Stereoselective HPLC determination of thyroxine enantiomers in pharmaceuticals

Journal of Liquid Chromatography and Related Technologies

Volumn 34, Issue 19, 2011, Pages 2304-2314

  Gondová, Tat'ána ^a   Petrovaj, Ján ^a   Suchá, Mária ^a   Armstrong, Daniel W ^b  

^a P J AFÁRIK UNIVERSITY   (Slovakia)

^b UNIVERSITY OF TEXAS AT ARLINGTON   (United States)

Author keywords

Enantioseparation; LC; Pharmaceutical formulation; Teicoplanin; Thyroxine; Validation

Indexed keywords

ENANTIOSEPARATIONS; LC; PHARMACEUTICAL FORMULATION; TEICOPLANIN; THYROXINE; VALIDATION;

CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; ENANTIOMERS; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; METHANOL; PH EFFECTS;

CHIRALITY;

GALLAMINE TRIETHIODIDE; METHANOL; TEICOPLANIN; THYROXINE;

ACCURACY; ARTICLE; CALIBRATION; CHEMICAL INTERACTION; CHEMICAL STRUCTURE; CHIRALITY; DRUG FORMULATION; DRUG STABILITY; ENANTIOMER; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHOBICITY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; NONHUMAN; PH; SEPARATION TECHNIQUE; STEREOCHEMISTRY; TEMPERATURE;

EID: 84855890986     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826076.2011.587225     Document Type: Article

References (19)

1. Powell, J. R.; Ambre, J. J.; Ruo, T. I. Drug Stereochemistry, Analytical Methods and Pharmacology; Marcel Dekker: New York, 1988; 254.
2. Schwandt, P.; Weisweiler, P. The Effect of D-Thyroxine on Lipoprotein Lipids and Apolipoproteins in Primary Type IIa Hyperlipoproteinemia. Atherosclerosis 1980, 35(3), 301-306. (Pubitemid 10174128)
3. Gika, H.; Lammerhofer, M.; Papadoyannis, I.; Lindner, W. Direct Separation and Quantitative Analysis of Thyroxine and Triiodothyronine Enantiomers in Pharmaceuticals by High-Performance Liquid Chromatography. J. Chromatogr. B 2004, 800(1-2), 193-201. (Pubitemid 38041025)
4. Abou-Basha, L. I.; Aboul-Enein, H. Y. Enantiomeric Separation and Optical Purity Determination of Thyroxine Enantiomers in Bulk and Pharmaceutical Formulations. Pharm. Acta Helv. 1995, 70(3), 237-240.
5. Sardella, R.; Lämmerhofer, M.; Natalini, B.; Lindner, W. J. In-Line Coupling of a Reversed-Phase Column to Cope with Limited Chemoselectivity of a Quinine Carbamate-Based Anion-Exchange Type Chiral Stationary Phase. J. Sep. Sci. 2008, 31(10), 1702-1711. (Pubitemid 351911733)
6. Koidl, J.; Hödl, H.; Schmid, M. G.; Neubauer, B.; Konrad, M.; Petschauer, S.; Gübitz, G. Enantiorecognition of Triiodothyronine and Thyroxine Enantiomers using Different Chiral Selectors by HPLC and Micro-HPLC. J. Biochem. Biophys. Methods 2008, 70(6), 1254-1260.
7. Jin, J. Y.; Baek, C. S.; Lee, W. Development of a Validated HPLC Method for the Simultaneous Determination of D-and L-Thyroxine in Human Plasma. Bull. Korean Chem. Soc. 2007, 28(6), 1070-1072. (Pubitemid 46983380)
8. Jeon, S. H.; Kim, M.; Han, H. K.; Lee, W. Direct Enantiomer Separation of Thyroxine in Pharmaceuticals Using Crown Ether Type Chiral Stationary Phase. Arch. Pharm. Res. 2010, 33(9), 1419-1423.
9. Wang, R.; Jia, Z. P.; Chen, L. R.; Ge, X.; Ma, J.; Zhang, Q.; Xie, H.; Ao, Y; Wang, J. Separation of the Enantiomers of Thyroxine by HPLC with Chiral Mobile Phases. Chromatographia 2004, 59(11-12), 749-752. (Pubitemid 38888023)
10. Hay, I. D.; Annesley, T M.; Jiang, N. S., Gorman, C. A. Simultaneous Determination of D-and L-Thyroxine in Human Serum by Liquid Chromatography with Electrochemical Detection. J. Chromatogr. B 1981, 226(2), 383-390. (Pubitemid 12132007)
11. Lankmayr, E. P.; Budna, K. W.; Nachtmann, F. Separation of Enantiomeric Iodinated Thyronines by Liquid Chromatography of Diastereomers. J. Chromatogr. A 1980, 198(4), 471-479. (Pubitemid 11218982)
12. Jin, D. R.; Zhang, M. N.; Jin, S. J.; Lee, M. K; Song, G. C; Back, G.; Lee, Y I. Enantioselective Resolution of Thyroxine Hormone by High-Performance Liquid Chromatography Utilizing a Highly Fluorescent Chiral Tagging Reagent. Chirality 2007, 19(8), 625-631. (Pubitemid 47075990)
13. Takahashi, M.; Nagashima, M.; Shigeoka, S.; Kamimura, H.; Kamata, K. Determination of Thyroid Hormones in Pharmaceutical Preparations, after Derivatization with 9-Anthroylnitrile, by High-Performance Liquid Chromatography with Fluorescence Detection. J. Chromatogr. A 2002, 958(1-2), 299-303. (Pubitemid 34556958)
14. Gübitz, G.; Juffmann, F. Resolution of the Enantiomers of Thyroid-Hormones by High-Performance Ligand-Exchange Chromatography Using a Chemically Bonded Chiral Stationary Phase. J. Chromatogr. 1987, 404(2), 391-393. (Pubitemid 17125993)
15. Ekborg-Ott, K. H.; Kulman, J. P.; Wang, X. D.; Gahm, K.; He, L. F.; Armstrong, D. W. Evaluation of the Macrocyclic Antibiotic Avoparcin as a New Chiral Selector for HPLC. Chirality 1998, 10(7), 627-660. (Pubitemid 28440730)
16. Kang, J. Z.; Kutscher, D.; Montes-Bayon, M.; Blanco-Gonzales, E.; Sans-Medel, A. Enantioselective Determination of Thyroxine Enantiomers by Ligand-Exchange CE with UVAbsorbance and ICP-MS Detection. Electrophoresis 2009, 30(10), 1774-1782.
17. ICH Harmonised Tripartite Guideline. Validation of Analytical Procedures: Text and Methodology Q2 (R1) Geneva, 2005.
18. Suchá, M. Diploma work; P. J. Šafárik University, Košice, Slovak Republic, 2003.
19. Armstrong, D. W.; Liu, Y. B.; Ekborg Ott, K. H. Covalently Bonded Teicoplanin Chiral Stationary Phase for HPLC Enantioseparation. Chirality 1995, 7(6), 474-497.