Rapid detection and identification of overdose drugs in saliva by surface-enhanced raman scattering using fused gold colloids

Pharmaceutics

Volumn 3, Issue 3, 2011, Pages 425-439

  Farquharson, Stuart ^a   Shende, Chetan ^a   Sengupta, Atanu ^a   Huang, Hermes ^a   Inscore, Frank ^a  

^a Real Time Analyzers Inc   (United States)

Author keywords

Drug analysis; Drug overdose; Emergency room; Illicit drugs; Raman spectroscopy; SERS

Indexed keywords

3,4 METHYLENEDIOXYMETHAMPHETAMINE; ACETYLSALICYLIC ACID; COCAINE; COLLOIDAL GOLD; DIAMORPHINE; DIAZEPAM; HOMOCOCAINE; HYDROCODONE; HYDROCODONE BITARTRATE PLUS PARACETAMOL; IBUPROFEN; LYSERGIDE; METHAMPHETAMINE; METHYLPHENIDATE; OXYCODONE; PARACETAMOL; PETHIDINE; SILVER;

ANALYZER; ARTICLE; CONTROLLED STUDY; DRUG DETERMINATION; DRUG IDENTIFICATION; DRUG ISOLATION; DRUG OVERDOSE; DRUG SALIVA LEVEL; DRUG STRUCTURE; EQUIPMENT DESIGN; HUMAN; POROSITY; PORTABLE EQUIPMENT; RAMAN SPECTROMETRY; REACTION TIME; SOLID PHASE EXTRACTION;

EID: 80053044859     PISSN: None     EISSN: 19994923     Source Type: Journal    
DOI: 10.3390/pharmaceutics3030425     Document Type: Article

References (37)

