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w = 0.1090 for reflections with I > 2σ(I). The crystal structure (1) was solved by direct methods using SHELX-97 (Sheldrich, G. M. University of Gottingen: Gottingen, Germany, 1990,) and expanded using difference Fourier techniques, refined by SHELX-97 (Sheldrich, G. M. 1997). Crystallographic data for the structure of 1 have been deposited in the Cambridge Crystallographic Data Centre (deposition number: CCDC851279). Copies of these data can be obtained free of charge via the Internet at www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB21EZ, UK; fax (+44) 1223-336-033; or deposit@ccdc.cam.ac.uk).
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