메뉴 건너뛰기




Volumn 217, Issue 1-3, 2012, Pages 157-167

Mass, NMR and IR spectroscopic characterization of pentedrone and pentylone and identification of their isocathinone by-products

Author keywords

Isocathinones; Mass spectrometry; NMR; Pentedrone; Pentylone; Product ion mass spectrometry

Indexed keywords

AMINOKETONE; DESIGNER DRUG; ISOCATHINONE; PENTEDRONE; PENTYLONE; UNCLASSIFIED DRUG;

EID: 84858797283     PISSN: 03790738     EISSN: 18726283     Source Type: Journal    
DOI: 10.1016/j.forsciint.2011.10.045     Document Type: Article
Times cited : (44)

References (25)
  • 1
    • 33646174260 scopus 로고    scopus 로고
    • Chromatographic and mass spectral studies on methoxymethcathinones related to 2,3-methylenedioxymethamphetamine
    • Awad T.C.R., Clark C.R., DeRuiter J. Chromatographic and mass spectral studies on methoxymethcathinones related to 2,3-methylenedioxymethamphetamine. J. Chromatogr. Sci. 2006, 44(3):155-161.
    • (2006) J. Chromatogr. Sci. , vol.44 , Issue.3 , pp. 155-161
    • Awad, T.C.R.1    Clark, C.R.2    DeRuiter, J.3
  • 2
    • 34248140784 scopus 로고    scopus 로고
    • Mass spectral and NMR spectral data of two new designer drugs with an α-aminophenone structure: 4'-methyl-α-pyrrolidinohexanophenone and 4'-methyl-α-pyrrolidinobutyrophenone
    • Westphal F., Junge Th., Rösner P., Fritschi G., Klein B., Girreser U. Mass spectral and NMR spectral data of two new designer drugs with an α-aminophenone structure: 4'-methyl-α-pyrrolidinohexanophenone and 4'-methyl-α-pyrrolidinobutyrophenone. Forensic Sci. Int. 2007, 169:32-42.
    • (2007) Forensic Sci. Int. , vol.169 , pp. 32-42
    • Westphal, F.1    Junge, T.2    Rösner, P.3    Fritschi, G.4    Klein, B.5    Girreser, U.6
  • 3
    • 60649105512 scopus 로고    scopus 로고
    • Fluoromethcathione, a new substance of abuse
    • Archer R.P. Fluoromethcathione, a new substance of abuse. Forensic Sci. Int. 2009, 185:1-8.
    • (2009) Forensic Sci. Int. , vol.185 , pp. 1-8
    • Archer, R.P.1
  • 4
    • 57049181322 scopus 로고    scopus 로고
    • Discrimination and identification of regioisomeric β-keto analogues of 3,4-methylenedioxyamphetamines by gas chromatography-mass spectrometry
    • Zaitsu K., Katagi M., Kamata H.T., Miki A., Tsuchihashi H. Discrimination and identification of regioisomeric β-keto analogues of 3,4-methylenedioxyamphetamines by gas chromatography-mass spectrometry. Fusion Technol. 2008, 26:45-51.
    • (2008) Fusion Technol. , vol.26 , pp. 45-51
    • Zaitsu, K.1    Katagi, M.2    Kamata, H.T.3    Miki, A.4    Tsuchihashi, H.5
  • 5
    • 67651023725 scopus 로고    scopus 로고
    • Mass and NMR spectroscopic characterization of 3,4-methylenedioxypyrovalerone: a designer drug with α-pyrrolidionophenone structure
    • Westphal F., Junge Th., Rösner P., Sönnichsen F., Schuster F. Mass and NMR spectroscopic characterization of 3,4-methylenedioxypyrovalerone: a designer drug with α-pyrrolidionophenone structure. Forensic Sci. Int. 2009, 190:1-8.
    • (2009) Forensic Sci. Int. , vol.190 , pp. 1-8
    • Westphal, F.1    Junge, T.2    Rösner, P.3    Sönnichsen, F.4    Schuster, F.5
  • 6
    • 77953869937 scopus 로고    scopus 로고
    • An analysis of the 'legal high' mephedrone