1. Jatlow, P. Cocaine: Analysis, Pharmacokinetics, and Metabolic Disposition. Yale J. Biol. Med. 1988, 61, 105-113.
2. Rainey, P.M.; Schonfeld, D.J. Toxicology, Monitoring of Drug Therapy, and Testing for Substance Abuse. In The Yale University School of Medicine Patient's Guide to Medical Tests; Zaret, B.L., Jatlow, P.I., Katz, L.D., Eds.; Houghton-Mifflin Co: New York, NY, USA, 1997; pp. 587-596.
3. Burgess, S. FDA limits acetaminophen in prescription combination products; requires liver toxicity warnings. U.S. Food and Drug Administration: Silver Spring, MD, USA, 13 January 2011; Available online http://www.fda.gov/NewsEvents/Newsroom/PressAnnouncements/ucm239894.htm. (accessed on 26 April 2011).
4. Bates, D.W.; Soldin, S.J.; Rainey, P.M.; Miceli, J.N. Strategies for Physician Education and Therapeutic Drug Monitoring. Clin. Chem. 1998, 44, 401-407.
5. Ammann, H.; Vinet, B. Accuracy, Precision, and Interferences of Three Modified EMIT Procedures for Determining Serum Phenobarbital, Urine Morphine, and Urine Cocaine Metabolite with a Cobas-Fara. Clin. Chem. 1991, 37, 2139-2141.
6. Rainey, P.M.; Rogers, K.E.; Roberts, W.L. Metabolite and Matrix Interference in Phenytoin Immunoassays. Clin. Chem. 1996, 42, 1645-1653.
7. Rainey, P.M.; Jatlow, P. Advances in Therapeutic Drug Monitoring In Advances in Pathology and Laboratory Medicine; Weinstein, R.S., Ed.; Mosby: St. Louis, MO, USA, 1993; Volume 6, pp. 185-206.
8. Puopolo, P.R.; Chamberlin, P.; Flood, J.G. Detection and Confirmation of Cocaine and Cocaethylene in Serum Emergency Toxicology Specimens. Clin. Chem. 1992, 38, 1838-1842.
9. Crouch, D.; Day, J.; Baudys, J.; Fatah, A. Evaluation of Saliva/Oral Fluid as an Alternate Drug Testing Specimen. Report Number 605-03. National Institute of Justice: Rockville, MD, USA, July 2004.
10. Van Dyke, C.; Ungerer, J.; Jatlow, P.; Barash, P.G.; Byck, R. Oral cocaine plasma concentrations and central effects. Science 1978, 200, 211-213.
11. Jenkins, A.J.; Oyler, J.M.; Cone, E.J. Comparison of heroin and cocaine concentrations in saliva with concentrations in blood and plasma. J. Anal. Toxicol. 1995, 19, 359-374.
12. Musshoff, F.; Madea, B. Cocaine and Benzoylecgonine Concentrations in Fluorinated Plasma Samples of Drivers Under Suspicion of Driving Under Influence. Forensic Sci. Int. 2010, 200, 67-72.
13. Sanaka, M.; Kuyama, Y.; Nishinakagawa, S.; Mineshita, S. Use of salivary acetaminophen concentration to assess gastric emptying rate of liquids. J. Gastroenterol. 2000, 35, 429-433.
14. Chamberlain, J. The Analysis of Drugs in Biological Fluids, 2nd ed.; CRC Press: Boca Raton, FL, USA, 1995. For example, Medimpex United Inc. (Bensalem, PA).
15. Shende, C.; Inscore, F.; Gift, A.; Maksymiuk, P.; Farquharson, S. Ten-minute analysis of drugs and metabolites in saliva by surface-enhanced Raman spectroscopy. P. Soc. Photo-Opt. Instrum. Eng. 2005, 6007, 165-171.
16. Farquharson, S.; Shende, C.; Inscore, F.; Maksymiuk, P.; Gift, A. Analysis of 5-fluorouracil in saliva using surface-enhanced Raman spectroscopy. J. Raman Spectrosc. 2005, 36, 208-212.
17. Kneipp, K.; Wang, Y.; Dasari, R.R.; Feld, M.S. Approach to Single-Molecule Detection Using Surface-Enhanced Resonance Raman Scattering (SERRS). Appl. Spectrosc. 1995, 49, 780-784.
18. Nie, S.; Emory, S.R. Probing Single Molecules and Single Nanoparticles by Surface-Enhanced Raman Scattering. Science 1997, 275, 1102-1106.
19. Farquharson, S.; Gift, A.; Shende, C.; Inscore, F.; Ordway, B.; Farquharson, C.; Murran, J. Surface-enhanced Raman Spectral Measurements of 5-Fluorouracil in Saliva. Molecules 2008, 13, 2608-2627.
20. Farquharson, S.; Lee, Y.H.; Nelson, C. Material for SERS and SERS sensors and method for preparing the same. U.S. Patent 6,623,977, 3 September 2003.
21. Farquharson, S.; Maksymiuk, P. Simultaneous chemical separation and surface-enhanced Raman spectral detection using metal-doped sol-gels. U.S. Patent 6,943,032, 13 September, 2005.
22. Farquharson, S.; Maksymiuk, P. Separation and Plural-point surface-enhanced Raman spectral detection using metal-doped sol-gels. U.S. Patent 6,943,031, 13 September 2005.
23. Turner, H.; Lamping, S. Commercial SERS Substrates for a Roadside Screening Device for Drugs in Oral Fluids. In Proceedings of the Joint Meeting of the International Council on Alcohol, Drugs and Traffic Safety and The International Association of Forensic Toxicologists, Seattle, WA, USA, 24 August, 2007.
24. Farquharson, S.; Gift, A.D.; Inscore, F.E.; Shende, C.S. SERS Method for Rapid Pharmacokinetic Analysis of Drugs in Saliva. U.S. Patent 7,393,691, 1 July 2008.
25. Farquharson, S.; Gift, A.D.; Maksymiuk, P.; Inscore, F. Rapid dipicolinic acid extraction from Bacillus spores detected by surface-enhanced Raman spectroscopy. Appl. Spectrosc. 2004, 58, 351-354.
26. Angel, S.M.; Carter, J.C.; Stratis, D.N.; Marquardt, B.J.; Brewer, W.E. Some new uses for filtered fiber-optic Raman probes: in situ drug identification and in situ and remote Raman imaging. J. Raman Spectrosc. 1999, 30, 795-805.
27. Carter, J.C.; Brewer, W.E.; Angel S.M. Raman spectroscopy for the in situ identification of cocaine and selected adulterants. Appl. Spectrosc. 2000, 54, 1876-1881.
28. Tsuchihashi, H.; Katagi, M.; Nishikawa, M.; Tatsuno, M.; Nishioka, H.; Nara, A.; Nishio, E.; Petty, C. Determination of Methamphetamine and Its Related Compounds Using Fourier Transform Raman Spectroscopy. Appl. Spectrosc. 1997, 51, 1796-1799.
29. Sägmüllera, B.; Schwarzeb, B.; Brehmc, G.; Trachtac, G.; Schneide, S. Identification of illicit drugs by a combination of liquid chromatography and surface-enhanced Raman scattering spectroscopy. J. Mol Struct. 2003, 661-662, 279-290.
30. Hodges, C.M.; Hendra, P.J.; Willis, H.A.; Farley, T. Fourier transform Raman spectroscopy of illicit drugs. J. Raman Spectrosc. 1989, 20, 745-749.
31. Neville, G.A.; Shurvell, H.F. Fourier transform Raman and infrared vibrational study of diazepam and four closely related 1,4-benzodiazepines. J. Raman Spectrosc. 1990, 21, 9-19.
32. Rana, V.; Cañamares, M.V.; Kubic, T.; Leona, M.; Lombardi, J.R. Surface-enhanced Raman Spectroscopy for Trace Identification of Controlled Substances: Morphine, Codeine, and Hydrocodone. J. Forensic Sci. 2011, 56, 200-207.
33. Gemperline, P. Practical Guide to Chemometrics, 2nd ed.; Taylor & Francis Group CRC Press: Boca Raton, FL, USA, 2006.
34. McCreery, R.; Horn, A.; Spencer, J.; Jefferson, E. Noninvasive Identification of Materials inside USP Vials with Raman Spectroscopy and a Raman Spectral Library. J. Pharm. Sci. 1998, 87, 1-8.
35. Kaliszan, R.; Nasal, A.; Turowski, M. Binding site for basic drugs on a1-acid glycoprotein as revealed by chemometric analysis of biochromatographic data. Biomed. Chromatogr. 1995, 9, 211-215.
36. Kala, J.; Pang, W.; Zubaidah, H.; Hashim, O. Proteomic Analysis of Whole Human Saliva Detects Different Altered Secretions of Seven Proteins in Heavy Cigarette Smokers Compared to Non-smokers. Int. J. Mol. Sci. 2010, 11, 4488-4505.
37. Badawi, N.; Simonsen, K.; Steentoft, A.; Bernhoft, I.; Linnet, K. Simultaneous Screening and Quantification of 29 Drugs of Abuse in Oral Fluid by Solid-Phase Extraction and Ultraperformance LC-MS/MS. Clin. Chem. 2009, 55, 2004-2018.