Drying effect on cement paste porosity at early age observed by NMR methods

Construction and Building Materials

Volumn 29, Issue , 2012, Pages 496-503

  Faure, Paméla F ^a   Caré, Sabine ^a   Magat, Julie ^a   Chaussadent, Thierry ^b  

^a UNIVERSITÉ PARIS EST   (France)

^b UNIVERSITÉ PARIS EST   (France)

Author keywords

A. Drying; A. Hydration; B. Microstructure; B. Nuclear Magnetic Resonance (NMR)

Indexed keywords

ADSORPTION MEASUREMENT; B. NUCLEAR MAGNETIC RESONANCE (NMR); CEMENT PASTE; CEMENTITIOUS MATERIALS; DRYING EFFECTS; DRYING MECHANISM; EARLY AGE; HYDRATION OF CEMENTS; HYDRATION PROCESS; MERCURY INTRUSION POROSIMETRY; OVEN DRYING; WATER-TO-CEMENT RATIOS;

CEMENTS; DRYING; GAS ADSORPTION; HYDRATION; MAGNETIC RESONANCE IMAGING; MERCURY (METAL); MICROSTRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PORE SIZE; RESONANCE;

NUCLEAR MAGNETIC RESONANCE;

EID: 84855915886     PISSN: 09500618     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.conbuildmat.2011.07.012     Document Type: Article

References (37)

