In situ X-ray diffraction study of Na+ saturated montmorillonite exposed to variably wet super critical CO2

Environmental Science and Technology

Volumn 46, Issue 7, 2012, Pages 4241-4248

  Ilton, Eugene S ^a   Schaef, H Todd ^a   Qafoku, Odeta ^a   Rosso, Kevin M ^a   Felmy, Andrew R ^a  

^a PACIFIC NORTHWEST NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CAP ROCK; CONTROL EXPERIMENTS; DEHYDRATION REACTIONS; DIOCTAHEDRAL SMECTITE; GEOLOGIC STORAGE; HIGH-PRESSURE X-RAY DIFFRACTIONS; HYDRATION STATE; IN-SITU; INITIAL CONDITIONS; INTERLAYER EXPANSION; INTERLAYER REGIONS; STEADY STATE; SUPER-CRITICAL; TRAPPING MECHANISMS;

CLAY MINERALS; DEHYDRATION; HYDRATION; SODIUM; X RAY DIFFRACTION;

CARBON DIOXIDE;

CARBON DIOXIDE; MONTMORILLONITE; SODIUM;

CAP ROCK; CARBON DIOXIDE; CARBON SEQUESTRATION; CATION; DEHYDRATION; HYDRATION; MONTMORILLONITE; SATURATION; SMECTITE; SODIUM; UNDERGROUND STORAGE; X-RAY DIFFRACTION;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; CLAY; HYDRATION; STEADY STATE; WATER SUPPLY; X RAY DIFFRACTION;

BENTONITE; CARBON DIOXIDE; PRESSURE; SILICATES; SODIUM; TEMPERATURE; WATER; X-RAY DIFFRACTION;

EID: 84859341184     PISSN: 0013936X     EISSN: 15205851     Source Type: Journal    
DOI: 10.1021/es300234v     Document Type: Article

References (51)

