메뉴 건너뛰기




Volumn 19, Issue 3, 2012, Pages 993-1004

Critical re-investigation of the alditol acetate method for analysis of substituent distribution in methyl cellulose

Author keywords

Alditol acetate method; Gas liquid chromatography; Methyl cellulose; Monomer analysis; Substituent distribution

Indexed keywords

1-METHYLIMIDAZOLE; ACIDIC CONDITIONS; ALDITOL ACETATE; CRITICAL POINTS; FREE HYDROXYL GROUPS; GAS-LIQUID CHROMATOGRAPHY; METHYL CELLULOSE; MONOMER UNITS; NO REMOVAL; REFERENCE METHOD; REPRODUCIBILITIES; SIDE REACTIONS; SUBSTITUENT DISTRIBUTION; SUGAR ANALYSIS; TIME REQUIREMENTS;

EID: 84860361719     PISSN: 09690239     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10570-012-9663-y     Document Type: Article
Times cited : (26)

References (39)
  • 1
    • 14344263010 scopus 로고    scopus 로고
    • A novel method for the analysis of the substitution pattern of O-methyl-[alpha]-and [beta]-1,4-glucans by means of electrospray ionisation-mass spectrometry/collision induced dissociation
    • Adden R, Mischnick P (2005) A novel method for the analysis of the substitution pattern of O-methyl-[alpha]-and [beta]-1, 4-glucans by means of electrospray ionisation-mass spectrometry/collision induced dissociation. Int J Mass Spectrom 242: 63-73.
    • (2005) Int J Mass Spectrom , vol.242 , pp. 63-73
    • Adden, R.1    Mischnick, P.2
  • 2
    • 33744547386 scopus 로고    scopus 로고
    • New approaches to the analysis of enzymatically hydrolyzed methyl cellulose. Part 1. Investigation of the influence of structural parameters on the extent of degradation
    • Adden R, Melander C, Brinkmalm G, Gorton L, Mischnick P (2006a) New approaches to the analysis of enzymatically hydrolyzed methyl cellulose. Part 1. Investigation of the influence of structural parameters on the extent of degradation. Biomacromolecules 7: 1399-1409.
    • (2006) Biomacromolecules , vol.7 , pp. 1399-1409
    • Adden, R.1    Melander, C.2    Brinkmalm, G.3    Gorton, L.4    Mischnick, P.5
  • 3
    • 33745308244 scopus 로고    scopus 로고
    • Fractionation of methyl cellulose according to polarity-a tool to differentiate first and second order heterogeneity of the substituent distribution
    • Adden R, Müller R, Mischnick P (2006b) Fractionation of methyl cellulose according to polarity-a tool to differentiate first and second order heterogeneity of the substituent distribution. Macromol Chem Phys 207: 954-965.
    • (2006) Macromol Chem Phys , vol.207 , pp. 954-965
    • Adden, R.1    Müller, R.2    Mischnick, P.3
  • 4
    • 33144479482 scopus 로고    scopus 로고
    • Comprehensive analysis of the substituent distribution in the glucosyl units and along the polymer chain of hydroxyethylmethyl celluloses and statistical evaluation
    • Adden R, Niedner W, Müller R, Mischnick P (2006c) Comprehensive analysis of the substituent distribution in the glucosyl units and along the polymer chain of hydroxyethylmethyl celluloses and statistical evaluation. Anal Chem 78: 1146-1157.
    • (2006) Anal Chem , vol.78 , pp. 1146-1157
    • Adden, R.1    Niedner, W.2    Müller, R.3    Mischnick, P.4
  • 5
    • 49949140444 scopus 로고
    • Mass spectrometry of partially methylated alditol acetates
    • Björndal H, Lindberg B, Svensson S (1967) Mass spectrometry of partially methylated alditol acetates. Carbohydr Res 5: 433-440.
    • (1967) Carbohydr Res , vol.5 , pp. 433-440
    • Björndal, H.1    Lindberg, B.2    Svensson, S.3
  • 6
    • 84981919275 scopus 로고
    • Gas-liquid chromatography and mass spectrometry in methylation analysis of polysaccharides
    • Björndal H, Hellerqvist CG, Lindberg B, Svensson S (1970) Gas-liquid chromatography and mass spectrometry in methylation analysis of polysaccharides. Angew Chem Int Ed Engl 9: 610-619.
    • (1970) Angew Chem Int Ed Engl , vol.9 , pp. 610-619
    • Björndal, H.1    Hellerqvist, C.G.2    Lindberg, B.3    Svensson, S.4
  • 7
    • 37649010407 scopus 로고
