Separation of enantiomers of norephedrine by capillary electrophoresis using cyclodextrins as chiral selectors: Comparative CE and NMR studies

Electrophoresis

Volumn 33, Issue 11, 2012, Pages 1637-1647

  Lomsadze, Ketevan ^a   Vega, Elena Domínguez ^b   Salgado, Antonio ^c   Crego, Antonio L ^b   Scriba, Gerhard K E ^d   Marina, Maria Luisa ^b   Chankvetadze, Bezhan ^a  

^a TBILISI STATE UNIVERSITY   (Georgia)

^b UNIVERSITY OF ALCALÁ   (Spain)

^c Structural Biology and Biocomputing Programme   (Spain)

^d FRIEDRICH SCHILLER UNIVERSITY JENA   (Germany)

Author keywords

Analyte selector complexes; Cyclodextrins; Enantiomer migration order; Enantioseparation; Norephedrine

Indexed keywords

CAPILLARY ELECTROPHORESIS; CYCLODEXTRINS; NUCLEAR MAGNETIC RESONANCE;

ANALYTE-SELECTOR COMPLEX; ANALYTES; CHIRAL RECOGNITION; CHIRAL SELECTOR; ENANTIOMER MIGRATION ORDER; ENANTIOSEPARATIONS; NMR STUDIES; NOREPHEDRINE; SEPARATION OF ENANTIOMERS; Β-CD;

ENANTIOMERS;

ALPHA CYCLODEXTRIN DERIVATIVE; BETA CYCLODEXTRIN DERIVATIVE; CYCLODEXTRIN DERIVATIVE; HEPTAKIS(2,3 DI O ACETYL 6 O SULFO) BETA CYCLODEXTRIN; HEPTAKIS(2,3 DI O METHYL 6 O SULFO) BETA CYCLODEXTRIN; NOREPHEDRINE; UNCLASSIFIED DRUG;

ARTICLE; CAPILLARY ELECTROPHORESIS; CHEMICAL ANALYSIS; CHEMICAL INTERACTION; CHEMICAL STRUCTURE; CHIRAL CHROMATOGRAPHY; DRUG DETERMINATION; ENANTIOMER; ENANTIOSELECTIVITY; EXPERIMENTATION; NUCLEAR MAGNETIC RESONANCE; PROCESS OPTIMIZATION; PROTON NUCLEAR MAGNETIC RESONANCE; ROTATING FRAME NUCLEAR OVERHAUSER EXPERIMENT; SEPARATION TECHNIQUE;

EID: 84862865558     PISSN: 01730835     EISSN: 15222683     Source Type: Journal    
DOI: 10.1002/elps.201200062     Document Type: Article

References (37)