    • Gibbons S., Zloh M. An analysis of the 'legal high' mephedrone. Bioorg. Med. Chem. Lett. 2011, 20:4135-4139.
    • (2011) Bioorg. Med. Chem. Lett. , vol.20 , pp. 4135-4139
    • Gibbons, S.1    Zloh, M.2
  • 7
    • 77956642096 scopus 로고    scopus 로고
    • Analyses of second-generation 'legal highs' in the UK: initial findings
    • Brandt S.D., Sumnall H.R., Measham F., Cole J. Analyses of second-generation 'legal highs' in the UK: initial findings. Drug Test. Anal. 2010, 2:377-382.
    • (2010) Drug Test. Anal. , vol.2 , pp. 377-382
    • Brandt, S.D.1    Sumnall, H.R.2    Measham, F.3    Cole, J.4
  • 8
    • 79959541920 scopus 로고    scopus 로고
    • Massenspektrometrische, infrarotspektroskopische und NMR-spektroskopische Daten von Mephedron Butylon und Methylon sowie einigen ihrer Derivate
    • (article in German)
    • Westphal F., Junge T., Rösner P., Girreser U., Fritsch R. Massenspektrometrische, infrarotspektroskopische und NMR-spektroskopische Daten von Mephedron Butylon und Methylon sowie einigen ihrer Derivate. Toxichem. Krimtech. 2010, 77(2):95-116. (article in German).
    • (2010) Toxichem. Krimtech. , vol.77 , Issue.2 , pp. 95-116
    • Westphal, F.1    Junge, T.2    Rösner, P.3    Girreser, U.4    Fritsch, R.5
  • 9
    • 79957604914 scopus 로고    scopus 로고
    • Spectroscopic characterization of 3,4-methylenedioxypyrrolidinobutyrophenone: a new designer drug with α-pyrrolidionophenone structure
    • Westphal F., Junge T., Klein B., Fritschi G., Girreser U. Spectroscopic characterization of 3,4-methylenedioxypyrrolidinobutyrophenone: a new designer drug with α-pyrrolidionophenone structure. Forensic Sci. Int. 2011, 209:126-132.
    • (2011) Forensic Sci. Int. , vol.209 , pp. 126-132
    • Westphal, F.1    Junge, T.2    Klein, B.3    Fritschi, G.4    Girreser, U.5
  • 10
    • 79959541684 scopus 로고    scopus 로고
    • New " party pill" components in New Zealand: The synthesis and analysis of some β-ketone analogues of 3,4-methylenedioxymethamphetamine (MDMA) including βk-DMBDB (β-ketone-N,N-dimethyl-1-(1,3-benzodioxol-5-yl)-2-butanamine
    • Russell M.J., Bogun B. New " party pill" components in New Zealand: The synthesis and analysis of some β-ketone analogues of 3,4-methylenedioxymethamphetamine (MDMA) including βk-DMBDB (β-ketone-N,N-dimethyl-1-(1,3-benzodioxol-5-yl)-2-butanamine. Forensic Sci. Int. 2011, 210:174-181.
    • (2011) Forensic Sci. Int. , vol.210 , pp. 174-181
    • Russell, M.J.1    Bogun, B.2
  • 11
    • 79959534957 scopus 로고    scopus 로고
    • Identification and characterization of the new designer drug 4'-methylethcathinone (4-MEC) and elaboration of a novel liquid chromatography-tandem mass spectrometry (LC-MS/MS) screening method for seven different methcathinone analogs
    • Jankovics P., Várady A., Tögyesi L., Lohner S., Németh-Palotás J., Köszegi-Szalai H. Identification and characterization of the new designer drug 4'-methylethcathinone (4-MEC) and elaboration of a novel liquid chromatography-tandem mass spectrometry (LC-MS/MS) screening method for seven different methcathinone analogs. Forensic Sci. Int. 2011, 210:213-220.
    • (2011) Forensic Sci. Int. , vol.210 , pp. 213-220
