A combination of in situ ESR and in situ NMR spectroelectrochemistry for mechanistic studies of electrode reactions: The case of p-benzoquinone

Magnetic Resonance in Chemistry

Volumn 49, Issue 11, 2011, Pages 725-729

  Klod, Sabrina ^a   Dunsch, Lothar ^a  

^a IFW DRESDEN   (Germany)

Author keywords

Benzoquinone; Electroreduction; ESR spectroscopy; In situ spectroelectrochemistry

Indexed keywords

ELECTRODES; ELECTROLYTIC REDUCTION; ELECTRON SPIN RESONANCE SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE; PARAMAGNETIC RESONANCE; PARAMAGNETISM; REACTION INTERMEDIATES; REDOX REACTIONS;

BENZOQUINONES; ELECTRO REDUCTION; ELECTRODE REACTIONS; ESR SPECTROSCOPY; IN SITU SPECTROELECTROCHEMISTRY; MECHANISTIC STUDIES; P-BENZOQUINONE; REACTION MECHANISM; SITU SPECTROELECTROCHEMISTRY; SPECTROELECTROCHEMICAL METHODS;

SPECTROELECTROCHEMISTRY;

EID: 84155171167     PISSN: 07491581     EISSN: 1097458X     Source Type: Journal    
DOI: 10.1002/mrc.2819     Document Type: Article

References (26)

1. See for the different spectroscopic methods for example: Spectroelectrochemistry (Ed.: R. J. Gale), Plenum: London and New York, 1988;
2. Spectroelectrochemistry (Eds: W. Kaim and A. Klein), Royal Society of Chemistry: London, 2008;
3. K. Ashley, S. Pons, Chem. Rev. 1988, 88, 673;
4. A. Petr, L. Dunsch, A. Neudeck, J. Electroanal. Chem. 1996, 412, 153;
5. H. E. Toma, K. Araki, Curr. Org. Chem. 2002, 6, 21;
6. L. Kavan, L. Dunsch, ChemPhysChem 2007, 8, 975.
7. A. M. Waller, R. G. Compton, In situ electrochemical ESR, in Comprehensive Chemical Kinetics, vol. 29 (Eds: R. G. Compton, A. Hamnett), Elsevier: Amsterdam, 1989.
8. P. Rapta, L. Dunsch, J. Electroanal. Chem. 2001, 506, 22.
9. S. F. Yang, M. Zalibera, P. Rapta, L. Dunsch, Chem. Eur. J. 2006, 12, 7848.
10. S. Liu, S. Sun, J. Organomet. Chem. 2000, 599, 74.
11. T. D. W. Claridge, High-Resolution NMR Techniques in Organic Chemistry, Elsevier: Amsterdam, 1999.
12. S. Klod, F. Ziegs, L. Dunsch, Analyt. Chem. 2009, 81, 10262.
13. A. P. Tomilov, S. G. Mairanovskii, M. Y. Floshin, V. A. Smimov, The Electrochemistry of Organic Compounds (1st edn), John Wiley and Sons: New York, 1972.
14. D. W. Mincey, M. J. Popovich, P. J. Faustino, M. M. Hurst, J. A. Caruso, Anal. Chem. 1990, 62, 1197.
15. K. J. Vetter, Electrochemical Kinetics, Academic Press, Inc.: London, 1967.
16. W. Lorenz, K. H. Lubert, Z. Phys. Chem. 1972, 251, 49.
17. B. R. Eggins, J. Q. Chambers, Chem. Commun. 1969, 232;
18. B. R. Eggins, J. Q. Chambers, J. Electrochem. Soc. 1970, 117, 186.
19. V. D. Parker, Chem. Commun. 1969, 716.
20. V. D. Parker, Electrochim. Acta 1973, 18, 519.
21. F. Gerson, W. Huber, Electron Spin Resonance Spectroscopy of Organic Radicals, Wiley-VCH: Weinheim, 2003;
22. Landolt-Börnstein, Numerical Data and Functional Relationships in Science and Technology, New Series, vol. 9, Springer: Berlin, Heidelberg, New York, 1980, p. 162.
23. D. T. Sawyer, A. Sobkowiak, J. L. Roberts, Electrochemistry for Chemists (2nd edn), John Wiley and Sons: NY, 1995.
24. G. W. C. Milner, The Principles and Applications of Polarography, Green and Co: Longmans, 1957.
25. A. Neudeck, A. Petr, L. Dunsch, Synth. Met. 1999, 107, 143.
26. P. Rapta, A. Neudeck, A. Petr, L. Dunsch, J. Chem. Soc. Faraday Trans. 1998, 94, 3625.