Preparative separation of 1,3,6-pyrenetrisulfonic acid trisodium salt from the color additive D&C Green No. 8 (pyranine) by pH-zone-refining counter-current chromatography

Journal of Chromatography A

Volumn 1218, Issue 45, 2011, Pages 8249-8254

  Weisz, Adrian ^a   Mazzola, Eugene P ^a   Ito, Yoichiro ^b  

^a CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

^b NATIONAL HEART LUNG AND BLOOD INSTITUTE   (United States)

Author keywords

1,3,6 Pyrenetrisulfonic acid; 8 Hydroxy 1,3,6 pyrenetrisulfonic acid; Counter current chromatography; D C Green No. 8; Dyes; PH zone refining CCC; Pyranine

Indexed keywords

1,3,6-PYRENETRISULFONIC ACID; 8-HYDROXY-1,3,6-PYRENETRISULFONIC ACID; COUNTERCURRENT CHROMATOGRAPHY; PH-ZONE-REFINING CCC; PYRANINE;

HYDROPHOBIC CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; REFINING; RESONANCE;

SULFURIC ACID;

1,3,6 PYRENETRISULFONIC ACID TRISODIUM SALT; BUTANOL; DODECYLAMINE; DYE; PYRANINE; SODIUM HYDROXIDE; SULFONIC ACID DERIVATIVE; SULFURIC ACID; UNCLASSIFIED DRUG; WATER;

ANALYTIC METHOD; ARTICLE; CHEMICAL STRUCTURE; COUNTER CURRENT CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PH ZONE REFINING COUNTER CURRENT CHROMATOGRAPHY; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; SEPARATION TECHNIQUE; ULTRAVIOLET SPECTROSCOPY;

AMINES; ARYLSULFONATES; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; COUNTERCURRENT DISTRIBUTION; HYDROGEN-ION CONCENTRATION; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PYRENES; REFERENCE STANDARDS; SPECTROPHOTOMETRY, ULTRAVIOLET; SULFONIC ACIDS;

EID: 80054709034     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.09.049     Document Type: Article

References (24)

1. Code of Federal Regulations, Title 21, Part 74.1208 2011, U.S. Government Printing Office, Washington, DC.
2. Tietze E., Bayer O. Justus Liebigs Ann. Chem. 1939, 540:189.
3. Richfield-Fratz N. J. Assoc. Off. Anal. Chem. 1984, 67:762.
4. Sherma J., Mahn M., Follweiler J. J. Planar Chromatogr.: Mod. TLC 1988, 1:65.
5. Weisz A., Scher A.L., Shinomiya K., Fales H.M., Ito Y. J. Am. Chem. Soc. 1994, 116:704.
6. Ito Y., Shinomiya K., Fales H.M., Weisz A., Scher A.L. Modern Countercurrent Chromatography 1995, 156. American Chemical Society, Washington, DC. W.D. Conway, R.J. Petroski (Eds.).
7. Ito Y. High-Speed Counter-Current Chromatography Chemical Analysis 1996, vol. 132:121. Wiley, New York, (Chapter 6).
8. Ito Y., Ma Y. J. Chromatogr. A 1996, 753:1. (references cited therein).
9. Billardello B., Berthod A. Countercurrent Chromatography, the Support-Free Liquid Stationary Phase, Wilson & Wilson's Comprehensive Analytical Chemistry 2002, vol. 38:177. Elsevier, Amsterdam.
10. Ito Y. J. Chromatogr. A 2005, 1065:145. (references cited therein).
11. Denekamp C., Mandelbaum A., Weisz A., Ito Y. J. Chromatogr. A 1994, 685.
12. Weisz A., Mazzola E.P., Murphy C.M., Ito Y. J. Chromatogr. A 2002, 966:111.
13. Weisz A., Idina A., Ben-Ari J., Karni M., Mandelbaum A., Ito Y. J. Chromatogr. A 2007, 1151:82.
14. Tong S., Yan J., Guan Y.-X. J. Chromatogr. A 2008, 1212:48.
15. Wang X., Geng Y., Li F., Liu J. J. Sep. Sci. 2007, 30:3214.
16. Degenhardt A., Winterhalter P. J. Liq. Chromatogr. Rel. Technol. 2001, 24:1745.
17. Weisz A. High-Speed Countercurrent Chromatography Chemical Analysis 1996, vol. 132:337. Wiley, New York, (Chapter 12).
18. Oka H., Suzuki M., Harada K.-I., Iwaya M., Fujii K., Goto T., Ito Y., Matsumoto H., Ito Y. J. Chromatogr. A 2002, 946:157.
19. Weisz A., Ito Y. Encyclopedia of Separation Science (III) 2000, vol. 6:2588. Academic Press, London, (references cited therein).
20. Weisz A., Mazzola E.P., Matusik J.E., Ito Y. J. Chromatogr. A 2001, 923:87.
21. Weisz A., Mazzola E.P., Ito Y. J. Chromatogr. A 2009, 1216:4161.
22. Chevolot L., Colliec-Jouault S., Foucault A., Ratiskol J., Sinquin C. J. Chromatogr. B 1998, 706:43.
23. Pennanec R., Viron C., Blanchard S., Lafosse M. J. Liq. Chromatogr. Rel. Technol. 2001, 24:1575.
24. Weisz A., Miller G.C., Simpson J.T., Mazzola E.P., Ito Y. Pittsburgh Conference and Exposition on Analytical Chemistry and Applied Spectroscopy, PITTCON'99 1999, (Abstract 772).