Spectrofluorimetric methods for the determination of gemifloxacin in tablets and spiked plasma samples

Journal of Fluorescence

Volumn 21, Issue 3, 2011, Pages 1001-1007

  Tekkeli, Serife Evrim Kepekci ^b   Önal, Armaǧan ^a  

^a ISTANBUL UNIVERSITY   (Turkey)

^b BEZMIALEM VAKIF UNIVERSITY   (Turkey)

Author keywords

7 Chloro 4 nitrobenzofurazon; Fluorescamine; Gemifloxacin; Spiked plasma; Tablets

Indexed keywords

7-CHLORO-4-NITROBENZOFURAZON; FLUORESCAMINES; GEMIFLOXACIN; SPIKED PLASMA; TABLETS;

CHLORINE COMPOUNDS; FLUORESCENCE;

PLASMAS;

ANTIINFECTIVE AGENT; GEMIFLOXACIN; NAPHTHYRIDINE DERIVATIVE; QUINOLONE DERIVATIVE;

BLOOD; CONFERENCE PAPER; HUMAN; METHODOLOGY; SPECTROFLUOROMETRY; STANDARD; TABLET;

ANTI-BACTERIAL AGENTS; FLUOROQUINOLONES; HUMANS; NAPHTHYRIDINES; REFERENCE STANDARDS; SPECTROMETRY, FLUORESCENCE; TABLETS;

EID: 80052587038     PISSN: 10530509     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10895-010-0759-1     Document Type: Conference Paper

References (31)