    • Jankovics, P.1    Várady, A.2    Tögyesi, L.3    Lohner, S.4    Németh-Palotás, J.5    Köszegi-Szalai, H.6
  • 12
    • 80053383779 scopus 로고    scopus 로고
    • Analysis of NRG 'legal highs' in the UK: identification and formation of novel cathinones
    • 10.1002/dta.204
    • Brand S.D., Freeman S., Sumnall H.R., Measham F., Cole J. Analysis of NRG 'legal highs' in the UK: identification and formation of novel cathinones. Drug Test. Anal. 2010, 10.1002/dta.204.
    • (2010) Drug Test. Anal.
    • Brand, S.D.1    Freeman, S.2    Sumnall, H.R.3    Measham, F.4    Cole, J.5
  • 14
    • 34248156376 scopus 로고    scopus 로고
    • Structure elucidation of new designer drugs by daughter ion mass spectroscopy
    • F. Pragst, R. Aderjan (Eds.)
    • Rösner P., Junge Th. Structure elucidation of new designer drugs by daughter ion mass spectroscopy. XII. GTFCh-Symposium in Mosbach 2001, 130-142. F. Pragst, R. Aderjan (Eds.).
    • (2001) XII. GTFCh-Symposium in Mosbach , pp. 130-142
    • Rösner, P.1    Junge, T.2
  • 15
    • 0010649635 scopus 로고
    • A round robin on the reproducibility of standard operating conditions for the acquisition of library MS/MS spectra using triple quadrupols
    • Dawson P.H., Sun W.F. A round robin on the reproducibility of standard operating conditions for the acquisition of library MS/MS spectra using triple quadrupols. Int. J. Mass Spectrom. Ion Processes 1984, 55:155-170.
    • (1984) Int. J. Mass Spectrom. Ion Processes , vol.55 , pp. 155-170
    • Dawson, P.H.1    Sun, W.F.2
  • 16
    • 85168041378 scopus 로고    scopus 로고
    • Product ion mass spectra of important organic ions, a free printed version can be ordered from the authors.
    • T. Junge, P. Rösner, F. Westphal, Product ion mass spectra of important organic ions, a free printed version can be ordered from the authors.
    • Junge, T.1    Rösner, P.2    Westphal, F.3
  • 17
    • 67651023725 scopus 로고    scopus 로고
    • Mass and NMR spectroscopic characterization of 3,4-methylenedioxypyrovalerone: a designer drug with α-pyrrolidionophenone structure
    • Westphal F., Junge Th., Rösner P., Sönnichsen F., Schuster F. Mass and NMR spectroscopic characterization of 3,4-methylenedioxypyrovalerone: a designer drug with α-pyrrolidionophenone structure. Forensic Sci. Int. 2009, 190:1-8.
    • (2009) Forensic Sci. Int. , vol.190 , pp. 1-8
    • Westphal, F.1    Junge, T.2    Rösner, P.3    Sönnichsen, F.4    Schuster, F.5
  • 18
    • 0000056907 scopus 로고
    • N-Methyl-1-(3,4-methylenedioxyphenyl)-2-butanamine, a representative of a new class of street drugs
    • Rösner P., Junge Th. N-Methyl-1-(3,4-methylenedioxyphenyl)-2-butanamine, a representative of a new class of street drugs. Microgram 1994, 27(12):411-418.
    • (1994) Microgram , vol.27 , Issue.12 , pp. 411-418
    • Rösner, P.1    Junge, T.2
  • 19
    • 0342409271 scopus 로고    scopus 로고
    • Synthesis of 2,3- and 3,4-methylenedioxyphenylalkylamines and their regioisomeric differentiation by mass spectral analysis using GC-MS-MS
    • Borth S., Hänsel W., Rösner P., Junge Th. Synthesis of 2,3- and 3,4-methylenedioxyphenylalkylamines and their regioisomeric differentiation by mass spectral analysis using GC-MS-MS. Forensic Sci. Int. 2000, 114:139-153.
