Molecularly imprinted-solid phase extraction combined with simultaneous derivatization and dispersive liquid-liquid microextraction for selective extraction and preconcentration of methamphetamine and ecstasy from urine samples followed by gas chromatography

Journal of Chromatography A

Volumn 1248, Issue , 2012, Pages 24-31

  Djozan, Djavanshir ^a   Farajzadeh, Mir Ali ^a   Sorouraddin, Saeed Mohammad ^a   Baheri, Tahmineh ^b  

^a UNIVERSITY OF TABRIZ   (Iran)

^b The Research Center of Antinarcotics Police   (Iran)

Author keywords

Dispersive liquid liquid microextraction; Gas chromatography; Methamphetamine; Molecularly imprinted polymer; Solid phase extraction

Indexed keywords

3 ,4-METHYLENEDIOXYMETHAMPHETAMINE; ANALYTES; CALIBRATION GRAPHS; DERIVATIZATION REAGENT; DERIVATIZATIONS; DETECTION LIMITS; DISPERSIVE LIQUID-LIQUID MICROEXTRACTION; EXPERIMENTAL PARAMETERS; EXTRACTION SOLVENTS; GAS CHROMATOGRAPHY-FLAME IONIZATION DETECTIONS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMAN URINE; METHAMPHETAMINE; MOLECULARLY IMPRINTED MICROSPHERES; MOLECULARLY IMPRINTED POLYMER; ORGANIC PHASE; PHASE EXTRACTION; PRE-CONCENTRATION; PRECIPITATION POLYMERIZATIONS; RELATIVE STANDARD DEVIATIONS; SELECTIVE EXTRACTION; SOLID-PHASE EXTRACTION; TARGET ANALYTES; URINE SAMPLE;

CENTRIFUGATION; DEIONIZED WATER; GAS CHROMATOGRAPHY; LIQUIDS; METHANOL; SORPTION;

SOLVENT EXTRACTION;

3,4 METHYLENEDIOXYMETHAMPHETAMINE; BUTYLCHLOROFORMATE; METHAMPHETAMINE; METHANOL; SOLVENT; UNCLASSIFIED DRUG; WATER;

ARTICLE; CENTRIFUGATION; CONCENTRATION PROCESS; CONTROLLED STUDY; DERIVATIZATION; DISPERSIVE LIQUID LIQUID MICROEXTRACTION; HUMAN; LIMIT OF DETECTION; LIQUID PHASE MICROEXTRACTION; MASS FRAGMENTOGRAPHY; MOLECULAR IMPRINTING; MOLECULARLY IMPRINTED SOLID PHASE EXTRACTION; PHYSICAL PHASE; POLYMERIZATION; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; REPEAT PROCEDURE; SOLID PHASE EXTRACTION; SOLVENT EXTRACTION; SYNTHESIS; URINE LEVEL;

CALIBRATION; CENTRAL NERVOUS SYSTEM AGENTS; CHROMATOGRAPHY, GAS; FLAME IONIZATION; HUMANS; LIMIT OF DETECTION; LIQUID PHASE MICROEXTRACTION; METHAMPHETAMINE; MOLECULAR IMPRINTING; N-METHYL-3,4-METHYLENEDIOXYAMPHETAMINE; SOLID PHASE EXTRACTION; SUBSTANCE ABUSE DETECTION;

EID: 84863086711     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.05.085     Document Type: Article

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