Determination of venlafaxine in post-mortem whole blood by HS-SPME and GC-NPD

Forensic Science International

Volumn 215, Issue 1-3, 2012, Pages 105-109

  Mastrogianni, O ^a   Theodoridis, G ^a   Spagou, K ^a   Violante, D ^a   Henriques, T ^a   Pouliopoulos, A ^a   Psaroulis, K ^a   Tsoukali, H ^a   Raikos, N ^a  

^a ARISTOTLE UNIVERSITY OF THESSALONIKI   (Greece)

Author keywords

GC NPD; HS SPME; Post mortem blood; Venlafaxine

Indexed keywords

DIMETICONE; MIRTAZAPINE; VENLAFAXINE;

ADULT; ANALYTIC METHOD; AQUEOUS SOLUTION; ARTICLE; AUTOPSY; BLOOD ANALYSIS; CASE REPORT; CAUSE OF DEATH; DRUG BLOOD LEVEL; DRUG DETERMINATION; DRUG INTOXICATION; DRUG OVERDOSE; ESOPHAGUS; FEMALE; FORENSIC TOXICOLOGY; GAS CHROMATOGRAPHY; GREECE; HEADSPACE SOLID PHASE MICROEXTRACTION; HUMAN; HUMAN TISSUE; LIMIT OF DETECTION; LIMIT OF QUANTITATION; NITROGEN PHOSPHORUS DETECTION; PRIORITY JOURNAL; PROCESS OPTIMIZATION; SOLID PHASE MICROEXTRACTION; STOMACH; TEMPERATURE; THIN LAYER CHROMATOGRAPHY;

EID: 84856459653     PISSN: 03790738     EISSN: 18726283     Source Type: Journal    
DOI: 10.1016/j.forsciint.2011.05.008     Document Type: Article

References (29)

1. Tournel G., Houdret N., Hédouin V., Deveaux M., Gosset D., Lhermitte M. High-performance liquid chromatographic method to screen and quantitate seven selective serotonin reuptake inhibitors in human serum. J. Chromatogr. B 2001, 761:147-158.
2. Baselt R.C., Cravey R.H. Disposition of Toxic Drugs and Chemicals in Man 1995, Chemical Toxicology Institute, Foster City, CA, 772 pp. 4th ed.
3. Bosse G.M., Spiller H.A., Collins A.M. A fatal case of venlafaxine overdose. J. Med. Toxicol. 2008, 4:18-20.
4. White C.M., Gailey R.A., Levin G.M., Smith T. Seizure resulting from a venlafaxine overdose. Ann. Pharmacother. 1997, 31(2):178-180.
5. Buckley N.A., McManus P.R. Fatal toxicity of serotoninergic and other antidepressant drugs: analysis of United Kingdom mortality data. BMJ 2002, 325(7376):1332-1333.
6. Smith E.G. Association between antidepressant half-life and the risk of suicidal ideation or behaviour among children and adolescents: confirmatory analysis and research implications. J. Affect. Disord. 2009, 114(1-3):143-148.
7. Goeringer K.E., McIntyre I.M., Drummer O.H. Postmortem tissue concentrations of venlafaxine. Forensic Sci. Int. 2001, 121(1-2):70-75.
8. Arthur C.L., Pawliszyn J. Solid phase microextraction with thermal desorption using fused silica optical fibers. Anal. Chem. 1990, 6(2):2145-2148.
9. Zhang Z.Y., Pawliszyn J. Headspace solid phase microextraction. Anal. Chem. 1993, 6(5):1843-1852.
10. Lord H., Pawliszyn J. Microextraction of drugs. J. Chromatogr. A 2000, 902:17-63.
11. Lord H., Pawliszyn J. Evolution of solid phase microextraction technology. J. Chromatogr. A 2000, 885:153-193.
12. Theodoridis G., Koster E.H.M., de-Jong G.J. Solid phase microextraction in the analysis of biological samples. J. Chromatogr. B 2000, 745:49-82.
13. Snow N.H. Solid phase microextraction of drugs from biological matrices. J. Chromatogr. A 2000, 885:445-455.
14. Handley J., Harris C.M. Great ideas of a decade. Anal. Chem. 2001, 7(3):660A-666A.
15. Tsoukali H., Raikos N., Theodoridis G., Psaroulis D. Headspace solid phase microextraction for the gas chromatographic analysis of methyl-parathion in post-mortem human samples, application in a suicide case by intravenous injection. Forensic Sci. Int. 2004, 143:127-132.
16. Lamas J.P., Salgado-Petinal C., Garcia-Jares C., Llompart M., Cela R., Gomez M. Solid-phase microextraction-gas chromatography-mass spectrometry for the analysis of selective serotonin reuptake inhibitors in environmental water. J. Chromatogr. A 2004, 1046:241-247.
17. Salgado-Petinal C., Lamas J.P., Garcia-Jares C., Llompart M., Cela R. Rapid screening of selective serotonin re-uptake inhibitors in urine samples using solid-phase microextraction gas chromatography-mass spectrometry. Anal. Bioanal. Chem. 2005, 382:1351-1359.
18. Pragst F. Application of solid-phase microextraction in analytical toxicology. Anal. Bioanal. Chem. 2007, 388(7):1393-1414.
19. Unceta N., Gomez-Caballero A., Sanchez A., Millan S., Sampedro M.C., Aranzazu Goicolea M., Salles J., Barrio R.J. Simultaneous determination of citalopram, fluoxetine and their main metabolites in human urine samples by solid-phase microextraction coupled with high-performance liquid chromatography. J. Pharm. Biomed. Anal. 2008, 46:763-770.
20. Sporkert F., Pragst F. Proceedings of TIAFT 2000 2001, 429-439. I. Rasanan (Ed.).
21. Pawliszyn J. Sampling and Sample Preparation in Field and Laboratory, 37 2002, University of Waterloo, Canada, Hardbound.
22. Raikos N., Christopoulou K., Theodoridis G., Tsoukali H., Psaroulis D. Determination of amphetamines in human urine by headspace solid-phase microextraction and gas chromatography. J. Chromatogr. B: Analyt. Technol. Biomed. Life Sci. 2003, 78(9):59-63.
23. J. Pawliszyn, Applications of Solid-Phase microextraction, Series Editor Roger M. Smith, RSC Chromatography Monographs, 1999, 470-471.
24. Wangkarn S., Wutiadirek W. Selective fiber used for headspace solid-phase microextraction of abused drugs in human urine. Mj. Int. J. Sci.Tech. 2007, 01(2):145-156.
25. Chai M., Tan G., Lal A. Optimization of headspace solid-phase microextraction for the determination of pesticide residues in vegetables and fruits. Anal. Sci. 2008, 2(4):273-276.
26. Tsoukali H., Theodoridis G., Raikos N., Grigoratou I. Solid phase microextraction gas chromatographic analysis of organophosphorus pesticides in biological samples. J. Chromatogr. B 2005, 822:194-200.
27. Musshoff F., Padosch S., Steinborn S., Madea B. Fatal blood and tissue concentrations of more than 200 drugs. Forensic Sci. Int. 2004, 142:161-210.
28. Jaffe P.D., Batziris H.P., van der Hoeven P., DeSilva D., McIntyre I.M. A study involving venlafaxine overdoses: comparison of fatal and therapeutic concentrations in post-mortem specimens. J. Forensic Sci. 1999, 44:193-196.
29. S.E. Denieul, H.M. Okely, A.J. Bentley, Venlafaxine (EFEXOR®) Acute Poisoning, Case Notes Archive from TIAFT Bulletin. 27 (3) 1997 6-7.