA FOENUM-GRAECUM;

EID: 84863494134     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201200020     Document Type: Article

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