Rapid characterization and identification of steroidal alkaloids in Sarcococca coriacea using liquid chromatography coupled with electrospray ionization quadropole time-of-flight mass spectrometry

Steroids

Volumn 77, Issue 1-2, 2012, Pages 138-148

  Musharraf, Syed Ghulam ^a   Goher, Madiha ^a   Ali, Arslan ^a   Adhikari, Achyut ^a   Choudhary, M Iqbal ^a,b   Atta Ur Rahman, ^a  

^a UNIVERSITY OF KARACHI   (Pakistan)

^b KING SAUD UNIVERSITY   (Saudi Arabia)

Author keywords

ESI QqTOF MS MS; Sarcococca coriacea; Steroidal alkaloids; Tandem mass spectrometry

Indexed keywords

5,6 DIHYDROSARCONIDINE; ALKALOID DERIVATIVE; CHONEMORPHINE; DICTYOPHLEBINE; DIMETHYLAMINE; EPIPACHYSAMINE D; HOOKERIANAMIDE B; HOOKERIANAMIDE C; ISO N FORMYLCHONEMORPHINE; ISOSARCODINE; N FORMYLCHONEMORPHINE; N3 METHYLEPIPACHYSAMINE D; N3 METHYLPACHYSAMINE A; SALIGENAMIDE; SARCORINE; SARCOVAGINE A; SARCOVAGINE D; SARCOVAGININE C; STEROID; TERMINALINE; UNCLASSIFIED DRUG;

ANALYTIC METHOD; ARTICLE; CHEMICAL BOND; COLLISIONALLY ACTIVATED DISSOCIATION; ELECTROSPRAY MASS SPECTROMETRY; ENERGY; LIQUID CHROMATOGRAPHY; MEDICINAL PLANT; NONHUMAN; PROTON TRANSPORT; SARCOCOCCA CORIACEA; TIME OF FLIGHT MASS SPECTROMETRY;

ALKALOIDS; BUXACEAE; CHROMATOGRAPHY, LIQUID; PLANT EXTRACTS; PLANT ROOTS; PLANTS, MEDICINAL; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; STEROIDS; TANDEM MASS SPECTROMETRY;

SARCOCOCCA;

EID: 83655201095     PISSN: 0039128X     EISSN: 18785867     Source Type: Journal    
DOI: 10.1016/j.steroids.2011.11.001     Document Type: Article

References (16)

1. M. Von Balthazar, P.K. Endress, and Y.-L. Qiu Phylogenetic relationships in Buxaceae based on nuclear internal transcribed spacers and plastid ndhF sequence Int J Plant Sci 161 2000 785 792
2. Atta-ur-Rahman, S. Anjum, A. Farooq, M.R. Khan, and M.I. Choudhary Two new pregnane-type steroidal alkaloids from Sarcococca saligna Phytochemistry 46 1997 771 775 (Pubitemid 27483842)
3. K.P. Devkota, M.I. Choudhary, R. Ranjit, Samreen, and N. Sewald Structure-activity relationship studies on antileishmanial steroidal alkaloids from Sarcococca hookeriana Nat Prod Res 21 2007 292 297 (Pubitemid 46729924)
4. M.I. Choudhary, A. Adhikari, Samreen, and Atta-ur-Rahman Antileishmanial Steroidal alkaloids from roots of Sarcococca coriacea J Chem Soc Pak 32 2010 799 802
5. K.M. Moghaddam, M. Arfan, M. Rafique, S. Rezaee, P.J. Fesharaki, A.R. Gohari, and A.R. Shahverdi The antifungal activity of Sarcococca saligna ethanol extract and its combination effect with fluconazole against different resistant Aspergillus species Biotechnol Appl Biochem 162 2010 127 133
6. K.P. Devkota, B.N. Lenta, M.I. Choudhary, Q. Naz, F.B. Fekam, P.J. Rosenthal, and N. Sewald Cholinesterase inhibiting and antiplasmodial steroidal alkaloids from Sarcococca hookeriana Chem Pharm Bull 55 2007 1397 1401 (Pubitemid 47414587)
7. Atta-ur-Rahman, F. Feroz, I. Naeem, Zaheer-ul-Haq, S.A. Nawaz, S. Khan, M.R. Khan, and M.I. Choudhary New pregnane-type steroidal alkaloids from Sarcococca saligna and their cholinesterase inhibitory activity Steroid 69 2004 735 741 (Pubitemid 39576717)
8. Atta-ur-Rahman, S. Anjum, A. Farooq, M.R. Khan, Z. Parveen, and M.I. Choudhary Antibacterial steroidal alkaloids from Sarcococca saligna J Nat Prod 61 1998 202 206 (Pubitemid 28136772)
9. W. Tuting, R. Alden, and P. Mischnick Fragmentation pattern of regioselectively O-methylated malto-oligosaccharides in electrospray ionization-mass spectrometry/collision induced dissociation Int J Mass Spectrom 232 2004 107 115
10. W.F. Smyth, S. McClean, C.J. Hack, V.N. Ramachandran, B. Doherty, C. Joyce, F. O'Donnell, T.J. Smyth, E. O'Kane, and P. Brooks The characterization of synthetic and natural-product pharmaceuticals by electrospray ionisation-mass spectrometry (ESI-MS) and liquid chromatography (LC)-ESI-MS Trends Anal Chem 25 2006 572 582 (Pubitemid 43767240)
11. A.J.C.F. Niege, V. Ricardo, C.T. Jose, E.G. Sergio, K.B. Jairo, P.L. Norbeto, and E.M.C. Antonio Fragmentation of diketopiperazines from Aspergillus fumigatus by electrospray ionization tandem mass spectrometry (ESI-MS/MS) J Mass Spectrom 42 2007 1279 1286
12. H.J. Li, Y. Jiang, and P. Li Characterizing distribution of steroidal alkaloids in Fritillaria spp. and related compound formulas by liquid chromatography-mass spectrometry combined with hierarchical cluster analysis J Chromatogr A 1216 2009 2142 2149
13. H.L. Li, J. Tang, R.H. Liu, M. Lin, B. Wang, Y. Lv, H. Huang, C. Zhang, and W. Zhang Characterization and identification of steroidal alkaloids in the Chinese herb Veratrum nigrum L. by high-performance liquid chromatography/ electrospray ionization with multi-stage mass spectrometry Rapid Commun Mass Spectrom 21 2007 869 879 (Pubitemid 46426806)
14. S.G. Musharraf, A. Ali, R.A. Ali, S. Yousuf, Atta-ur-Rahman, and M.I. Choudhary Analysis and development of structure-fragmentation relationships in with anolides using an electrospray ionization quadropole time-of-flight tandem mass spectrometry hybrid instrument Rapid Commun Mass Spectrom 25 2011 104 114
15. K.P. Devkota, B.N. Lenta, J.D. Wansi, M.I. Choudhary, D.P. Kisangau, Samreen, Q. Naz, and N. Sewald Bioactive 5α-pregnane-type steroidal alkaloids from Sarcococca hookeriana J Nat Prod 71 2008 1481 1484
16. M.I. Choudhary, K.P. Devkota, S.A. Nawaz, F. Shaheen, and Atta-ur-Rahman Cholinesterase-inhibiting new steroidal alkaloids from Sarcococca hookeriana of Nepalese origin Helv Chim Acta 87 2004 1099 1107