Improving the double quantum filtered COSY experiment by "moving Tube" NMR

Journal of Magnetic Resonance

Volumn 219, Issue , 2012, Pages 41-45

  Donovan, Kevin J ^a,b   Allen, Mary ^a   Martin, Rachel W ^a   Shaka, A J ^a  

^a UNIVERSITY OF CALIFORNIA   (United States)

^b WEIZMANN INSTITUTE OF SCIENCE   (Israel)

Author keywords

2D NMR; Double quantum; DQF COSY; Moving tube; MT NMR; Rapid pulsing artifacts; Sensitivity

Indexed keywords

DOUBLE-QUANTUM; DQF-COSY; MOVING TUBE; RAPID PULSING ARTIFACTS; SENSITIVITY;

EXPERIMENTS; HARDWARE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SPECTROSCOPIC ANALYSIS;

TUBES (COMPONENTS);

ARTICLE; EQUIPMENT; EQUIPMENT DESIGN; INSTRUMENTATION; LABORATORY DIAGNOSIS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

EQUIPMENT DESIGN; EQUIPMENT FAILURE ANALYSIS; MAGNETIC RESONANCE SPECTROSCOPY; SPECIMEN HANDLING;

EID: 84861618254     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2012.03.007     Document Type: Article

References (15)

1. C.T. Turner, and S.L. Patt Artifacts in two-dimensional NMR J. Magn. Reson. 85 1989 492 505
2. A.D. Bain, I.W. Burton, and W.F. Reynolds Artifacts in two-dimensional NMR Prog. Nucl. Magn. Reson. Spectrosc. 26 1994 59 89 (Pubitemid 124003824)
3. A.E. Derome, and M.P. Williamson Rapid-pulsing artifacts in double-quantum-filtered COSY J. Magn. Reson. 88 1990 177 185
4. M. Rance, O.W. Sorensen, G. Bodenhausen, G. Wagner, R.R. Ernst, and K. Wüthrich Improved spectral resolution in COSY 1H NMR spectra of proteins via double quantum filtering Biochem. Biophys. Res. Commun. 117 1983 479 485
5. C.J. Turner Phase cycling in double-quantum-filtered COSY J. Magn. Reson. 96 1992 551 562
6. C.J. Turner, and W.C. Hutton Suppression of artifacts in phase-sensitive COSY J. Magn. Reson. 100 1992 469 483
7. J.G. Bowden, and P.M.J. Elimination of longitudinal multiple-quantum artifacts in 2D COSY spectra J. Magn. Reson. 107 1994 32 39
8. J.K. Hardy, and P.L. Rinaldi Principal component analysis for artifact reduction in COSY spectra J. Magn. Reson. 88 1990 320 333
9. P.L. Rinaldi, and D.J. Iverson A new method of 2D NMR data collection for time-saving and artifact reduction J. Magn. Reson. 92 1991 528 537
10. 1 artifacts in two-dimensional NMR spectroscopy J. Magn. Reson. 140 1999 513 515 (Pubitemid 129608318)
11. A.A. Shaw, C. Salaun, J.-F. Dauphin, and B. Ancian Artifact-free PFG-enhanced double-quantum-filtered COSY experiments J. Magn. Reson. Ser. A 120 1996 110 115 (Pubitemid 126751744)
12. B. Ancian, I. Bourgeois, J.-F. Dauphin, and A.A. Shaw Artifact-free pure absorption PFG-enhanced DQF-COSY spectra including a gradient pulse in the evolution period J. Magn. Reson. 125 1997 348 354 (Pubitemid 127451896)
13. K.J. Donovan, M. Allen, R.W. Martin, and A. Shaka Sensitive, quantitative carbon-13 NMR spectra by mechanical sample translation J. Magn. Reson. 197 2009 237 241
14. D. Marion, and K. Wüthrich Application of phase sensitive two-dimensional correlated spectroscopy (COSY) for measurements of 1H-1H spin-spin coupling constants in proteins Biochem. Biophys. Res. Commun. 113 1983 967 974
15. C.A. Michal Magnetic field homogeneity: a new approach to orthogonalizing and optimizing shim gradients J. Magn. Reson. 185 2007 110 117 (Pubitemid 46484408)