Isolation and X-ray structure of deoxycholic acid from the sponge Ircinia sp.

Natural Product Communications

Volumn 6, Issue 9, 2011, Pages 1237-1238

  Singh, Keisham Sarjit ^a   Kaminsky, Werner ^b  

^a NATIONAL INSTITUTE OF OCEANOGRAPHY   (India)

^b UNIVERSITY OF WASHINGTON   (United States)

Author keywords

Crystallography; Deoxycholic acid; Ircinia sp.; Marine sponges; Spectroscopy; Sterol

Indexed keywords

3ALPHA 7BETA DIHYDROXY 5BETA CHOLAN 24 OIC ACID; DEOXYCHOLIC ACID; UNCLASSIFIED DRUG;

ANIMAL TISSUE; ANTIMICROBIAL ACTIVITY; ARTICLE; CHIRALITY; CONTROLLED STUDY; CRYSTAL STRUCTURE; DRUG ISOLATION; DRUG STRUCTURE; INDIA; IRCINIA; NONHUMAN; OPTICAL ROTATION; SEASHORE; SPECTROSCOPY; SPONGE (PORIFERA); STRUCTURE ACTIVITY RELATION; X RAY CRYSTALLOGRAPHY; X RAY DIFFRACTION; ANIMAL; CHEMICAL STRUCTURE; CHEMISTRY;

IRCINIA;

ANIMALS; CRYSTALLOGRAPHY, X-RAY; DEOXYCHOLIC ACID; MODELS, MOLECULAR; MOLECULAR STRUCTURE; PORIFERA;

EID: 80155169071     PISSN: 1934578X     EISSN: 15559475     Source Type: Journal    
DOI: 10.1177/1934578x1100600906     Document Type: Article

References (11)

1. Singh KS, Kaminsky WH, Rodrigues C, Naik CG. (2009) Structural studies and antimicrobial properties of norcembrane diterpenoid from an Indian soft coral Sinularia inelegans Tixier-Durivault. Journal of Chemical Sciences, 121, 1041-1046.
2. Allen FH, Kennard O, Watson DG, Brammer L, Orpen AG. (1987) Tables of bond lengths determined by X-ray and neutron-diffraction.1. Bond lengths in organic-compounds. Journal of the Chemical Society, Perkin Transactions, 2, S1-S19.
3. (a) Miyata M, Tohnai N, Hisaki I. (2007) Supramolecular chirality in crystalline assemblies of bile acids and their derivatives; Three-axial, tilt, helical, and bundle chirality. Molecules, 12, 1973-2000;
4. (b) Miyata M, Tohnai N, Hisaki I. (2007) Crystalline host-guest assemblies of steroidal and related molecules: Diversity, hierarchy, and supramolecular chirality. Accounts of Chemical Research, 40, 694-702;
5. (c) Jover A, Meijide F, Soto VH, Tato JV, Nunez ER, Ton-Nu H-T, Hofmann AF. (2004) Successful prediction of the hydrogen bond network of the 3-oxo-12 alpha-hydroxy-5 beta-cholan-24-oic acid crystal from resolution of the crystal structure of deoxycholic acid and its three 3,12-dihydroxy epimers. Steroids, 69, 379-388;
6. (d) Cerrini S, Pochetti G, Gallese F, Possagno, E. (1993) The monoclinic phase of the 2/1 inclusion compound between deoxycholic-acid and o-xylene. Acta Crystallographica, C49, 1087-1092;
7. (e) Limmatvapirat S, Yamaguchi K, Yonemochi E, Oguchi T, Yamamoto K. (1997) A 1:1 deoxycholic acid salicylic acid complex. Acta Crystallographica, C53, 803-805. (Pubitemid 127544213)
8. (a) Bruker 2007:APEX2 Version 2.1-4, SAINT version 7.34A, SADABS version 2007/4, Bruker AXS Inc, Madison, Wisconsin, USA;
9. (b) Altomare A, Burla C, Camalli M, Cascarano L, Giacovazzo C, Guagliardi A, Moliterni AGG, Polidori G, Spagna R. (1999) SIR97: a new tool for crystal structure determination and refinement Journal of Applied Crystallography, 32, 115-119;
10. (c) Sheldrick GM. (1997) SHELXL-97, Program for the Refinement of Crystal Structures. University of Göttingen, Germany;
11. (d) Farrugia LJ. (1997) Ortep-3 for Windows. Journal of Applied Crystallography, 30, 565.