    • A simple and rapid preparation of alditol acetates for monosaccharide analysis
    • Blakeney AB, Harris PJ, Henry RJ, Stone BA (1983) A simple and rapid preparation of alditol acetates for monosaccharide analysis. Carbohydr Res 113: 291-299.
    • (1983) Carbohydr Res , vol.113 , pp. 291-299
    • Blakeney, A.B.1    Harris, P.J.2    Henry, R.J.3    Stone, B.A.4
  • 8
    • 4243620067 scopus 로고
    • Mechanism in carbohydrate chemistry
    • Capon B (1969) Mechanism in carbohydrate chemistry. Chem Rev 69: 407-498.
    • (1969) Chem Rev , vol.69 , pp. 407-498
    • Capon, B.1
  • 9
    • 0002380473 scopus 로고
    • Linkage structure of carbohydrates by gas chromatography-mass spectrometry (GC-MS) of partially methylated alditol acetates
    • C. J. Biermann and G. D. McGinnis (Eds.), Boca Raton, FL: CRC Press
    • Carpita NC, Shea EM (1989) Linkage structure of carbohydrates by gas chromatography-mass spectrometry (GC-MS) of partially methylated alditol acetates. In: Biermann CJ, McGinnis GD (eds) Analysis of carbohydrates by GC and MS. CRC Press, Boca Raton, FL, pp 157-216.
    • (1989) Analysis of Carbohydrates by GC and MS , pp. 157-216
    • Carpita, N.C.1    Shea, E.M.2
  • 10
    • 34447326804 scopus 로고
    • A simple and rapid method for the permethylation of carbohydrates
    • Ciucanu I, Kerek F (1984) A simple and rapid method for the permethylation of carbohydrates. Carbohydr Res 131: 209-217.
    • (1984) Carbohydr Res , vol.131 , pp. 209-217
    • Ciucanu, I.1    Kerek, F.2
  • 11
    • 0024287887 scopus 로고
    • Analysis of positions of substitution of O-methyl or O-ethyl groups in partially methylated or ethylated cellulose by the reductive-cleavage method
    • D'Ambra AJ, Rice MJ, Zeller SG, Gruber PR, Gray GR (1988) Analysis of positions of substitution of O-methyl or O-ethyl groups in partially methylated or ethylated cellulose by the reductive-cleavage method. Carbohydr Res 177: 111-116.
    • (1988) Carbohydr Res , vol.177 , pp. 111-116
    • D'Ambra, A.J.1    Rice, M.J.2    Zeller, S.G.3    Gruber, P.R.4    Gray, G.R.5
  • 12
    • 84942400895 scopus 로고
    • Trifluoressigsäure zur schnellen und schonenden Hydrolyse von Cellulose und anderen Polysacchariden
    • Fengel D, Wegener G, Heizmann A, Przyklenk M (1977) Trifluoressigsäure zur schnellen und schonenden Hydrolyse von Cellulose und anderen Polysacchariden. Holzforschung 31: 65-71.
    • (1977) Holzforschung , vol.31 , pp. 65-71
    • Fengel, D.1    Wegener, G.2    Heizmann, A.3    Przyklenk, M.4
  • 13
    • 13444299645 scopus 로고
    • Polysaccharides elaborated by Armillaria mellea (tricholomataceae): Part I. A water-soluble polysaccharide from the fruit bodies
    • Fraser RN, Lindberg B (1967) Polysaccharides elaborated by Armillaria mellea (tricholomataceae): Part I. A water-soluble polysaccharide from the fruit bodies. Carbohydr Res 4: 12-19.
    • (1967) Carbohydr Res , vol.4 , pp. 12-19
    • Fraser, R.N.1    Lindberg, B.2
  • 17
    • 0037137195 scopus 로고    scopus 로고
    • Preparation and structural characterisation of O-aminopropyl starch and amylose
    • Gonera A, Goclik V, Baum M, Mischnick P (2002) Preparation and structural characterisation of O-aminopropyl starch and amylose. Carbohydr Res 337: 2263-2272.
    • (2002) Carbohydr Res , vol.337 , pp. 2263-2272
    • Gonera, A.1    Goclik, V.2    Baum, M.3    Mischnick, P.4
  • 18
    • 0002949950 scopus 로고
    • Analysis of sugar mixtures by gas-liquid partition chromatography
    • Gunner SW, Jones JKN, Perry MB (1961) Analysis of sugar mixtures by gas-liquid partition chromatography. Chem Ind (London) 6: 255-256.
    • (1961) Chem Ind (London) , vol.6 , pp. 255-256
    • Gunner, S.W.1    Jones, J.K.N.2    Perry, M.B.3
  • 19
    • 77955764774 scopus 로고
    • A Rapid permethylation of glycolipid, and polysaccharide catalyzed by methylsulfinyl carbanion in dimethyl sulfoxide