1. Benson, S. M.; Cole, D. R. CO(2) Sequestration in Deep Sedimentary Formations Elements 2008, 4, 325-331
2. Xu, T. F.; Apps, J. A.; Pruess, K. Numerical simulation of CO2 disposal by mineral trapping in deep aquifers Appl. Geochem. 2004, 19, 917-936
3. McGrail, B. P.; Schaef, H. T.; Ho, A. M.; Chien, Y. J.; Dooley, J. J.; Davidson, C. L. Potential for carbon dioxide sequestration in flood basalts J. Geophys. Res.-Solid Earth 2006, 111
4. Oelkers, E. H.; Gislason, S. R.; Matter, J. Mineral Carbonation of CO(2) Elements 2008, 4, 333-337
5. Schaef, H. T.; McGrail, B. P.; Owen, A. T. Carbonate mineralization of volcanic province basalts Int. J. Greenhouse Gas Control 2010, 4, 249-261
6. Giammar, D. E.; Bruant, R. G.; Peters, C. A. Forsterite dissolution and magnesite precipitation at conditions relevant for deep saline aquifer storage and sequestration of carbon dioxide Chem. Geol. 2005, 217, 257-276
7. King, H. E.; Plumper, O.; Putnis, A. Effect of Secondary Phase Formation on the Carbonation of Olivine Environ. Sci. Technol. 2010, 44, 6503-6509
8. Garcia, B.; Beaumont, V.; Perfetti, E.; Rouchon, V.; Blanchet, D.; Oger, P.; Dromart, G.; Huc, A. Y.; Haeseler, F. Experiments and geochemical modelling of CO(2) sequestration by olivine: Potential, quantification Appl. Geochem. 2010, 25, 1383-1396
9. Daval, D.; Sissmann, O.; Menguy, N.; Saldi, G. D.; Guyot, F.; Martinez, I.; Corvisier, J.; Garcia, B.; Machouk, I.; Knauss, K. G.; Hellmann, R. Influence of amorphous silica layer formation on the dissolution rate of olivine at 90 degrees C and elevated pCO(2) Chem. Geol. 2011, 284, 193-209
10. Kwak, J. H.; Hu, J. Z.; Turcu, R. V. F.; Rosso, K. M.; Ilton, E. S.; Wang, C. M.; Sears, J. A.; Engelhard, M. H.; Felmy, A. R.; Hoyt, D. W. The role of H(2)O in the carbonation of forsterite in supercritical CO(2) Int. J. Greenhouse Gas Control 2011, 5, 1081-1092
11. Kwak, J. H.; Hu, J. Z.; Hoyt, D. W.; Sears, J. A.; Wang, C. M.; Rosso, K. M.; Felmy, A. R. Metal Carbonation of Forsterite in Supercritical CO(2) and H(2)O Using Solid State (29)Si, (13)C NMR Spectroscopy J. Phys. Chem. C 2010, 114, 4126-4134
12. Loring, J. S.; Thompson, C. J.; Wang, Z. M.; Joly, A. G.; Sklarew, D. S.; Schaef, H. T.; Ilton, E. S.; Rosso, K. M.; Felmy, A. R. In Situ Infrared Spectroscopic Study of Forsterite Carbonation in Wet Supercritical CO(2) Environ. Sci. Technol. 2011, 45, 6204-6210
13. Matter, J. M.; Takahashi, T.; Goldberg, D. Experimental evaluation of in situ CO2-water-rock reactions during CO2 injection in basaltic rocks: Implications for geological CO2 sequestration Geochem., Geophys., Geosyst. 2007, 8
14. Matter, J. M.; Kelemen, P. B. Permanent storage of carbon dioxide in geological reservoirs by mineral carbonation Nat. Geosci. 2009, 2, 837-841
15. Li, Z. W.; Dong, M. Z.; Li, S. L.; Huang, S. CO2 sequestration in depleted oil and gas reservoirs-caprock characterization and storage capacity Energy Convers. Manage. 2006, 47, 1372-1382
16. Gaus, I. Role and impact of CO(2)-rock interactions during CO(2) storage in sedimentary rocks Int. J. Greenhouse Gas Control 2010, 4, 73-89
17. Credoz, A.; Bildstein, O.; Jullien, M.; Raynal, J.; Petronin, J. C.; Lillo, M.; Pozo, C.; Geniaut, G. Experimental and modeling study of geochemical reactivity between clayey caprocks and CO(2) in geological storage conditions. In Greenhouse Gas Control Technologies 9; Gale, J.; Herzog, H.; Braitsch, J., Eds.; Elsevier Science Bv: Amsterdam, 2009; pp. 3445-3452.
18. Bildstein, O.; Jullien, M.; Credoz, A.; Garnier, J. Integrated modeling and experimental approach for caprock integrity, risk analysis, and long term safety assessment. In Greenhouse Gas Control Technologies 9 Book Series; Gale, J.; Herzog, H.; Braitsch, J., Eds.; Energy Procedia 2009, 1, 1; pp. 3237-3244 10.1016/j.egypro.2009.02.135.
19. Bildstein, O.; Kervevan, C.; Lagneau, V.; Delaplace, P.; Credoz, A.; Audigane, P.; Perfetti, E.; Jacquemet, N.; Jullien, M. Integrative Modeling of Caprock Integrity in the Context of CO(2) Storage: Evolution of Transport and Geochemical Properties and Impact on Performance and Safety Assessment Oil Gas Sci. Technol.-Revue De L Institut Francais Du Petrole 2010, 65, 485-502
20. Shukla, R.; Ranjith, P.; Haque, A.; Choi, X. A review of studies on CO(2) sequestration and caprock integrity Fuel 2010, 89, 2651-2664
21. Shao, H. B.; Ray, J. R.; Jun, Y. S. Dissolution and Precipitation of Clay Minerals under Geologic CO2 Sequestration Conditions: CO2-Brine-Phlogopite Interactions Environ. Sci. Technol. 2010, 44, 5999-6005
22. Duguid, A.; Radonjic, M.;; Bruant, R.; Mandecki, T.; Scherer, G. W.; Celia, M. A. The effects of CO2 sequestration on oil well cements. In 7th International Conference on Greenhouse Gas Control Technologies, Vancouver, Canada, September 9, 2004.
23. Kutchko, B. G.; Strazisar, B. R.; Huerta, N.; Lowry, G. V.; Dzombak, D. A.; Thaulow, N. CO(2) Reaction with Hydrated Class H Well Cement under Geologic Sequestration Conditions: Effects of Flyash Admixtures Environ. Sci. Technol. 2009, 43, 3947-3952
24. Bigley, C.; Brown, I.; Geoghegan, B.; Brandl, A. A new portland cement derived composite binder for use in geothermnal wells. In Proceedings World Geothermal Congress, Bali, Indonesia, April 25 - 29, 2010.
