Characterization of the pore structure of metakaolin-derived geopolymers by neutron scattering and electron microscopy

Journal of Applied Crystallography

Volumn 44, Issue 4, 2011, Pages 697-707

  Maitland, C F ^a   Buckley, C E ^a   Oconnor, B H ^a   Butler, P D ^b   Hart, R D ^a  

^a CURTIN UNIVERSITY   (Australia)

^b NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

Author keywords

geopolymers; scanning electron microscopy; Small angle neutron scattering; transmission electron microscopy; ultra small angle neutron scattering

Indexed keywords

CHEMICAL COMPOSITIONS; CLOSED PORE; CONTRAST VARIATION; EXPECTED VALUES; EXPERIMENTAL CONDITIONS; LENGTH SCALE; LOWER LIMITS; METAKAOLINS; MULTIPHASE MATERIALS; NANOPOROSITY; PORE FLUIDS; PORE MORPHOLOGY; PORE SYSTEM; PORE WIDTH; Q-DEPENDENCE; QUANTITATIVE PREDICTION; SCANNING AND TRANSMISSION ELECTRON MICROSCOPY; SCANNING ELECTRONS; SCATTERING LENGTH DENSITY; SMALL-ANGLE NEUTRON SCATTERING; STRUCTURAL CHANGE; THREE PHASIS; TRANSMISSION ELECTRON; ULTRA-SMALL-ANGLE NEUTRON SCATTERING; ULTRAMICROTOMING;

COMPRESSIVE STRENGTH; DEHYDRATION; DEWATERING; ELECTRONS; EXPERIMENTS; GEOPOLYMERS; INORGANIC POLYMERS; MORPHOLOGY; NEUTRONS; SCANNING ELECTRON MICROSCOPY; SODIUM; TRANSMISSION ELECTRON MICROSCOPY;

NEUTRON SCATTERING;

EID: 79960641908     PISSN: 00218898     EISSN: 16005767     Source Type: Journal    
DOI: 10.1107/S0021889811021078     Document Type: Article

References (38)

1. Barker, J. G., Glinka, C. J., Moyer, J. J., Kim, M. H., Drews, A. R. & Agamalian, M. (2005). J. Appl. Cryst. 38, 1004-1011.
2. Bell, J. L. (2007). Personal communication.
3. Bell, J. L., Gordon, M. & Kriven, W. M. (2006). Microsc. Microanal. 12(Suppl. 2), 552CD-553CD.
4. Bell, J. L. & Kriven, W. M. (2004). Microsc. Microanal. 10, 590-591.
5. Buckley, C. E., O' Connor, B. & Rowles, M. (2002). AINSE Progress Report for 02/014. Australian Institute of Nuclear Science and Engineering, Lucas Heights, NSW, Australia.
6. Ciccariello, S. (2003). Fibres Text. Eastern Eur. 11, 54-60.
7. Ciccariello, S. & Riello, P. (2007). J. Appl. Cryst. 40, 282-289.
8. Davidovits, J. (1991). J. Therm. Anal. 37, 1633-1656.
9. Duxson, P., Fernandez-Jimenez, A., Provis, J. L., Lukey, G. C., Palomo, A. & Van Deventer, J. S. J. (2007). J. Mater. Sci. 42, 2917-2933.
10. Duxson, P., Mallicoat, S. L., Lukey, G. C., Kriven, W. M. & van Deventer, J. S. J. (2007). Colloids Surf. A, 292, 8-20.
11. Duxson, P., Provis, J. L., Lukey, G. C., Mallicoat, S. L., Kriven, W. M. & Van Deventer, J. S. J. (2005). Colloids Surf. A, 269, 47-58.
12. Goodisman, J. & Brumberger, H. (1971). J. Appl. Cryst. 4, 347-351.
13. Gourley, J. T. & Johnson, G. B. (2005). GGC2005 International Workshop on Geopolymers and Geopolymer Concrete, 28-29 September, Curtin University, Perth, Western Australia, Australia.
14. Hardjito, D., Wallah, S. E., Sumajouw, D. M. J. & Rangan, B. V. (2005). Aust. J. Struct. Eng. 6, 77-85.
15. Hos, J. P., McCormick, P. G. & Byrne, L. T. (2002). J. Mater. Sci. 37, 2311-2316.
16. Kline, S. R. (2006). J. Appl. Cryst. 39, 895-900.
17. Kriven, W. M. (2004). Geopolymers: Recent Work and Future Directions, http://www.porotech.net/images/ACERS2004.pdf.
18. Kriven, W. M. & Bell, J. L. (2004). 28th International Conference on Advanced Ceramics and Composites B, Ceramic Engineering and Science Proceedings, Vol. 25, pp. 99-104.
19. Kriven, W. M., Bell, J. L. & Gordon, M. (2003). Advances in Ceramic Matrix Composites IX, Ceramic Transactions, Vol. 153, pp. 227-250. Westerville: American Ceramic Society.
20. Kriven, W. M., Gordon, M. & Bell, J. L. (2004). Microsc. Microanal. 10(Suppl 2), 404-405.
21. Lukey, G. C. & Van Deventer, J. S. J. (2005). GGC2005 International Workshop on Geopolymers and Geopolymer Concrete, 28-29 September, Curtin University, Perth, Western Australia, Australia.
22. Maitland, C. F. (2011). PhD thesis, Curtin University of Technology, Perth, Western Australia, Australia. In preparation.
23. Palomo, A., Grutzeck, M. W. & Blanco, M. T. (1999). Cem. Concr. Res. 29, 1323-1329.
24. Perera, D. S., Uchida, O., Vance, E. R. & Finnie, K. S. (2007). J. Mater. Sci. 42, 3099-3106.
25. Perera, D. S., Vance, E. R., Aly, Z., Finnie, K. S., Hanna, J. V., Nicholson, C. L., Trautman, R. L. & Stewart, M. W. A. (2003). ASME Conf. Proc. 2003, 1807-1814.
26. Peterlin, A. (1965). Makromol. Chem. 87, 152-155.
27. Phair, J. W., Schulz, J. C., Bertram, W. K. & Aldridge, L. P. (2003). Cem. Concr. Res. 33, 1811-1824.
28. Porod, G. (1982). Small-Angle X-ray Scattering, edited by O. Glatter & O. Kratky, pp. 17-51. New York: Academic Press.
29. Rahier, H., van Mele, B. & Wastiels, J. (1995). J. Mater. Sci. 31, 80-85.
30. Rowles, M. (2004). PhD thesis, Curtin University of Technology, Perth, Western Australia, Australia.
31. Rowles, M. R., Hanna, J. V., Pike, K. J., Smith, M. E. & O' Connor, B. H. (2007). Appl. Magn. Reson. 32, 663-689.
32. Rowles, M. R. & O' Connor, B. H. (2003). J. Mater. Chem. 13, 1161-1165.
33. Rowles, M. R. & O'Connor, B. H. (2009). J. Am. Ceram. Soc. 92, 2354-2361.
34. Spurr, A. R. (1969). J. Ultrastruct. Res. 26, 31-43.
35. Stuhrman, H. B. & Kirste, R. G. (1965). Z. Phys. Chem. Frankfurt, 46, 247-250.
36. Subaer (2004). PhD thesis, Curtin University, Perth, Western Australia, Australia.
37. Vance, E. R., Hadley, J. H., Hsu, F. H. & Drabarek, E. (2007). J. Am. Ceram. Soc. 91, 664-666.
38. Wu, W. (1982). Polymer, 23, 1907-1912.