A test to determine the nature and presence of the memory effect columns packed with the amylose tris(3,5-dimethylphenylcarbamate) stationary phase

Journal of Chromatography A

Volumn 1218, Issue 37, 2011, Pages 6302-6307

  Putnam, Joel ^a   Guiochon, Georges ^a  

^a UNIVERSITY OF TENNESSEE   (United States)

Author keywords

CHIRALPAK AD; Ethanesulfonic acid; Memory effect; Normal phase chromatography; Reproducibility

Indexed keywords

CHIRALPAK AD; ETHANESULFONIC ACID; MEMORY EFFECTS; NORMAL-PHASE CHROMATOGRAPHY; REPRODUCIBILITIES;

CHROMATOGRAPHY; ENANTIOMERS; ENANTIOSELECTIVITY; SOLVENTS;

BEHAVIORAL RESEARCH;

AMYLOSE TRIS(3,5 DIMETHYLPHENYLCARBAMATE); AROMATIC AMINO ACID; FENCLONINE ETHYL ESTER; FENCLONINE METHYL ESTER; HALOAMINO ACID; KETOPROFEN; POLYSACCHARIDE; PROPRANOLOL; SEROTONIN ANTAGONIST; TRANS STILBENE OXIDE; UNCLASSIFIED DRUG;

ARTICLE; CHROMATOGRAPHY; CONTROLLED STUDY; DRUG DETERMINATION; ENANTIOMER; ENANTIOSELECTIVITY; PRIORITY JOURNAL; RACEMIC MIXTURE; SENSITIVITY ANALYSIS; SEPARATION TECHNIQUE;

ALKANESULFONATES; AMYLOSE; CHROMATOGRAPHY, LIQUID; FENCLONINE; KETOPROFEN; MODELS, CHEMICAL; PHENYLCARBAMATES; PROPRANOLOL; STEREOISOMERISM; STILBENES;

EID: 80051875015     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.06.060     Document Type: Article

References (8)

1. Guillarme D., Nguyen D.T., Rudaz S., Veuthey J. Eur. J. Pharm. Biopharm. 2007, 66:475.
2. Introduction to Modern Liquid Chromatography, 3rd Edition, Wiley Sons, 2010, Ch. Method Validation, pp. 554-555.
3. Ye Y.K., Stringham R.W. J. Chromatogr. A 2001, 927:47.
4. Ye Y.K., Lord B., Stringham R.W. J. Chromatogr. A 2002, 945:139.
5. Putnam J., Guiochon G. J. Chromatogr. A 2009, 1216:8488.
6. J. Putnam, G. Guiochon, Minimizing the Memory Effect on the CHIRALPAK AD Stationary Phase, Tech. rep., University of Tennesse, Knoxville, TN, USA, PREP, 2009 Symposium (2009).
7. Mihlbachler K., Kaczmarski K., Seidel-Morgenstern A., Guiochon G. J. Chromatogr. A 2002, 955:35.
8. Applications CD, Tech. rep., Chiral Technologies, Inc (2006).