Toward single-shot pure-shift solution 1H NMR by trains of BIRD-based homonuclear decoupling

Journal of Magnetic Resonance

Volumn 218, Issue , 2012, Pages 141-146

  Lupulescu, Adonis ^a   Olsen, Gregory L ^a   Frydman, Lucio ^a  

^a WEIZMANN INSTITUTE OF SCIENCE   (Israel)

Author keywords

1D NMR; BIRD pulses; Homonuclear J decoupling; Resolution enhancement

Indexed keywords

ANALYTICAL APPLICATIONS; HETERONUCLEAR DECOUPLING; HOMONUCLEAR; HOMONUCLEAR DECOUPLING; J-DECOUPLING; LIQUID STATE; REPRESENTATIVE COMPOUND; RESOLUTION ENHANCEMENT; SINGLE-SHOT;

BIOCHEMISTRY; RESONANCE;

PROTONS;

EID: 84861094415     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2012.02.018     Document Type: Article

References (28)

1. R. Freeman, and W.A. Anderson Use of weak perturbing radio-frequency fields in nuclear magnetic double resonance J. Chem. Phys. 37 1962 2053 2073
2. R. Freeman, J.B. Grutzner, G.A. Morris, and D.L. Turner Carbon-13 nuclear magnetic resonance spectra with coherent proton decoupling: peak-height distortions within spin multiplets J. Am. Chem. Soc 100 1978 5637 5640
3. W.P. Aue, J. Karhan, and R.R. Ernst Homonuclear broad band decoupling and two-dimensional J-resolved NMR spectroscopy J. Chem. Phys. 64 1976 4226 4227
4. A. Bax, and R. Freeman Investigation of complex networks of spin-spin coupling by two-dimensional NMR J. Magn. Reson. 44 1981 542 561
5. J.R. Garbow, D.P. Weitekamp, and A. Pines Bilinear rotation decoupling of homonuclear scalar interactions Chem. Phys. Lett. 93 1982 504 509
6. A. Bax Broadband homonuclear decoupling in heteronuclear shift correlation NMR spectroscopy J. Magn. Reson. 53 1983 517 520
7. 1-decoupled 2D correlation spectra to the study of proteins J. Magn. Reson. 59 1984 250 261
8. A.J. Shaka, J. Keeler, and R. Freeman Separation of chemical shifts and spin coupling in proton NMR. Elimination of dispersion signals from two-dimensional spectra J. Magn. Reson. 56 1984 294 313
9. 1 decoupling in two-dimensional NOE spectroscopy J. Am. Chem. Soc. 107 1985 7778 7779
10. 1 decoupling in two-dimensional NMR spectroscopy J. Magn. Res. 78 1988 178 185
11. M.A. McCoy, and L. Mueller Selective shaped pulse decoupling in NMR: homonuclear [carbon-13]carbonyl decoupling J. Am. Chem. Soc. 114 1992 2108 2112
12. M. Woodley, and R. Freeman Elimination of spin-spin splittings from high-resolution proton NMR spectra J. Magn. Reson. A 111 1994 225 228
13. J. Nuzillard Time-reversal of NMR signals by linear prediction. Application to phase-sensitive homonuclear J-resolved spectroscopy J. Magn. Reson. A 118 1996 132 135
14. K. Zangger, and H. Sterk Homonuclear broadband-decoupled NMR spectra J. Magn. Reson. 124 1997 486 489
15. A.J. Pell, R.A.E. Edden, and J. Keeler Broadband proton-decoupled proton spectra Magn. Reson. Chem. 45 2007 296 316
16. A.J. Pell, and J. Keeler Two-dimensional J-spectra with absorption-mode lineshapes J. Magn. Reson. 189 2007 293 299
17. J.A. Aguilar, S. Faulkner, M. Nilsson, and G.A. Morris Pure shift 1H NMR: a resolution of the resolution problem? Angew. Chem. Int. Ed. 49 2010 3901 3903
18. B. Baishya, T.F. Segawa, and G. Bodenhausen Quenching homonuclear couplings in magnetic resonance by trains of non-refocusing pulses J. Magn. Reson 211 2011 240 242
19. J.A. Aguilar, M. Nilsson, and G.A. Morris Simple proton spectra from complex spin systems: pure shift NMR spectroscopy using BIRD Angew. Chem 123 2011 9890 9891
20. A.J. Shaka, and J. Keeler Broadband spin decoupling in isotropic-liquids Prog. Nucl. Magn. Reson. Spectrosc. 19 1987 1 47
21. A.J. Shaka, P.B. Barker, and R. Freeman Computer-optimized decoupling scheme for wideband applications and low-level operation J. Magn. Reson. 64 1985 547 552
22. T. Gullion, D.B. Baker, and M.S. Conradi New, compensated carr-purcell sequences J. Magn. Reson. 89 1989 479 484
23. M.H. Levitt Composite pulses Prog. Nucl. Magn. Reson. Spectrosc. 18 1986 61 122
24. E. Kupče, and R. Freeman Compensation for spin-spin coupling effects during adiabatic pulses J. Magn. Reson. 127 1997 36 48
25. E. Kupče, and R. Freeman Fast multidimensional NMR by polarization sharing Magn. Reson. Chem. 45 2007 2 4
26. H. Hatanaka, and C.S. Yannoni Selective creation of coherence by nonselective excitation in a spin-1 system J. Magn. Reson. 42 1981 330 333
27. T. Carlomagno, W. Peti, and C. Griesinger A new method for the simultaneous measurement of magnitude and sign of 1DCH and 1DHH dipolar couplings in methylene groups J. Biomol. NMR 17 2000 99 109
28. E. Miclet, D.C. Williams Jr., G.M. Clore, D.L. Bryce, J. Boisbouvier, and A. Bax Relaxation-optimized NMR spectroscopy of methylene groups in proteins and nucleic acids J. Am. Chem. Soc. 126 2004 10560 10570