Phosgenation reactions with phosgene from triphosgene

Chimica Oggi

Volumn 29, Issue 6, 2011, Pages 40-46

  Eckert, Heiner ^a  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

Author keywords

BTC; Cartridge Phosgenation; Phosgenation; Phosgene; Phosgene Generator; Solid Phosgene; Triphosgene

Indexed keywords

EID: 84856152821     PISSN: 0392839X     EISSN: 19738250     Source Type: Journal    
DOI: None     Document Type: Review

References (30)

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27. Sigma Aldrich, Starter Kit (1 Cartridge for Safe Phosgenation 0.02 mol, 1 gastight adapter with hose, 1 dosimeter badge + paper, instructions) 519782; Replacement Cartridges 0.02 mol 519758 and 0.05 mol 519766.
28. The cartridge and hose are fully filled with ethanol, which can be disposed of as chlorinated organic waste solvent 10 min later. The cartridge can be disposed of as solid waste. The phosgene resistant adapter and tubing can be often reused.
29. Buss Chem Tech AG, Hohenrainstr. 12a, CH-4133 Pratteln, Switzerland, info@buss-ct.com.
30. The cooling unit was not efficient enough to hold the temperature at the rated value.