1. Chankvetadze, L., Ghibradze, N., Karchkhadze, M., Peng, L., Farkas, T., Chankvetadze, B., J. Chromatogr. A 2011, 1218, 6554-6560.
2. Dossou, K. S. S., Edorh, P. A., Chiap, P., Chankvetadze, B., Servais, A.-C., Fillet, M., Crommen, J., J. Sep. Sci. 2011, 34, 1772-1780.
3. Domínguez-Vega, E., Lomsadze, K., Chankvetadze, L., Salgado, A., Scriba, G. K. E., Calvo, E., López, J. A., Marina, M. L., Chankvetadze, B., Electrophoresis 2011, 32, 2640-2647.
4. Chankvetadze, B., Rev. Chem. Soc. 2004, 33, 337-347.
5. Scriba G. K. E., Electrophoresis 2003, 24, 2409-2421.
6. Chankvetadze, B., Electrophoresis 2002, 23, 4022-4035.
7. Chankvetadze, B., Electrophoresis 2009, 30, S211-S221.
8. Chankvetadze, B., Fillet, M., Burjanadze, N., Bergenthal, D., Bergander, C., Luftmann, H., Crommen, J., Blaschke, G., Enantiomer 2000, 5, 313-322.
9. Chankvetadze, B., Burjanadze, N., Crommen, J., Blaschke, G., Chromatographia 2001, 53, S-296-S-301.
10. Chankvetadze, B., Pintore, G., Burjanadze, N., Bergenthal, D., Strickmann, D., Cerri, R., Blaschke, G., Electrophoresis 1998, 19, 2101-2108.
11. Chankvetadze, B., Burjanadze, N., Pintore, G., Strickmann, D., Bergenthal, D., Blaschke, G., Chirality 1999, 11, 635-644.
12. Chankvetadze, B., Burjanadze, N., Santi, M., Massolini, G., Blaschke, G., J. Sep. Sci. 2002, 25, 733-740.
13. Castro-Puyana, M., Lomsadze, K., Crego, A. L., Marina, M. L., Chankvetadze, B., Electrophoresis 2007, 28, 388-394.
14. Chankvetadze, B., Lomsadze, K., Bergenthal, D., Breitkreutz, J., Bergander, K., Blaschke, G., Electrophoresis 2001, 22, 3178-3184.
15. Chankvetadze, B., Burjanadze, N., Maynard, D. M., Bergander, K., Bergenthal, D., Blaschke, G., Electrophoresis 2002, 23, 3027-3034.
16. Süß, F., Poppitz, W., Sänger-van de Griend, C. E., Scriba, G. K. E., Electrophoresis 2001, 22, 2416-2423.
17. Servais, A.-C., Rousseau, A., Fillet, M., Lomsadze, K., Salgado, A., Crommen, J., Chankvetadze, B., Electrophoresis 2010, 31, 1467-1474.
18. Servais, A.-C., Rousseau, A., Fillet, M., Lomsadze, K., Salgado, A., Crommen, J., Chankvetadze, B., J. Sep. Sci. 2010, 33, 1617-1624.
19. Chankvetadze, B., J. Chromatogr. A 1997, 792, 269-295.
20. Chankvetadze, B., Lindner, W., Scriba, G. K. E., Anal. Chem. 2004, 76, 4256-4260.
21. Lomsadze, K., Martínez-Girón, A. B., Castro-Puyana, M., Chankvetadze, L., Crego, A. L., Salgado, A., Marina, M. L., Chankvetadze, B., Electrophoresis 2009, 30, 2803-2811.
22. Hammitzsch-Wiedemann, M. M., Scriba, G. K. E., Anal. Chem. 2009, 81, 8765-8773.
23. Miyatake, N., Miyake, H., Nagashima, M., Takahashi, M., Yasuda, K., Yasuda, I., Yakugaku Zasshi 2004, 124, 333-339.
24. Iio, R., Chinaka, S., Takayama, N., Hayakawa, K., J. Health Sci. 2005, 51, 693-701.
25. Wedig, M., Holzgrabe, U., Electrophoresis 1999, 20, 2698-2704.
26. Iwata, Y. T., Kanamori, T., Ohmae, Y., Tsijikawa, K., Inoue, H., Kishi, T., Electrophoresis 2003, 24, 1770-1776.
27. Tábi, T., Magyar, K., Szöko, E., Electrophoresis 2003, 24, 2665-2673.
28. Hou, J., Zheng, Z., Rizvi, S. A. A., Shamsi, S. A., Electrophoresis 2007, 28, 1352-1363.
29. Hou, J., Zheng, Z., Shamsi, S. A., Electrophoresis 2007, 28, 1426-1434.
30. Borst, C., Holzgrabe, U., J. Pharm. Biomed. Anal. 2010, 53, 1201-1209.
31. Zheng, Z.-X., Ming, J.-L., Chan, W.-H., Lee, A. W. M., Huie, C. W., Electrophoresis 2004, 25, 3263-3269.
32. Mori, Y., Ueno, K., Umeda, T., J. Chromatogr. A 1997, 757, 328-332.
33. Hedeland, M., Nygård, M., Isaksson, R., Pettersson, C., Electrophoresis 2000, 21, 1587-1596.
34. Kasat, R. B., Franses, E. I., Wang, N.-H. L, Chirality 2010, 22, 565-579.
35. Kasat, R. B., Wang, N.-H. L., Franses, E. I., J. Chromatogr. A 2008, 1190, 110-119.
36. Takeo, K., Mitoh, H., Uemura, K., Carbohydr. Res. 1989, 187, 203-221.
37. Bax, A., Davis, D. G., J. Magn. Reson., 1985, 63, 207-213.