Novel synthesis and structural analysis of ferrihydrite

Inorganic Chemistry

Volumn 51, Issue 11, 2012, Pages 6421-6424

  Smith, Stacey J ^a,b   Page, Katharine ^c   Kim, Hyunjeong ^c   Campbell, Branton J ^b   Boerio Goates, Juliana ^a   Woodfield, Brian F ^a  

^a Brigham Young University   (United States)

^b BRIGHAM YOUNG UNIVERSITY   (United States)

^c LOS ALAMOS NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84861947955     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic300937f     Document Type: Article

References (34)

1. Michel, F. M.; Ehm, L.; Antao, S. M.; Lee, P. L.; Chupas, P. J.; Liu, G.; Strongin, D. R.; Schoonen, M. A. A.; Phillips, B. L.; Parise, J. B. The Structure of Ferrihydrite, a Nanocrystalline Material Science (Washington, DC, U. S.) 2007, 316, 1726-1729
2. Rancourt, D. G.; Fortin, D.; Pichler, T.; Thibault, P.-J.; Lamarche, G.; Morris, R. V.; Mercier, P. H. J. Mineralogy of a natural As-rich hydrous ferric oxide coprecipitate formed by mixing of hydrothermal fluid and seawater: implications regarding surface complexation and color banding in ferrihydrite deposits Am. Mineral. 2001, 86 (7-8) 834-851
3. Schwertmann, U.; Carlson, L.; Murad, E. Properties of iron oxides in two Finnish lakes in relation to the environment of their formation Clays Clay Miner. 1987, 35 (4) 297-304
4. Jambor, J. L.; Dutrizac, J. E. Occurrence and Constitution of Natural and Synthetic Ferrihydrite, a Widespread Iron Oxyhydroxide Chem. Rev. 1998, 98 (7) 2549-2585
5. Fortin, D.; Langley, S. Formation and occurrence of biogenic iron-rich minerals Earth-Sci. Rev. 2005, 72 (1-2) 1-19
6. Ford, R. G.; Bertsch, P. M.; Farley, K. J. Changes in Transition and Heavy Metal Partitioning during Hydrous Iron Oxide Aging Environ. Sci. Technol. 1997, 31 (7) 2028-2033
7. Raven, K. P.; Jain, A.; Loeppert, R. H. Arsenite and Arsenate Adsorption on Ferrihydrite: Kinetics, Equilibrium, and Adsorption Envelopes Environ. Sci. Technol. 1998, 32 (3) 344-349
8. Li, Z.; Zhang, T.; Li, K. One-step synthesis of mesoporous two-line ferrihydrite for effective elimination of arsenic contaminants from natural water Dalton Trans. 2011, 40 (9) 2062-2066
9. Huffman, G. P.; Ganguly, B.; Zhao, J.; Rao, K. R. P. M.; Shah, N.; Feng, Z.; Huggins, F. E.; Taghiei, M. M.; Lu, F. Structure and dispersion of iron-based catalysts for direct coal liquefaction Energy Fuels 1993, 7 (2) 285-296
10. Riveros, P. A.; Dutrizac, J. E.; Spencer, P. Arsenic disposal practices in the metallurgical industry Can. Metall. Q. 2001, 40 (4) 395-420
11. Mathew, T.; Suzuki, K.; Nagai, Y.; Nonaka, T.; Ikuta, Y.; Takahashi, N.; Suzuki, N.; Shinjoh, H. Mesoporous 2-Line Ferrihydrite by a Solution-Phase Cooperative Assembly Process for Removal of Organic Contaminants in Air Chem.-Eur. J. 2011, 17 (4) 1092-1095-S1092/1-S1092/9
12. Liu, G.; Debnath, S.; Paul, K. W.; Han, W.; Hausner, D. B.; Hosein, H.-A.; Michel, F. M.; Parise, J. B.; Sparks, D. L.; Strongin, D. R. Characterization and Surface Reactivity of Ferrihydrite Nanoparticles Assembled in Ferritin Langmuir 2006, 22 (22) 9313-9321
13. Lewin, A.; Moore, G. R.; Le Brun, N. E. Formation of protein-coated iron minerals Dalton Trans. 2005, 22, 3597-3610
14. Towe, K. M.; Bradley, W. F. Mineralogical constitution of colloidal ″hydrous ferric oxides″ J. Colloid Interface Sci. 1967, 24 (3) 384-92