25. 2-Induced Phlogopite Dissolution and Secondary Mineral Formation Environ. Sci. Technol. 2011, 45, 1737-1743
26. 2 media at low pressure and temperture conditions: an experimental approach Clays Clay Miner. 2009, 57, 616-637
27. Credoz, A.; Bildstein, O.; Jullien, M.; Raynal, J.; Trotignon, L.; Pokrovsky, O. Mixed-layer Illite-smectite reactivity in acidified solutions: Implications for clayey caprock stability in CO(2) geological storage Appl. Clay Sci. 2011, 53, 402-408
28. Sato, T.; Watanabe, T.; Otsuka, R. Effects of layer charge, charge location, and energy change on expansion properties of dioctahedral smectites Clays Clay Miner. 1992, 40, 103-113
29. Ferrage, E.; Lanson, B.; Sakharov, B. A.; Drits, V. A. Investigation of smectite hydration properties by modeling experimental X-ray diffraction patterns: Part I. Montmorillonite hydration properties Am. Mineral. 2005, 90, 1358-1374
30. Schaef, H. T.; Ilton, E. S.; Qafoku, O.; Martin, P. F.; Felmy, A. R.; Rosso, K. M. In situ XRD study of Ca2+ saturated montmorillonite (STX-1) exposed to anhydrous and wet supercritical carbon dioxide Int. J. Greenhouse Gas Control 2012, 6, 220-229
31. 2 sequestration Int. J. Greenhouse Gas Control 2012, 8, 73-81
32. Olphen, H. V.; Fripiat, J. J., Eds. Data Handbook for Clay Materials and Other Non-Metallic Minerals; Pergamon Press: New York, 1979.
33. Jaynes, W. F.; Bigham, J. M. Multiple cation-exchange capacity measurements on standard clays using a commercial mechamical extractor Clays Clay Miner. 1986, 34, 93-98
34. Jaynes, W. F.; Bigham, J. M. Charge reduction, octahedral charge, and lithiumk retention in heated, Li-saturated smectites Clays Clay Miner. 1987, 35, 440-448
35. Schilling, M. R. Effects of sample-size and packing in the thermogravimetric analysis of calcium montmorillonite STX-1 Clays Clay Miner. 1990, 38, 556-558
36. Chipera, S. J.; Bish, D. L. Baseline studies of The Clay Minerals Society Source Clays: Powder X-ray diffraction analyses Clays Clay Miner. 2001, 49, 398-409
37. Madejova, J.; Komadel, P. Baseline studies of The Clay Minerals Society Source Clays: Infrared methods Clays Clay Miner. 2001, 49, 410-432
38. Mermut, A. R.; Lagaly, G. Baseline studies of The Clay Minerals Society Source Clays: Layer-charge determination and characteristics of those minerals containing 2: 1 layers Clays Clay Miner. 2001, 49, 393-397
39. Mermut, A. R.; Cano, A. F. Baseline studies of The Clay Minerals Society Source Clays: Chemical analyses of major elements Clays Clay Miner. 2001, 49, 381-386
40. Kunze, G. W. Pretreatment for mineralogical analysis. In Methods of Soil Analysis, Part I, Physical and Mineralogical Properties, Including Statistics of Measurements and Sampling; American Society of Agronomy: Madison, 1965; pp 568-577.
41. Moore, D. M.; Reynolds, R. C. X-Ray Diffraction and the Identification and Analysis of Clay Minerals; Oxford University Press: New York, 1989.
42. 2: An in situ high pressure X-ray diffraction study. Geochim. Cosmochim. Acta 2011, 75, 7458-7471
43. Ferrage, E.; Lanson, B.; Michot, L. J.; Robert, J. L. Hydration Properties and Interlayer Organization of Water and Ions in Synthetic Na-Smectite with Tetrahedral Layer Charge. Part 1. Results from X-ray Diffraction Profile Modeling J. Phys. Chem. C 2010, 114, 4515-4526
44. Morodome, S.; Kawamura, K. Swelling behavior of Na- and Ca-montmorillonite up to 150 degrees C by in situ x-ray diffraction experiments Clays Clay Miner. 2009, 57, 150-160
45. Yamada, H.; Nakazawa, H.; Hashizume, H.; Shimomura, S.; Watanabe, T. Hydration behaviour of Na-smectite crystals synthesized at high-pressure and high-temperature Clays Clay Miner. 1994, 42, 77-80
46. Spycher, N.; Pruess, K.; Ennis-King, J. CO2-H2O mixtures in the geological sequestration of CO2. I. Assessment and calculation of mutual solubilities from 12 to 100 degrees C and up to 600 bar Geochim. Cosmochim. Acta 2003, 67, 3015-3031
47. Chapoy, A.; Mohammadi, A. H.; Tohidi, B.; Richon, D. Gas solubility measurement and modeling for the nitrogen plus water system from 274.18 to 363.02 K J. Chem. Eng. Data 2004, 49, 1110-1115
48. Ferrage, E.; Lanson, B.; Malikova, N.; Plancon, A.; Sakharov, B. A.; Drits, V. A. New insights on the distribution of interlayer water in bi-hydrated smectite from X-ray diffraction profile modeling of 00l reflections Chem. Mater. 2005, 17, 3499-3512
49. Benrhaiem, H.; Tessier, D.; Pons, C. H. Swelling behavior and structural and textural evolution of montmorillonites during dessication humectation cycle.1. calcium montmorillonites Clay Miner. 1986, 21, 9-29
50. Huang, W. L.; Bassett, W. A.; Wu, T. C. Dehydration and hydration of montmorillonite at elevated temperatures and pressures monitored using synchrotron radiation Am. Mineral. 1994, 79, 683-691
51. de Siqueira, A. V.; Lobban, C.; Skipper, N. T.; Williams, G. D.; Soper, A. K.; Done, R.; Dreyer, J. W.; Humphreys, R. J.; Bones, J. A. R. The structure of pore fluids in swelling clays at elevated pressures and temperatures J. Phys.: Condens. Matter 1999, 11, 9179-9188