    • Hakomori S-I (1964) A Rapid permethylation of glycolipid, and polysaccharide catalyzed by methylsulfinyl carbanion in dimethyl sulfoxide. J Biochem (Tokyo) 55: 205-208.
    • (1964) J Biochem (Tokyo) , vol.55 , pp. 205-208
    • Hakomori, S.-I.1
  • 20
    • 0028452841 scopus 로고
    • Methylation analysis of complex carbohydrates: Overview and critical comments
    • Hanisch FG (1994) Methylation analysis of complex carbohydrates: Overview and critical comments. Biol Mass Spectrom 23: 309-312.
    • (1994) Biol Mass Spectrom , vol.23 , pp. 309-312
    • Hanisch, F.G.1
  • 21
    • 0021753546 scopus 로고
    • An improved procedure for the methylation analysis of oligosaccharides and polysaccharides
    • Harris PJ, Henry RJ, Blakeney AB, Stone BA (1984) An improved procedure for the methylation analysis of oligosaccharides and polysaccharides. Carbohydr Res 127: 59-73.
    • (1984) Carbohydr Res , vol.127 , pp. 59-73
    • Harris, P.J.1    Henry, R.J.2    Blakeney, A.B.3    Stone, B.A.4
  • 22
    • 0016849974 scopus 로고
    • Quantitative analysis of iduronic acid and glucuronic acid in sulfated galactosaminoglycuronans by gas chromatography
    • Inoue S, Miyawaki M (1975) Quantitative analysis of iduronic acid and glucuronic acid in sulfated galactosaminoglycuronans by gas chromatography. Anal Biochem 65: 164-174.
    • (1975) Anal Biochem , vol.65 , pp. 164-174
    • Inoue, S.1    Miyawaki, M.2
  • 23
    • 0030516968 scopus 로고    scopus 로고
    • The methylation reaction in carbohydrate analysis
    • Jay A (1996) The methylation reaction in carbohydrate analysis. J Carbohydr Chem 15: 897-923.
    • (1996) J Carbohydr Chem , vol.15 , pp. 897-923
    • Jay, A.1
  • 24
    • 0000077145 scopus 로고
    • Prediction of gas chromatography flame ionization detector response factors from molecular structures
    • Jorgensen AD, Picel KC, Stamoudis VC (1990) Prediction of gas chromatography flame ionization detector response factors from molecular structures. Anal Chem 62: 683-689.
    • (1990) Anal Chem , vol.62 , pp. 683-689
    • Jorgensen, A.D.1    Picel, K.C.2    Stamoudis, V.C.3
  • 25
    • 0023655196 scopus 로고
    • A new catalyst for reductive cleavage of methylated glycans
    • Jun J-G, Gray GR (1987) A new catalyst for reductive cleavage of methylated glycans. Carbohydr Res 163: 247-261.
    • (1987) Carbohydr Res , vol.163 , pp. 247-261
    • Jun, J.-G.1    Gray, G.R.2
  • 26
    • 0000806061 scopus 로고
    • Distribution of substituents in O-ethyl-O-(2-hydroxy-ethyl) cellulose
    • Lindberg B, Lindquist U, Stenberg O (1988) Distribution of substituents in O-ethyl-O-(2-hydroxy-ethyl) cellulose. Carbohydr Res 176: 137-144.
    • (1988) Carbohydr Res , vol.176 , pp. 137-144
    • Lindberg, B.1    Lindquist, U.2    Stenberg, O.3
  • 27
    • 0030565602 scopus 로고    scopus 로고
    • Model studies on methyl amyloses: correlation between reaction conditions and primary structure
    • Mischnick P, Kühn G (1996) Model studies on methyl amyloses: correlation between reaction conditions and primary structure. Carbohydr Res 290: 199-207.
    • (1996) Carbohydr Res , vol.290 , pp. 199-207
    • Mischnick, P.1    Kühn, G.2
  • 28
    • 77955473282 scopus 로고    scopus 로고
    • Homogeneous methylation of wood pulp cellulose dissolved in LiOH/urea/H2O
    • Nagel MCV, Koschella A, Voiges K, Mischnick P, Heinze T (2010) Homogeneous methylation of wood pulp cellulose dissolved in LiOH/urea/H2O. Eur Polym J 46: 1726-1735.
    • (2010) Eur Polym J , vol.46 , pp. 1726-1735
    • Nagel, M.C.V.1    Koschella, A.2    Voiges, K.3    Mischnick, P.4    Heinze, T.5
  • 29
    • 0028375915 scopus 로고
    • A critical assessment of a one-tube procedure for the linkage analysis of polysaccharides as partially methylated alditol acetates
    • Needs PW, Selvendran RR (1994) A critical assessment of a one-tube procedure for the linkage analysis of polysaccharides as partially methylated alditol acetates. Carbohydr Res 254: 229-244.
