Development of a liquid chromatography-tandem mass spectrometry method for the identification of natural androgen steroids and their conjugates in urine samples

Analytica Chimica Acta

Volumn 526, Issue 2, 2004, Pages 113-120

  Buiarelli, F ^a   Coccioli, F ^a   Merolle, M ^a   Neri, B ^b   Terracciano, A ^a  

^a SAPIENZA UNIVERSITY OF ROME   (Italy)

^b Italy   (Italy)

Author keywords

Conjugated hormones; LC MS MS; Natural androgen steroids; Urine

Indexed keywords

ENZYMATIC HYDROLYSIS; HUMAN URINE; MULTIPLE REACTION MONITORING (MRM); NEGATIVE IONIZATION;

DERIVATIVES; ENZYMES; HYDROLYSIS; IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETERS;

BODY FLUIDS;

ANDROGEN; STEROID;

ADULT; ARTICLE; CATTLE; CONJUGATION; ENZYME MECHANISM; EVALUATION; EXTRACTION; HUMAN; HYDROLYSIS; IONIZATION; LIQUID CHROMATOGRAPHY; MALE; MONITORING; NONHUMAN; NORMAL HUMAN; PRIORITY JOURNAL; SOLID; TANDEM MASS SPECTROMETRY; URINALYSIS;

BOVINAE;

EID: 8444251849     PISSN: 00032670     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.aca.2004.09.068     Document Type: Article

References (15)

1. Goodman, and Gilman Le basi farmacologiche della terapia 8th ed. 1993 Zanichelli Bologna, Italy
2. L.D. Bowers Clin. Chem. 43 7 1997 1299 1304
3. V. Ferchaud, P. Courcoux, B. Le Bizec, F. Monteau, and F. Andrè Analyst 25 2000 2255 2259
4. C. Ayotte, D. Goudreault, and A. Charlebois J. Chromatogr. B 687 1996 3 25
5. S.A. Hewitt, M. Kearney, J.W. Currie, P.B. Young, and D.G. Kennedy Anal. Chim. Acta 473 2002 99 109
6. M. Ho Choi, K. Rae Kim, and B. Chul Chung Steroids 65 2000 54 59
7. L.D. Bowers, and Sanaullah J. Chromatogr. B 687 1996 61 68
8. K.A. Bean, and J.D. Henion J. Chromatogr. B 690 1997 65 75
9. D.J. Borts, and L.D. Bowers J. Mass Spectr. 35 2000 50 61
10. Q. Jia, M.-F. Hong, Z.-X. Pan, and S. Orndorff J. Chromatogr. B 750 2001 81 91
11. T. Kuuranne, M. Vahermo, A. Leinonen, and R. Kostiainen J. Am. Soc. Mass Spectr. 11 2000 722 730
12. S. Liu, J. Griffiths, and J. Sjövall Anal. Chem. 75 2003 791 797
13. M. Benincasa, G.P. Cartoni, and F. Coccioli Ann. Chim. 77 1987 801 811
14. F. Buiarelli, G.P. Cartoni, F. Coccioli, A. De Rossi, and B. Neri J. Chromatogr. B 784 2003 1 15
15. 2002/657/EC (Commission decision of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results) Official Journal of the European Communities.