1. Hohl AF, Frei R, Punter V, Graevenitz A, Knapp C, Washington J, Johnson D, Jones RN (1998) International multicenter investigation of LB20304, a new fluoronaphthyridone. Clin Microbiol Infect 4:280-284 (Pubitemid 28256632)
2. World Medical Association (1996) World Medical Association Declaration of Helsinki: ethical principles for medical research involving human subjects
3. Krishna MV, Sankar DG (2008) Utility of δ and π acceptors for the spectrophotometric determination of gemifloxacin mesylate in pharmaceutical formulations. E-J Chem 5(3):493-498
4. Krishna MV, Sankar DG (2008) Spectrophotometric determination of gemifloxacin mesylate in pharmaceutical formulations through ion-pair complex formation. E-J Chem 5(3):515-520
5. Elbashir AA, Saad B, Ali ASM, Al-Azzam KMM, Aboul-Enein HY (2008) Validated stability indicating assay of gemifloxacin and lomefloxacin in tablet formulations by capillary electrophoresis. J Liq Chromatogr Related Technol 31:1465-1477 (Pubitemid 351596374)
6. Doyle E, Fowles SE, McDonnell DF, White SA (2000) Rapid determination of gemifloxacin in human plasma by high performance liquid chromatography-tandem mass spectrometry. J Chromatogr B 746:191-198 (Pubitemid 30657935)
7. Lee W, Yong Hong C (2000) Direct liquid chromatographic enantiomer seperation for new fluoroquinolones including gemifloxacin. J Chromatogr A 879(2):113-118
8. Cho SI, Shim J, Kim MS, Kim YK (2004) On-line sample cleanup and chiral separation of gemifloxacin in a urinary solution using chiral crown ether as a chiral selector in microchip electrophoresis. J Chromatogr A 1055:241-245 (Pubitemid 39422466)
9. Ghosh PB, Whitehouse M (1968) 7-Chloro-4-nitrobenzofurazan: a new fluorogenic reagent for amino acids and other amines. Biochem J 108:155-156
10. Undefriend S, Stein S, Bohlem P, Dairman W, Leimgruber W, Weigele M (1972) Fluorescamine: a reagent for assay of amino acids, peptides, proteins, and primary amines in the picomole range. Science (Washington, DC) 178:871-872
11. Taha EA, Salama NN, Fattah L (2006) Spectrofluorimetric and spectrophotometric stability-indicating methods for determination of some oxicams using 7-chloro-4-nitrobenz-2-oxa-1, 3-diazole (NBD-Cl). Chem Pharm Bull 54(5):653-658
12. Darwish IA, Amer SM, Abdine HH, Al-Rayes LI (2009) Spectrofluorimetric determination of fluvoxamine in dosage forms and plasma via derivatization with 4-chloro-7-nitrobenzo-2-oxa-1, 3-diazole. J Fluoresc 19(3):463-471
13. Hassan EM, Belal F, Al-Deeb OA, Khalil NY (2001) Spectrofluorimetric determination of vigabatrin and gabapentin in dosage forms and spiked plasma samples through derivatization with 4- chloro-7-nitrobenzo-2-oxa-1, 3-diazole. J AOAC Int 84(4):1017-1024 (Pubitemid 33610531)
14. El-Emam AA, Hansen SH, Moustafa MA, El-Ashry SM, El- Sherbiny DT (2004) Determination of lisinopril in dosage forms and spiked human plasma through derivatization with 7-chloro-4- nitrobenzo-2-oxa-1, 3-diazole (NBD-Cl) followed by spectrophotometry or HPLC with fluorimetric detection. J Pharm Biomed Anal 34(1):35-44 (Pubitemid 38114765)
15. Onal A, Kepekci SE, Oztunc A (2005) Spectrophotometric methods for the determination of the antidepressant drug paroxetine hydrochloride in tablets. J AOAC Int 88(2):490-495 (Pubitemid 40479405)
16. Onal A, Sagirli O (2009) Spectrophotometric and spectrofluorimetric methods for the determination of pregabalin in bulk and pharmaceutical preparation. Spectrochim Acta A Mol Biomol Spectrosc 72(1):68-71, Epub 2008 Aug 28
17. El-Enany N (2007) Spectrofluorometric determination of fluvoxamine in dosage forms, spiked plasma, and real human plasma by derivatization with fluorescamine. J AOAC Int 90(2):376-383 (Pubitemid 350067235)
18. Suliman FE, Al-Lawati ZH, Al-Kindy SM (2008) A spectrofluorimetric sequential injection method for the determination of penicillamine using fluorescamine in the presence of betacyclodextrins. J Fluoresc 18(6):1131-1138, Epub 2008 May 22
19. Adamou R, Coly A, Douabalé SE, Saleck ML, Gaye-Seye MD, Tine A (2005) J Fluoresc 15(5):679-688
20. Aydogmus Z (2009) Simple and sensitive spectrofluorimetric method for the determination of oseltamivir phosphate in capsules through derivatization with fluorescamine. J Fluoresc 19(4):673-679, Epub 2009 Jan 28
21. Belal F, Abdine H, Al-Majed A, Khalil NY (2002) Spectrofluorimetric determination of vigabatrin and gabapentin in urine and dosage forms through derivatization with fluorescamine. J Pharm Biomed Anal 27:253-260 (Pubitemid 33001403)
22. Segura Carretero A, Cruces-Blanco C, Fernández Peinado S, El Bergmi R, Fernández Gutiérrez A (1999) Fluorimetric determination of procaine in pharmaceutical preparations based on its reaction with fluorescamine. J Pharm Biomed Anal 21:969-974
23. Lakowicz JR (1999) Principles of fluorescence spectroscopy. Kluwer Academic/Plenum, New York
24. Weber G, Teale FWJ (1957) Fluorescence excitation spectrum of organic compounds in solution-Part 1: systems with quantum yield independent of the exciting wavelenght. Trans Faraday Soc 53:640-648
25. Eastman JW (1967) Quantitative spectrofluorimetry-the fluorescence quantum yield of quinine sulfate. Photochem Photobiol 6:55-72
26. Rote AR, Pingle SP (2009) Reverse phase-HPLC and HPTLC methods for determination of gemifloxacin mesylate in human plasma. J Chromatogr, B 877(29):3719-3723
27. Pesez M, Batros J (1974) Colorimetric and fluorimetric analysis of organic compounds and drugs. Marcel Dekker, New York, p 170
28. Imai K, Toyo'oka T, Miyano H (1984) Fluorigenic reagents for primary and secondary amines and thiols in high-performance liquid chromatography: a review. Analyst 109:1365-1373
29. Imai K, Uzu S, Toyoóka T (1989) Fluorogenic reagents having benzofurazan structure in liquid chromatography. J Pharm Biomed Anal 7:1395-1403 (Pubitemid 20253561)
30. Job P (1928) Formation and stability of inorganic complexes in solution. Anal Chem 9:113-203
31. Allen A, Bygate E, Oliver S, Johnson M, Ward C, Cheon AJ, Choo YS, Kim IC (2000) Pharmacokinetics and tolerability of gemifloxacin (SB-265805) after administration of single oral doses to healthy volunteers. Antimicrob Agents Chemother 44 (6):1604-1608 (Pubitemid 30340802)