Development of high temperature comprehensive two-dimensional liquid chromatography hyphenated with infrared and light scattering detectors for characterization of chemical composition and molecular weight heterogeneities in polyolefin copolymers

Journal of Chromatography A

Volumn 1218, Issue 40, 2011, Pages 7173-7179

  Lee, D ^a   Miller, M D ^a   Meunier, D M ^a   Lyons, J W ^a   Bonner, J M ^a   Pell, R J ^a   Shan, C Li Pi ^a   Huang, T ^a  

^a DOW CHEMICAL COMPANY   (United States)

Author keywords

High temperature liquid chromatography; Polymers; Polyolefins; Size exclusion chromatography; Two dimensional liquid chromatography

Indexed keywords

2D SEPARATIONS; ABSORBANCES; ANALYTE CONCENTRATION; ANALYTES; CHEMICAL COMPOSITIONS; COMPLEX STRUCTURE; COMPREHENSIVE TWO-DIMENSIONAL; COMPREHENSIVE TWO-DIMENSIONAL LIQUID CHROMATOGRAPHY; HIGH TEMPERATURE; HIGH-TEMPERATURE LIQUID CHROMATOGRAPHIES; IR DETECTOR; LIGHT-SCATTERING DETECTORS; LOW-TO-HIGH; METHYL GROUP; QUANTITATIVE CHARACTERIZATION; SCATTERING SIGNALS; SIZE EXCLUSION; STRUCTURE PROPERTY RELATIONSHIPS; TWO DIMENSIONAL LIQUID CHROMATOGRAPHY; WAVELENGTH REGIONS;

ADSORPTION; BLENDING; COPOLYMERIZATION; COPOLYMERS; DETECTORS; ETHYLENE; FUNCTIONAL GROUPS; GEL PERMEATION CHROMATOGRAPHY; LIGHT SCATTERING; LIQUIDS; MOLECULAR WEIGHT; POLYETHYLENES; POLYPROPYLENES; PROPYLENE; REFRACTION; SCATTERING; THERMOPLASTICS; TWO DIMENSIONAL;

SIZE EXCLUSION CHROMATOGRAPHY;

COPOLYMER; ETHYLENE; POLYOLEFIN; POLYPROPYLENE;

ADSORPTION CHROMATOGRAPHY; ANALYTIC METHOD; ARTICLE; CHEMICAL COMPOSITION; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; ELUTION; FRACTIONATION; GEL PERMEATION CHROMATOGRAPHY; HIGH TEMPERATURE PROCEDURES; INFRARED SPECTROSCOPY; LIGHT SCATTERING; LIQUID CHROMATOGRAPHY; MOLECULAR WEIGHT; PRIORITY JOURNAL; QUANTITATIVE STUDY; SEPARATION TECHNIQUE; SPECTRAL SENSITIVITY; STRUCTURE ANALYSIS; TWO DIMENSIONAL LIQUID CHROMATOGRAPHY;

CHROMATOGRAPHY, AFFINITY; CHROMATOGRAPHY, GEL; HOT TEMPERATURE; LINEAR MODELS; MOLECULAR WEIGHT; POLYENES; POLYETHYLENES; POLYPROPYLENES; REPRODUCIBILITY OF RESULTS;

EID: 80052620930     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.08.036     Document Type: Article

References (41)

