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Volumn 72, Issue , 2012, Pages 10-19

A new view on the metastable zone width during cooling crystallization

Author keywords

Batch crystallization; Metastable zone width; Particulate processes; Pharmaceuticals; Single nucleus mechanism; Stochastic modeling

Indexed keywords

BATCH CRYSTALLIZATION; CONSTANT COOLING RATE; COOLING CRYSTALLIZATION; CRYSTAL NUCLEATION; CRYSTALLIZATION PROCESS; METASTABLE ZONE WIDTH; MODEL SYSTEM; NUCLEATION RATE; OPERATING WINDOWS; PARTICULATE PROCESS; POPULATION BALANCE MODELS; POPULATION BALANCES; PRIMARY NUCLEATION; PROCESS WINDOW; PRODUCT QUALITY; SATURATION TEMPERATURE; STOCHASTIC MODELING; VOLUME DEPENDENCY;

EID: 84856153403     PISSN: 00092509     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ces.2012.01.002     Document Type: Article
Times cited : (123)

References (27)
  • 1
    • 0025251455 scopus 로고
    • Secondary nucleation kinetcs of ammonium sulfate in a CMSMPR crystallizer
    • Daudey P.J., van Rosmalen G.M., de Jong E.J. Secondary nucleation kinetcs of ammonium sulfate in a CMSMPR crystallizer. J. Cryst. Growth 1990, 99:1076-1081.
    • (1990) J. Cryst. Growth , vol.99 , pp. 1076-1081
    • Daudey, P.J.1    van Rosmalen, G.M.2    de Jong, E.J.3
  • 2
    • 66149084331 scopus 로고    scopus 로고
    • Nucleation of crystals from solution: classical and two-step models
    • Erdemir D., Lee A.Y., Myerson A.S. Nucleation of crystals from solution: classical and two-step models. Acc. Chem. Res. 2009, 42:621-629.
    • (2009) Acc. Chem. Res. , vol.42 , pp. 621-629
    • Erdemir, D.1    Lee, A.Y.2    Myerson, A.S.3
  • 3
    • 0033133650 scopus 로고    scopus 로고
    • Brittle fracture in crystallization processes Part B. Growth of fragments and scale-up of suspension crystallizers
    • Gahn C., Mersmann A. Brittle fracture in crystallization processes Part B. Growth of fragments and scale-up of suspension crystallizers. Chem. Eng. Sci. 1999, 54:1283-1292.
    • (1999) Chem. Eng. Sci. , vol.54 , pp. 1283-1292
    • Gahn, C.1    Mersmann, A.2
  • 5
    • 26944503495 scopus 로고    scopus 로고
    • Crystal growth rates of paracetamol in mixtures of water+acetone+toluene
    • Granberg R.A., Rasmuson Å.C. Crystal growth rates of paracetamol in mixtures of water+acetone+toluene. AlChE J. 2005, 51:2441-2456.
    • (2005) AlChE J. , vol.51 , pp. 2441-2456
    • Granberg, R.A.1    Rasmuson, Å.C.2
  • 6
    • 50549203562 scopus 로고
    • Some problems in particle technology: a statistical mechanical formulation
    • Hulburt H.M., Katz S. Some problems in particle technology: a statistical mechanical formulation. Chem. Eng. Sci. 1964, 19:555-574.
    • (1964) Chem. Eng. Sci. , vol.19 , pp. 555-574
    • Hulburt, H.M.1    Katz, S.2
  • 7
    • 78651110533 scopus 로고    scopus 로고
    • Crystal nucleation rates from probability distributions of induction times
    • Jiang S., ter Horst J.H. Crystal nucleation rates from probability distributions of induction times. Cryst. Growth Des. 2011, 11:256-261.
    • (2011) Cryst. Growth Des. , vol.11 , pp. 256-261
    • Jiang, S.1    ter Horst, J.H.2
  • 8
    • 79953859647 scopus 로고    scopus 로고
    • Combination of a single primary nucleation event and secondary nucleation in crystallization processes
    • Kadam S.S., Kramer H.J.M., ter Horst J.H. Combination of a single primary nucleation event and secondary nucleation in crystallization processes. Cryst. Growth Des. 2011, 11:1271-1277.
    • (2011) Cryst. Growth Des. , vol.11 , pp. 1271-1277
    • Kadam, S.S.1    Kramer, H.J.M.2    ter Horst, J.H.3
  • 9
    • 79956364033 scopus 로고    scopus 로고
    • Rapid online calibration for ATR-FTIR spectroscopy during batch crystallization of ammonium sulphate in a semi-industrial scale crystallizer
    • Kadam S.S., Mesbah A., van der Windt E., Kramer H.J.M. Rapid online calibration for ATR-FTIR spectroscopy during batch crystallization of ammonium sulphate in a semi-industrial scale crystallizer. Chem. Eng. Res. Des. 2011, 89:995-1005.
