An NMR thermometer for cryogenic magic-angle spinning NMR: The spin-lattice relaxation of 127I in cesium iodide

Journal of Magnetic Resonance

Volumn 212, Issue 2, 2011, Pages 460-463

  Sarkar, Riddhiman ^a   Concistr, Maria ^a   Johannessen, Ole G ^a   Beckett, Peter ^a   Denning, Mark ^a   Carravetta, Marina ^a   Al Mosawi, Maitham ^a   Beduz, Carlo ^a   Yang, Yifeng ^a   Levitt, Malcolm H ^a  

^a UNIVERSITY OF SOUTHAMPTON   (United Kingdom)

Author keywords

Magic angle spinning (MAS); Solid state NMR; Temperature measurement

Indexed keywords

MAGIC ANGLE SPINNING; SAMPLE TEMPERATURE; SOLID SAMPLES; SOLID STATE NMR; SPIN-LATTICE RELAXATION-TIME; TEMPERATURE DEPENDENT; TEMPERATURE RANGE;

CESIUM; CRYOGENICS; RELAXATION PROCESSES; SPIN-LATTICE RELAXATION; TEMPERATURE MEASUREMENT;

CESIUM IODIDE;

BROMIDE; CESIUM; CESIUM IODIDE; IODIDE; IODINE;

ARTICLE; CALIBRATION; CHEMISTRY; COLD; INSTRUMENTATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; THERMOMETER;

BROMIDES; CALIBRATION; CESIUM; COLD TEMPERATURE; IODIDES; IODINE; IODINE ISOTOPES; MAGNETIC RESONANCE SPECTROSCOPY; THERMOMETERS;

EID: 80053282632     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2011.08.021     Document Type: Article

References (20)

1. http://www.lakeshore.com/pdf-files/IRFILTERS/FOSdatasheet.pdf.
2. J.F. Haw, R.A. Crook, and R.C. Crosby Solid-solid phase transitions for temperature calibration in magic-angle spinning J. Magn. Reson. 66 1986 551 554
3. K.L. Anderson-Altmann, and D.M. Grant A solid-state 15N NMR study of the phase transitions in ammonium nitrate J. Phys. Chem. 97 1993 11096 11102
4. H.H. Limbach, J. Hennig, R. Kendrick, and C.S. Yannoni Proton-transfer kinetics in solids: tautomerism in free base porphines by 15N CPMAS NMR J. Am. Chem. Soc. 106 1984 4059 4060
5. R. Tycko Adiabatic rotational splittings and berrys phase in nuclear-quadrupole resonance Phys. Rev. Lett. 58 1987 2281 2284
6. R. Tycko, and K.R. Thurber Biomolecular solid state NMR with magic-angle spinning at 25 K J. Magn. Reson. 195 2008 179 186
7. 207Pb MAS spectra of solid lead nitrate. An accurate, sensitive thermometer for variable-temperature MAS J. Magn. Reson., Ser A 116 1995 215 220
8. 13C nuclear magnetic resonance of bathorhodopsin, the first photointermediate in mammalian vision J. Am. Chem. Soc. 130 2008 10490
9. G. Neue, and C. Dybowski Determining temperature in a magic-angle spinning probe using the temperature dependence of the isotropic chemical shift of lead nitrate Solid State Nucl. Magn. Reson. 7 1997 333 336 (Pubitemid 127451944)
10. 79Br in KBr powder J. Magn. Reson. 196 2009 84 87
11. B. Wehrle, F. Aguilar-Parrilla, and H.H. Limbach A novel 15N chemical-shift NMR thermometer for magic angle spinning experiments J. Magn. Reson. 87 1990 584 591
12. 7. Three sensitive chemical-shift thermometers J. Magn. Reson., Ser A 101 1993 299 306
13. T.F. Kemp, G. Balakrishnan, K.J. Pike, M.E. Smith, and R. Dupree Thermometers for low temperature magic angle spinning NMR J. Magn. Reson. 204 2010 169 172
14. M. Carravetta, O.G. Johannessen, M.H. Levitt, I. Heinmaa, R. Stern, A. Samoson, A.J. Horsewill, Y. Murata, and K. Komatsu Cryogenic NMR spectroscopy of endohedral hydrogen-fullerene complexes J. Chem. Phys. 124 2006
15. C.E. Tarr, L.M. Stacey, and C.V. Briscoe Nuclear spin-lattice relaxation in alkali halides at low temperatures Phys. Rev. 155 1967 272 278
16. J.v. Kranendonk Theory of quadrupolar nuclear spin-lattice relaxation Physica 20 1954 781 800
17. E.G. Wikner, W.E. Blumberg, and E.L. Hahn Nuclear quadrupole spin-lattice relaxation in alkali halides Phys. Rev. 118 1960 631 639
18. A. Hackmann, H. Seidel, R.D. Kendrick, P.C. Myhre, and C.S. Yannoni Magic-angle spinning NMR at near liquid-helium temperatures J. Magn. Reson. 79 1988 148 153
19. P.C. Myhre, G.G. Webb, and C.S. Yannoni Magic angle spinning nuclear magnetic resonance near liquid-helium temperatures. Variable temperature CPMAS spectra of the 2-norbornyl cation to 6 K J. Am. Chem. Soc. 112 1990 8991 8992
20. 7+ to 5 K J. Am. Chem. Soc. 112 1990 8992 8994