1. Balke S.T., Patel R.D. J. Polym. Sci. C: Polym. Lett. 1980, 18:453.
2. Trathnigg B. Prog. Polym. Sci. 1995, 20:615.
3. Yau W.W., Kirkland J.J., Bly D.D. Modern Size Exclusion Liquid Chromatography 1979, John Wiley & Sons, New York.
4. Yau W.W., Gillespie D. Polymer 2001, 42:8947.
5. Wild L. Adv. Polym. Sci. 1991, 98:1.
6. Monrabal B. J. Appl. Polym. Sci. 1994, 52:491.
7. Monrabal B., Sancho-Tello J., Mayo N., Romero L. Macromol. Symp. 2007, 257:71.
8. Flory P.J. Trans. Faraday Soc. 1955, 51:848.
9. Flory P.J. J. Chem. Phys. 1949, 17:223.
10. Bruaseth I., Soares J.B.P., Rytter E. Polymer 2004, 45:7853.
11. Brüll R., Pasch H., Raubenheimer H.G., Sanderson R., van Reenen A.J., Wahner U.M. Macromol. Chem. Phys. 2001, 202:1281.
12. Paredes B., Soares J.B.P., van Grieken R., Carrero A., Suarez I. Macromol. Symp. 2007, 257:103.
13. Tso C.C., DesLauriers P.J. Polymer 2004, 45:2657.
14. Miller M.D., DeGroot A.W., Lyons J.W., van Damme F., Winniford B., Pasch H., Macko T. Abstracts of Papers, 236th ACS National Meeting 2008, ANYL.
15. Albrecht A., Heinz L.-C., Lilge D., Pasch H. Macromol. Symp. 2007, 257:46.
16. Miller M.D., Lyons J.W., Degroot A.W., Winniford W.L., Herceg E. J. Appl. Polym. Sci. 2011, 10.1002/app.33809.
17. Macko T., Brüll R., Alamo R.G., Thomann Y., Grumel V. Polymer 2009, 50:5443.
18. Glöckner G. Gradient HPLC of Copolymers and Chromatographic Cross-fractionation 1991, Springer-Verlag, Berlin.
19. Malik M.I., Trathnigg B., Bartl K., Saf R. Anal. Chim. Acta 2010, 658:217.
20. van der Horst A., Schoenmakers P.J. J. Chromatogr. A 2003, 1000:693.
21. Kok S.J., Hankemeier T., Schoenmakers P.J. J. Chromatogr. A 2005, 1098:104.
22. Coulier L., Kaal E.R., Hankemeier T. J. Chromatogr. A 2005, 1070:79.
23. Edam R., Meunier D.M., Mes E.P.C., Van Damme F.A., Schoenmakers P.J. J. Chromatogr. A 2008, 1201:208.
24. Im K., Kim Y., Chang T., Lee K., Choi N. J. Chromatogr. A 2006, 1103:235.
25. Raust J.A., Brull A., Moire C., Farcet C., Pasch H. J. Chromatogr. A 2008, 1203:207.
26. Winther B., Reubsaet J.L.E. J. Sep. Sci. 2005, 28:477.
27. Im K., Park H.W., Lee S., Chang T. J. Chromatogr. A 2009, 1216:4606.
28. Jiang X.L., van der Horst A., Lima V., Schoenmakers P.J. J. Chromatogr. A 2005, 1076:51.
29. Moyses S. J. Sep. Sci. 2010, 33:1480.
30. Trathnigg B., Ahmed H. Anal. Bioanal. Chem. 2011, 399:1523.
31. Roy A., Miller M.D., Meunier D.M., Degroot A.W., Winniford W.L., Van Damme F.A., Pell R.J., Lyons J.W. Macromolecules 2010, 43:3710.
32. Ginzburg A., Macko T., Dolle V., Brull R. Eur. Polym. J. 2011, 47:319.
33. Adrian J., Esser E., Hellmann G., Pasch H. Polymer 2000, 41:2439.
34. Ortin A., Monrabal B., Montesinos J., del Hierro P. Macromol. Symp. 2009, 282:65.
35. Qiu X.H., Zhou Z., Gobbi G., Redwine O.D. Anal. Chem. 2009, 81:8585.
36. Monrabal B., Sancho-Tello J. LC-GC N. Am. 2009, 58.
37. Yau W.W. Macromol. Symp. 2007, 257:29.
38. Macko T., Brüll R., Wang Y., Coto B., Suarez I. J. Appl. Polym. Sci. ASAP 2011.
39. Tracz A., Jeszka J., Kucinska I., Chapel J.-P., Boiteux G. Macromol. Symp. 2001, 169:129.
40. Polymer Handbook 2005, John Wiley & Sons, New York. J. Brandrup, E.H. Immergut, E.A. Grulke, A. Abe, D.R. Bloch (Eds.).
41. Mourey T.H., Balke S.T. ACS Symp. Ser. 1993, 521:180.