Improvement of accuracy in quantification of 3-monochloropropane-1,2-diol esters by Deutsche Gesellschaft für Fettwissenschaft standard methods C-III 18

European Journal of Lipid Science and Technology

Volumn 113, Issue 9, 2011, Pages 1168-1171

  Kaze, Naoki ^a   Sato, Hirofumi ^b   Yamamoto, Hiroshi ^a   Watanabe, Yomi ^b  

^a Ueda Oils and Fats MFG Co Ltd   (Japan)

^b OSAKA MUNICIPAL TECHNICAL RESEARCH INSTITUTE   (Japan)

Author keywords

3 Monochloropropane 1,2 diol (3 MCPD); Chloroform; DGF standard methods; Ethyl acetate; Extraction; Solvent

Indexed keywords

EID: 80052650952     PISSN: 14387697     EISSN: 14389312     Source Type: Journal    
DOI: 10.1002/ejlt.201000564     Document Type: Article

References (6)

1. Food Advisory Committee 2000 (accessed Oct. 2010). Genotoxicity of 3-monochloropropane-1, 2-diol, FdAC/Contaminants/48. Paper for Discussion. UK Food Standards Agency, London.
2. FAO/WHO 2001 (accessed Oct. 2010). Joint FAO/WHO Expert Committee on Food Additives (JECFA) Fifty-Seventh Meeting, Rome, 2001, Summary and Conclusions (Rome: Food and Agriculture Organization of the United Nations/World Health Organization).
3. Ester-bound 3-Chloropropane-1, 2-diol (3-MCPD esters) and Glycidol (glycidol esters). Deutsche Gesellschaft fuer Fettwissenschaft: DGF Standard Methods (14. Supplement) C-III 18, 2009.
4. Kaze, N., Sato, H., Yamamoto, H., Watanabe, Y., Bidirectional conversion between 3-monochloro-1, 2-propanediol and glycidol in course of the analytical procedure of DGF standard method. J. Am. Oil Chem Soc. DOI: 10.1007/s11746-011-1802-3.
5. Catalán, J., López, V., Pérez, P., Martín-Villamil, R., Rodriguez, J.-G., Progress towards a generalized solvent polarity scale: The solvatochromism of 2-(dimethylamino)-7-nitrofluorene and its homomorph 2-fluoro-7-nitrofluorene. Liebigs Ann. 1995, 2, 241- 252.
6. Weisshaar, R., Determination of total 3-chloropropane-1, 2-diol (3-MCPD) in edible oils by cleavage of MCPD esters with sodium methoxide. Eur. J. Lipid Sci. Technol. 2008, 110, 183- 186.