Evaluation of the influence of intermolecular electron-nucleus couplings and intrinsic metal binding sites on the measurement of 15N longitudinal paramagnetic relaxation enhancements in proteins by solid-state NMR

Journal of Biomolecular NMR

Volumn 51, Issue 3, 2011, Pages 293-302

  Nadaud, Philippe S ^a   Sengupta, Ishita ^a   Helmus, Jonathan J ^a   Jaroniec, Christopher P ^a  

^a OHIO STATE UNIVERSITY   (United States)

Author keywords

Magic angle spinning; Metal ion; Paramagnetic relaxation enhancement; Protein structure; Pseudocontact shift; Solid state NMR; Spin label

Indexed keywords

ASPARTIC ACID; COPPER ION; EDETIC ACID; GLUTAMIC ACID; NITROGEN 15;

ANALYTICAL PARAMETERS; ARTICLE; BINDING AFFINITY; BINDING SITE; CONTROLLED STUDY; ELECTRON; ISOTOPE LABELING; METAL BINDING; MOLECULAR INTERACTION; NITROGEN NUCLEAR MAGNETIC RESONANCE; PARAMAGNETIC RELAXATION ENHANCEMENT; PRIORITY JOURNAL; PROTEIN STRUCTURE; SOLID STATE; STOICHIOMETRY;

BINDING SITES; EDETIC ACID; ELECTRONS; NITROGEN ISOTOPES; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PROTEINS;

EID: 80755125957     PISSN: 09252738     EISSN: 15735001     Source Type: Journal    
DOI: 10.1007/s10858-011-9536-y     Document Type: Article

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