    • (2011) Chem. Eng. Res. Des. , vol.89 , pp. 995-1005
    • Kadam, S.S.1    Mesbah, A.2    van der Windt, E.3    Kramer, H.J.M.4
  • 12
    • 0000881952 scopus 로고
    • Chiral symmetry breaking in sodium chlorate crystallizaton
    • Kondepudi D.K., Kaufman R.J., Singh N. Chiral symmetry breaking in sodium chlorate crystallizaton. Science 1990, 250:975-976.
    • (1990) Science , vol.250 , pp. 975-976
    • Kondepudi, D.K.1    Kaufman, R.J.2    Singh, N.3
  • 14
    • 37849043845 scopus 로고    scopus 로고
    • A new interpretation of metastable zone widths measured for unseeded solutions
    • Kubota N. A new interpretation of metastable zone widths measured for unseeded solutions. J. Cryst. Growth 2008, 310:629-634.
    • (2008) J. Cryst. Growth , vol.310 , pp. 629-634
    • Kubota, N.1
  • 15
    • 84857232202 scopus 로고    scopus 로고
    • Validation of the single nucleus mechanism by polymorphism. In: Kadam, S.S., Kulkarni, S. A., ter Horst, J.H. (Eds.), 18th International Workshop on Industrial Crystallization, Delft, The Netherlands
    • Kulkarni, S.A., Kadam S.S., Stankiewicz, A.I., Meekes, H., ter Horst, J.H., 2011. Validation of the single nucleus mechanism by polymorphism. In: Kadam, S.S., Kulkarni, S. A., ter Horst, J.H. (Eds.), 18th International Workshop on Industrial Crystallization, Delft, The Netherlands, pp. 75-80.
    • (2011) , pp. 75-80
    • Kulkarni, S.A.1    Kadam, S.S.2    Stankiewicz, A.I.3    Meekes, H.4    Ter Horst, J.H.5
  • 16
    • 0031677648 scopus 로고    scopus 로고
    • How to predict the metastable zone width
    • Mersmann A., Bartosch K. How to predict the metastable zone width. J. Cryst. Growth 1998, 183:240-250.
    • (1998) J. Cryst. Growth , vol.183 , pp. 240-250
    • Mersmann, A.1    Bartosch, K.2
  • 18
    • 0004294969 scopus 로고    scopus 로고
    • Butterworth-Heinemann, Oxford
    • Mullin J.W. Crystallization 2001, Butterworth-Heinemann, Oxford. 4th edn.
    • (2001) Crystallization
    • Mullin, J.W.1
  • 20
    • 40449122877 scopus 로고    scopus 로고
    • Determination of the kinetic parameters for the crystallization of paracetamol from water using metastable zone width experiments
    • Nagy Z.K., Fujiwara M., Woo X.Y., Braatz R.D. Determination of the kinetic parameters for the crystallization of paracetamol from water using metastable zone width experiments. Ind. Eng. Chem. Res. 2008, 47:1245-1252.
    • (2008) Ind. Eng. Chem. Res. , vol.47 , pp. 1245-1252
    • Nagy, Z.K.1    Fujiwara, M.2    Woo, X.Y.3    Braatz, R.D.4
  • 21
    • 0000251107 scopus 로고
    • Homogeneous nucleation in barium sulfate precipitation
    • Nielsen A.E. Homogeneous nucleation in barium sulfate precipitation. Acta Chem. Scand. 1961, 15:441-442.
    • (1961) Acta Chem. Scand. , vol.15 , pp. 441-442
    • Nielsen, A.E.1
  • 22
    • 0001708068 scopus 로고
    • Kinetics of nucleation in solutions
    • Nyvlt J. Kinetics of nucleation in solutions. J. Cryst. Growth 1968, 3-4:377-383.
    • (1968) J. Cryst. Growth , pp. 377-383
    • Nyvlt, J.1
  • 23
    • 33645692757 scopus 로고    scopus 로고
    • Determination of the solid liquid interfacial energy and thereby the critical nucleus size of paracetamol in different solvents
    • Omar W., Mohnicke M., Ulrich J. Determination of the solid liquid interfacial energy and thereby the critical nucleus size of paracetamol in different solvents. Cryst. Res. Technol. 2006, 41:337-343.
    • (2006) Cryst. Res. Technol. , vol.41 , pp. 337-343
    • Omar, W.1    Mohnicke, M.2    Ulrich, J.3
  • 25
    • 61549106307 scopus 로고    scopus 로고
    • Co-crystal polymorphs from a solvent-mediated transformation
    • ter Horst J.H., Cains P.W. Co-crystal polymorphs from a solvent-mediated transformation. Cryst. Growth Des. 2008, 8:2537-2542.
    • (2008) Cryst. Growth Des. , vol.8 , pp. 2537-2542
    • ter Horst, J.H.1    Cains, P.W.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.