Preparation of high selectivity silicalite-1 membranes by two-step in situ hydrothermal synthesis

Chinese Science Bulletin

Volumn 56, Issue 33, 2011, Pages 3578-3582

  Chen, HongLiang ^a,b   Li, YanShuo ^b   Yang, JiSong ^a   Hou, YongXia ^a   Song, XueYing ^a   Hu, XiaoJun ^a   Yang, WeiShen ^b  

^a BEIJING UNIVERSITY OF POSTS AND TELECOMMUNICATIONS   (China)

^b DALIAN INSTITUTE OF CHEMICAL PHYSICS   (China)

Author keywords

high selectivity; hydrothermal synthesis; pervaporation; silica tube; silicalite 1 membrane

Indexed keywords

EID: 80355137007     PISSN: 10016538     EISSN: 18619541     Source Type: Journal    
DOI: 10.1007/s11434-011-4774-7     Document Type: Article

References (18)

1. Liu Y, Li Y, Yang W. Fabrication of highly b-oriented MFI film with molecular sieving properties by controlled in-plane secondary growth. J Am Chem Soc, 2010, 132: 1768-1769.
2. Caro J, Noack M. Zeolite membranes - recent developments and progress. Micropor Mesopor Mater, 2008, 115: 215-223.
3. Xiao W, Yang J, Shen D, et al. Synthesis and property of silicalite-1 membranes by restricting growth method with dilute solution. Micropor Mesopor Mater, 2010, 129: 22-29.
4. Bowen T C, Noble R D, Falconer J L. Fundamentals and applications of pervaporation through zeolite membrane. J Membr Sci, 2004, 245: 1-33.
5. Lin X, Kita H, Okamoto K. Silicalite membrane preparation, characterization, and separation performance. Ind Eng Chem Res, 2001, 40: 4069-4078.
6. Sato K, Sugimoto K, Nakane T. Synthesis of industrial scale NaY zeolite membranes and ethanol permeating performance in pervaporation and vapor permeation up to 130°C and 570 kPa. J Memb Sci, 2008, 310: 161-173.
7. McLeary E R, Jansen J C. basic views on the preparation of porous ceramic membrane layers. Topics Catalysis, 2004, 29: 85-92.
8. Wee S, Tye C, Bhatia S. Membrane separation process-pervaporation through zeolite membrane. Sep Purif Technol, 2008, 63: 500-516.
9. Li Y, Chen H, Liu J, et al. Microwave synthesis of LTA zeolite membranes without seeding. J Memb Sci, 2006, 277: 230-239.
10. Morigami Y, Kondo M, Abe J, et al. The first large-scale pervaporation plant using tubular-type module with zeolite NaA membrane. Sep Purif Technol, 2001, 25: 251-260.
11. Caro J, Noack M, Kolsch P, et al. Zeolite membranes-state of their development and perspective. Micropor Mesopor Mater, 2000, 38: 3-24.
12. van de Graaf J M, van der Bijl E, Stol A, et al. Effect of operating conditions and membrane quality on the separation performance of composite silicalite-1 membranes. Ind Eng Chem Res, 1998, 37: 4071-4083.
13. Nomura M, Bin T, Nakao S. Selective ethanol extraction from fermentation broth using a silicalite membrane. Sep Purif Technol, 2002, 27: 59-66.
14. Qureshi N, Meagher M M, Hutkins R W. Recovery of butanol from model solutions and fermentation broth using a silicalite/silicone membrane. J Membr Sci, 2004, 158: 115-125.
15. O'Brien D J, Roth L H, McAloon A J. Ethanol production by continuous fermentation-pervaporation: a preliminary economic analysis. J Membr Sci, 2000, 166: 105-111.
16. Li Q, Mihailova B, Creaser D, et al. Aging effects on the nucleation and crystallization kinetics of colloidal TPA-silicalite-1. Micropor Mesopor Mater, 2001, 43: 51-59.
17. Chen H, Li Y, Yang W. Preparation of silicalite-1 membrane by solution-filling method and its alcohol extraction properties. J Memb Sci, 2007, 296: 122-130.
18. Chen H, Song C, Yang W. Effects of aging on the synthesis and performance of silicalite membranes on silica tubes without seeding. Micropor Mesopor Mater, 2007, 102: 249-257.