    • (1994) Carbohydr Res , vol.254 , pp. 229-244
    • Needs, P.W.1    Selvendran, R.R.2
  • 30
    • 0028255064 scopus 로고
    • Characterization of cellulose and cellulose derivatives in solution by high resolution 13C-NMR spectroscopy
    • Nehls I, Wagenknecht W, Philipp B, Stscherbina D (1994) Characterization of cellulose and cellulose derivatives in solution by high resolution 13C-NMR spectroscopy. Prog Polym Sci 19: 29-78.
    • (1994) Prog Polym Sci , vol.19 , pp. 29-78
    • Nehls, I.1    Wagenknecht, W.2    Philipp, B.3    Stscherbina, D.4
  • 31
    • 0014094243 scopus 로고
    • Gas-liquid chromatography of alditol acetates and its application to the analysis of sugars in complex hydrolysates
    • Oades JM (1967) Gas-liquid chromatography of alditol acetates and its application to the analysis of sugars in complex hydrolysates. J Chromatogr A 28: 246-252.
    • (1967) J Chromatogr A , vol.28 , pp. 246-252
    • Oades, J.M.1
  • 32
    • 0019980770 scopus 로고
    • Reductive cleavage of glycosides
    • Rolf D, Gray GR (1982) Reductive cleavage of glycosides. J Am Chem Soc 104: 3539-3541.
    • (1982) J Am Chem Soc , vol.104 , pp. 3539-3541
    • Rolf, D.1    Gray, G.R.2
  • 33
    • 0034824586 scopus 로고    scopus 로고
    • A new approach in the analysis of the substituent distribution of carboxymethyl celluloses
    • Saake B, Horner S, Puls J, Heinze T, Koch W (2001) A new approach in the analysis of the substituent distribution of carboxymethyl celluloses. Cellulose 8: 59-67.
    • (2001) Cellulose , vol.8 , pp. 59-67
    • Saake, B.1    Horner, S.2    Puls, J.3    Heinze, T.4    Koch, W.5
  • 34
    • 0002432128 scopus 로고
    • Kinetics of wood saccharification-hydrolysis of cellulose and decomposition of sugars in dilute acid at high temperature
    • Saeman JF (1945) Kinetics of wood saccharification-hydrolysis of cellulose and decomposition of sugars in dilute acid at high temperature. Ind Eng Chem 37: 43-52.
    • (1945) Ind Eng Chem , vol.37 , pp. 43-52
    • Saeman, J.F.1
  • 35
    • 0022112648 scopus 로고
    • Calculation of flame ionization detector relative response factors using the effective carbon number concept
    • Scanlon JT, Willis DE (1985) Calculation of flame ionization detector relative response factors using the effective carbon number concept. J Chromatogr Sci 23: 333-339.
    • (1985) J Chromatogr Sci , vol.23 , pp. 333-339
    • Scanlon, J.T.1    Willis, D.E.2
  • 36
    • 0018791923 scopus 로고
    • Determination of aldoses and uronic acid content of vegetable fiber
    • Selvendran RR, March JF, Ring SG (1979) Determination of aldoses and uronic acid content of vegetable fiber. Anal Biochem 96: 282-292.
    • (1979) Anal Biochem , vol.96 , pp. 282-292
    • Selvendran, R.R.1    March, J.F.2    Ring, S.G.3
  • 37
    • 0026428333 scopus 로고
    • Chemical methods for the analysis of sulphated galactans from red algae
    • Stevenson TT, Furneaux RH (1991) Chemical methods for the analysis of sulphated galactans from red algae. Carbohydr Res 210: 277-298.
    • (1991) Carbohydr Res , vol.210 , pp. 277-298
    • Stevenson, T.T.1    Furneaux, R.H.2
  • 38
    • 0000866236 scopus 로고
    • Quantitative analysis by various g.l.c. response-factor theories for partially methylated and partially ethylated alditol acetates
    • Sweet DP, Shapiro RH, Albersheim P (1975) Quantitative analysis by various g. l. c. response-factor theories for partially methylated and partially ethylated alditol acetates. Carbohydr Res 40: 217-225.
    • (1975) Carbohydr Res , vol.40 , pp. 217-225
    • Sweet, D.P.1    Shapiro, R.H.2    Albersheim, P.3
  • 39
    • 0002761969 scopus 로고
    • Chemical analysis of lignocellulose materials
    • Theander O (1991) Chemical analysis of lignocellulose materials. Anim Feed Sci Technol 32: 35-44.
    • (1991) Anim Feed Sci Technol , vol.32 , pp. 35-44
    • Theander, O.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.