1. Bentz DP, Snyder KA, Stutzman PE. Hydration of Portland cement: effect of curing conditions. In: Justnes H editor. Proceedings of the 10th international congress on the chemistry of cement, Vol. 2, Gothenberg, Sweden; 1997.
2. S. Caré Aggregate influence on chloride ion diffusion into mortar Cem Concr Res 33 2003 1021 1028
3. S. Caré, and E. Hervé Application of n-phase model to the diffusion coefficient of chloride in mortar Transport in Porous Media 2 2004 119 135 (Pubitemid 38536571)
4. E. Hervé, S. Caré, and J.S. Seguin Influence of the porosity gradient in cement paste matrix on the mechanical behaviour of mortar Cem Concr Res 40 2010 1060 1071 10.1016/j.cemconres.2010.02.01
5. H.M. Jennings Design of high strength cement-based materials, Part II: Microstructure Mater Sci Technol 4 1988 285 290 (Pubitemid 18649462)
6. H.M. Jennings, J.J. Thomas, J.S. Gevrenov, G. Constantinides, and F.-J. Ulm A multi-technique investigation of the nanoporosity of cement paste Cem Concr Res 37 3 2007 329 336 (Pubitemid 46275622)
7. S. Caré Effect of temperature on porosity and chloride diffusion in cement pastes Construct Build Mater 22 2008 1560 1573 10.1016/j.conbuildmat. 2007.03.01 (Pubitemid 351635867)
8. M.C. Garci Juenger, and H.M. Jennings The use of nitrogen adsorption to assess the microstructure of cement paste Cem Concr Res 31 2001 883 892 (Pubitemid 32544490)
9. C. Gallé Effect of drying on cement-based materials pore structure as identified by mercury intrusion porosimetry: a comparative study between oven-, vacuum-, and freeze-drying Cem Concr Res 31 2001 1467 1477 (Pubitemid 32935080)
10. P. Faure, S. Caré, C. Po, and S. Rodts An MRI-SPI and NMR relaxation study of drying-hydration coupling effect on microstructure of cement-based materials at early age Magn Reson Imaging 23 2005 311 314
11. 1 de l'effet du couplage hydratation-séchage sur la microstructure de pâte de ciment Comptes Rendus Chimie, CRAS 9 2006 548 555 (Pubitemid 43292915)
12. Song Yi-Qiao Novel NMR techniques for porous media research Cem Concr Res 37 2007 325 328
13. R. Viola, A. Tucci, G. Timellini, and P. Fantazzini NMR techniques: a non destructive analysis to follow microstructural changes induced in ceramics J European Ceram Soc 26 2006 3343 3349 (Pubitemid 44210479)
14. S. Emid, and J.H.N. Creyghton High resolution NMR imaging in solids Physica B 81 1985 128
15. 1 Enhancement (SPRITE) J Mag Res A 123 1996 131
16. P.J. Prado, B.J. Balcom, S.D. Beyea, R.L. Armstrong, and T.W. Bremner Concrete thawing studied by single-point ramped imaging Solid State NMR 10 1997 1 8 (Pubitemid 127452877)
17. S.D. Beya, B.J. Balcom, T.W. Bremner, P.J. Prado, D.P. Green, and R.L. Armstrong Magnetic Resonance Imaging and moisture content profiles of drying concrete Cem Conc Res 28 1998 453
18. P.F.de.J. Cano-Barrita, B.J. Balcom, T.W. Bremner, M.B. MacMillan, and W.S. Langley Moisture distribution in drying ordinary and high performance concrete cured in a simulated hot dry climate Mater Struct 37 2004 522
19. G.C. Borgia, R.J.S. Brown, and P. Fantazzini Uniform-penalty inversion of multiexponential decay data J Magn Reson 132 1998 65 77 (Pubitemid 128450587)
20. G.C. Borgia, R.J.S. Brown, and P. Fantazzini Uniform-penalty inversion of multiexponential decay data II J Magn Reson 147 2000 273 285
21. S. Philippot, J.P. Korb, D. Petit, and H. Zanni Analysis of microporosity and setting of reactive powder concrete by proton nuclear relaxation Magn Reson Imaging 16 1998 515 519 (Pubitemid 28506311)
22. T. Apih, G. Lahajnar, A. Sepe, R. Blinc, F. Milia, and R. Cvelbar Proton spin-lattice relaxation study of the hydration of self-stressed expansive cement Cem Concr Res 31 2001 263 269 (Pubitemid 33763349)
23. J.-P. Gorce, and N.B. Milestone Probing the microstructure and water phases in composite cement blends Cem Concr Res 37 2007 310 318 (Pubitemid 46275629)
24. N. Nestle, P. Galvosas, and O. Geier Nuclear magnetic resonance study of diffusion and relaxation in hydrating white cement pastes of different water content J Appl Phys 89 12 2001 8061 8065 (Pubitemid 33662875)
25. R. Blinc, M. Burgar, G. Lahajnar, M. Rozmarin, V. Rutar, and I. Kocuvan NMR relaxation study of adsorbed water in cement and C3S pastes A. Cer. S. 61 1978 35 37 (Pubitemid 8578246)
26. J.-Y. Jehng, D.T. Sprague, and W.P. Halperin Pore structure of hydrating cement paste by magnetic resonance relaxation analysis and freezing Magn Reson Imaging 14 1996 785
27. L. Pel, K. Hazrati, K. Kopinga, and J. Marchand Water absorption in mortar determined by NMR Magn Reson Imaging 16 1998 525 528 (Pubitemid 28506313)
28. R.M.E. Valckenborg, L. Pel, K. Hazrati, K. Kopinga, and J. Marchand Pore water distribution in mortar during drying as determined by NMR Mater Struct 34 2001 599 604 (Pubitemid 33701169)
29. A.J. Bohris, U. Goerke, P.J. McDonald, M. Mulheron, B. Newling, and B. Le Page A broad line NMR and MRI study of water and water transport in portland cement pastes Magn Reson Imaging 16 1998 455 461 (Pubitemid 28506301)
30. S.D. Beya, B.J. Balcom, T.W. Bremner, R.L. Armstrong, and P.E. Gratten-Bellew Detection of drying-induced microcracking in cementitious materials with space-resolved 1H nuclear magnetic resonance relaxometry J Am Ceram Soc 86 5 2003 800 805
31. J.J. Young, P. Szomolanyi, T.W. Bremner, and B.J. Balcom Magnetic resonance imaging of crack formation in hydrated cement paste materials Cem Concr Res 34 2004 1459 1466
32. P.F. Faure, and S. Rodts Proton NMR relaxation as a probe for setting cement pastes Magn Reson Imaging 26 2008 1183 1196
33. K.P. Whitall, and A.L. MacKay Quantitative interpretation of NMR relaxation data J Magn Res 84 1989 134 152
34. M.C.R. Farage, J. Sercombe, and C. Gallé Rehydratation and microstructure of cement paste after heating at temperatures up to 300 °C Cem Concr Res 33 2003 1047 1056
35. D.P. Bentz, and E.J. Garbocz Percolation of phases in a three-dimensional cement paste microstructure model Cem Concr Res 21 1991 325 344
36. P.J. McDonald, J.-P. Korb, J. Mitchell, and L. Monteilhet Surface relaxation and chemical exchange in hydrating cement pastes: a two dimensional NMR relaxation study Phys Rev E 72 2005 011409
37. F.A.L. Dullien Porous Media, Fluid Transport and Pore Structure 1979 Academic Press New York 396 p