    • (2000) Forensic Sci. Int. , vol.114 , pp. 139-153
    • Borth, S.1    Hänsel, W.2    Rösner, P.3    Junge, T.4
  • 20
    • 0342264632 scopus 로고    scopus 로고
    • Regioisomeric differentiation of 2,3- and 3,4-methylenedioxy ring-substituted phenylalkylamines by gas chromatography/tandem mass spectrometry
    • Borth S., Hänsel W., Rösner P., Junge Th. Regioisomeric differentiation of 2,3- and 3,4-methylenedioxy ring-substituted phenylalkylamines by gas chromatography/tandem mass spectrometry. J. Mass Spectrom. 2000, 35:705-710.
    • (2000) J. Mass Spectrom. , vol.35 , pp. 705-710
    • Borth, S.1    Hänsel, W.2    Rösner, P.3    Junge, T.4
  • 21
    • 72449136653 scopus 로고    scopus 로고
    • Differentiation of regioisomeric ring-substituted fluorophenethylamines with product ion spectrometry
    • Westphal F., Rösner P., Junge Th. Differentiation of regioisomeric ring-substituted fluorophenethylamines with product ion spectrometry. Forensic Sci. Int. 2010, 194:53-59.
    • (2010) Forensic Sci. Int. , vol.194 , pp. 53-59
    • Westphal, F.1    Rösner, P.2    Junge, T.3
  • 22
    • 85168044544 scopus 로고    scopus 로고
    • Differenzierung regioisomerer N-alkylierter Fluorcathinone durch Tochterionenspektroskopie mittels CI-GC-MS/MS (Differentiation of N-alkylated regioisomeric fluorocathinones with product ion spectrometry using chemical ionization and GC-MS/MS)
    • (article in German)
    • Westphal F., Rösner P., Junge Th. Differenzierung regioisomerer N-alkylierter Fluorcathinone durch Tochterionenspektroskopie mittels CI-GC-MS/MS (Differentiation of N-alkylated regioisomeric fluorocathinones with product ion spectrometry using chemical ionization and GC-MS/MS). Toxichem. Krimtech. 2003, 70(2):82-86. (article in German).
    • (2003) Toxichem. Krimtech. , vol.70 , Issue.2 , pp. 82-86
    • Westphal, F.1    Rösner, P.2    Junge, T.3
  • 23
    • 85168038493 scopus 로고    scopus 로고
    • Figures of 13C NMR, TOCSY-experiment, DEPT-, HMBC- and HSQC-NMR experiments are provided in PDF-format in the supplemental data published alongside the electronic version of this article.
    • Figures of 13C NMR, TOCSY-experiment, DEPT-, HMBC- and HSQC-NMR experiments are provided in PDF-format in the supplemental data published alongside the electronic version of this article.
  • 24
    • 33847121295 scopus 로고    scopus 로고
    • A detailed mechanistic fragmentation analysis of methamphetamine and select regioisomers by GC/MS
    • Sachs S.B., Woo F. A detailed mechanistic fragmentation analysis of methamphetamine and select regioisomers by GC/MS. J. Forensic Sci. 2007, 52(2):308-319.
    • (2007) J. Forensic Sci. , vol.52 , Issue.2 , pp. 308-319
    • Sachs, S.B.1    Woo, F.2
  • 25
    • 84989030552 scopus 로고
    • A 13C T1 study of conformational and molecular mobility of mono- and difucosyllactoses
    • Eichart A., Dabrowski J. A 13C T1 study of conformational and molecular mobility of mono- and difucosyllactoses. Magn. Reson. Chem. 1992, 30:115-124.
    • (1992) Magn. Reson. Chem. , vol.30 , pp. 115-124
    • Eichart, A.1    Dabrowski, J.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.