15. Carta, D.; Casula, M. F.; Corrias, A.; Falqui, A.; Navarra, G.; Pinna, G. Structural and magnetic characterization of synthetic ferrihydrite nanoparticles Mater. Chem. Phys. 2009, 113 (1) 349-355
16. Anschutz, A. J.; Penn, R. L. Reduction of crystalline iron(III) oxyhydroxides using hydroquinone: influence of phase and particle size Geochem. Trans. 2005, 6 (3) 60-66
17. Schwertmann, U. F., J.; Kyek, A. Formation and properties of a continuous crystallinity series of synthetic ferrihydrites (2- to 6-line) and their relation to FeOOH forms Clays Clay Miner. 2004, 52 (2) 221-226
18. Dyer, L.; Fawell, P. D.; Newman, O. M. G.; Richmond, W. R. Synthesis and characterisation of ferrihydrite/silica co-precipitates J. Colloid Interface Sci. 2010, 348 (1) 65-70
19. Woodfield, B. F.; Liu, S.; Boerio-Goates, J.; Liu, Q.; Smith, S. J. Preparation of uniform nanoparticles of ultra-high purity metal oxides, mixed metal oxides, metals, and metal alloys. 2007-US4279, 2007098111, 20070216, 2007.
20. Smith, S. J.; Liu, S.; Liu, Q.; Olsen, R. E.; Boerio-Goates, J.; Woodfield, B. F. Mechanism behind the ″solvent-deficient″ synthetic method. Chem. Mater. 2012, in press.
21. Smith, S. J.; Liu, S.; Liu, Q.; Olsen, R. E.; Rytting, M.; Selck, D. A.; Simmons, C. L.; Boerio-Goates, J.; Woodfield, B. F. Synthesis of metal oxide nanoparticles via a robust "solvent-deficient" method. Chem. Mater. 2012, in press.
22. Fit2D V. 9.129 reference manual V. 3.1.
23. Qiu, X.; Thompson, J. W.; Billinge, S. J. L. PDFgetX2: a GUI-driven program to obtain the pair distribution function from X-ray powder diffraction data J. Appl. Crystallogr. 2004, 37 (4) 678
24. Egami, T. B.; S., J. L., Underneath the Bragg Peaks: Structural Analysis of Complex Materials; 1 st ed.; Pergamon: Kidlington, Oxford, U.K., 2003; Vol. 7, p 404.
25. Farrow, C. L.; Juhas, P.; Liu, J. W.; Bryndin, D.; Bozin, E. S.; Bloch, J.; Proffen, T.; Billinge, S. J. L. PDFfit2 and PDFgui: computer programs for studying nanostructure in crystals J. Phys.: Condens. Matter 2007, 19 (33) 335219/1-335219/7
26. Kukkadapu, R. K.; Zachara, J. M.; Fredrickson, J. K.; Smith, S. C.; Dohnalkova, A. C.; Russell, C. K. Transformation of 2-line ferrihydrite to 6-line ferrihydrite under oxic and anoxic conditions Am. Mineral. 2003, 88, 1903-1914
27. Schwertmann, U.; Friedl, J.; Stanjek, H.; From, Fe(III ions to ferrihydrite and then to hematite J. Colloid Interface Sci. 1999, 209 (1) 215-223
28. Nanda, K. K.; Maisels, A.; Kruis, F. E.; Fissan, H.; Stappert, S. Higher surface energy of free nanoparticles Phys. Rev. Lett. 2003, 91 (10) 106102/1-106102/4
29. Jansen, E.; Kyek, A.; Schafer, W.; Schwertmann, U. The structure of six-line ferrihydrite Appl. Phys. A: Mater. Sci. Process 2002, 74 (Suppl., Pt. 2) S1004-S1006
30. Maillot, F.; Morin, G.; Wang, Y.; Bonnin, D.; Ildefonse, P.; Chaneac, C.; Calas, G. New insight into the structure of nanocrystalline ferrihydrite: EXAFS evidence for tetrahedrally coordinated iron(III) Geochim. Cosmochim. Acta 2011, 75 (10) 2708-2720
31. Drits, V. A.; Sakharov, B. A.; Salyn, A. L.; Manceau, A. Structural model for ferrihydrite Clay Miner. 1993, 28 (2) 185-207
32. Chukhrov, F. V.; Zvyagin, B. B.; Gorshkov, A. I.; Ermilova, L. P.; Balashova, V. V. Ferrihydrite Izvestiya Akademii Nauk SSSR, Seriya Geologicheskaya 1973, 4, 23-33
33. Casey, W. H. Large Aqueous Aluminum Hydroxide Molecules Chem. Rev. 2006, 106 (1) 1-16
34. Paglia, G.; Bozin, E. S.; Billinge, S. J. L. Fine-Scale Nanostructure in gamma -Al2O3 Chem. Mater. 2006, 18 (14) 3242-3248