Solid-phase microextraction-gas chromatography-mass spectrometry method validation for the determination of endogenous substances: Urinary hexanal and heptanal as lung tumor biomarkers

Analytica Chimica Acta

Volumn 701, Issue 1, 2011, Pages 29-36

  Guadagni, Rossella ^a,b   Miraglia, Nadia ^a   Simonelli, Angela ^a,b   Silvestre, Angela ^a   Lamberti, Monica ^a   Feola, Daniela ^a   Acampora, Antonio ^a   Sannolo, Nicola ^a  

^a SECOND UNIVERSITY OF NAPLES   (Italy)

^b UNIVERSITY OF NAPLES FEDERICO II   (Italy)

Author keywords

Bioanalytical method validation; Endogenous substances; Heptanal; Hexanal; Lung tumor biomarkers; Urine

Indexed keywords

BIOANALYTICAL METHODS; ENDOGENOUS SUBSTANCES; HEPTANAL; HEXANAL; LUNG TUMOR; URINE;

ALDEHYDES; BIOMARKERS; BLOOD; CHEMICAL ANALYSIS; DISEASES; EXTRACTION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; ORGANIC COMPOUNDS; TUMORS;

BIOLOGICAL ORGANS;

ALDEHYDE; HEPTYL ALDEHYDE; HEXANAL; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; CLINICAL ARTICLE; CONTROLLED STUDY; HEPTANAL URINE LEVEL; HEXANAL URINE LEVEL; HUMAN; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LUNG CANCER; MASS FRAGMENTOGRAPHY; MOLECULAR STABILITY; PRIORITY JOURNAL; PROCESS OPTIMIZATION; REPRODUCIBILITY; SOLID PHASE MICROEXTRACTION; STORAGE TEMPERATURE; THERMOSTABILITY; URINALYSIS; URINARY EXCRETION; URINE LEVEL; VALIDATION PROCESS;

ALDEHYDES; CALIBRATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; LUNG NEOPLASMS; SENSITIVITY AND SPECIFICITY; SOLID PHASE MICROEXTRACTION; TUMOR MARKERS, BIOLOGICAL;

EID: 79960337690     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2011.05.035     Document Type: Article

References (42)

1. Mlakar A., Spiteller G. Biochim. Biophys. Acta 1994, 1214:209-220.
2. Li N., Deng C., Yin X., Yao N., Shen X., Zang X. Anal. Biochem. 2005, 342:318-326.
3. Toyokuni S., Okamoto K., Yodoi J., Hiai H. FEBS Lett. 1995, 358:1-3.
4. Szatrowski T.P., Nathan C.F. Cancer Res. 1991, 51:794-798.
5. Halliwell B. Lancet 1994, 344:721-724.
6. Kato S., Post G.C., Bierbaum V.M., Koch T.H. Anal. Biochem. 2002, 305:251-259.
7. Elbeler S.E., Clifford A.J., Shibamoto T. J. Chromatogr. B 1997, 702:211-215.
8. Kato S., Burke P.J., Koch T.H., Bierbaum V.M. Anal. Chem. 2001, 73:2992-2997.
9. Yazdanpanah M., Luo X., Lau R., Greenberg M., Fisher L.J., Lehotay D.C. Free Radic. Biol. Med. 1997, 23:870-878.
10. Phillips M., Gleeson K., Hughes J.M.B., Greenberg J., Cataneo R.N., Baker L. Lancet 1999, 353:1930-1933.
11. O'Neill H.J., Gordon S.M., O'Neill M.H., Gibbons R.D., Szidon J.P. Clin. Chem. 1988, 34:1613-1618.
12. Gordon S.M., Szidon J.P., Krotoszynki B.K., Gibbons R.D., O'Neill H.J. Clin. Chem. 1985, 31:1278-1282.
13. Preti G., Labows J.N., Kostelc J.G., Aldinger S., Daniele R. J. Chromatogr. 1988, 432:1-11.
14. Fuchs P., Loeseken C., Schubert J.K., Mieikisch W. Int. J. Cancer 2010, 126:2663-2670.
15. Larstad M., Ljungkvist G., Olin A.C., Toren K. J. Chromatogr. B 2002, 766:107-114.
16. St German F., Vachon B., Montgomery J., Des Rosiers C. Free Radic. Biol. Med. 1997, 23:166-172.
17. Deng C.H., Li N., Zhang X.M. J. Chromatogr. B 2004, 813:47-52.
18. Deng C.H., Zhang X.M., Li N. J. Chromatogr. B 2004, 808:269-277.
19. Phillips M., Greenberg J. J. Chromatogr. 1991, 564:242-249.
20. Qin T., Xu X.B., Polak T., Pacakova V., Stulik K., Jech L. Talanta 1997, 44:1683-1690.
21. Andreoli R., Manini P., Corradi M., Mutti A., Niessen W.M.A. Rapid Commun. Mass Spectrom. 2003, 17:637-645.
22. Frankel E.N., Tappel A.L. Lipids 1991, 26:479-484.
23. Nakazono T., Kashimura S., Hayashiba Y., Hisatomi T., Hara K. J. Forensic Sci. 2002, 47:568-572.
24. Nagy K., Pollreissz F., Takats Z., Vekey K. Rapid Commun. Mass Spectrom. 2004, 18:2473-2478.
25. Struys E.A., Jansen E.E.W., Gibson K.M., Jakobs C., Inherit J. Metab. Dis. 2005, 28:913-920.
26. Luo X.P., Yazdanpanah M., Bhooi N., Lehotay D.C. Anal. Biochem. 1995, 228:294-298.
27. Stalikas C.D., Konidari C.N. Anal. Biochem. 2001, 290:108-115.
28. Spies-Martin D., Sommerburg O., Langhans C.D., Leichsenring M. J. Chromatogr. B 2002, 774:231-239.
29. Lili L., Xu H., Song D., Cui Y., Hu S., Zhang G. J. Chromatogr. A 2010, 1217:2365-2370.
30. Eggink M., Wijtmans M., Ekkebus R., Lingeman H., de Esch I.J.P., Kool J., Niessen W.M.A., Irth H. Anal. Chem. 2008, 80:9042-9051.
31. Baños C.E., Silva M. J. Chromatogr. B 2010, 878:653-658.
32. Takamoto S., Sakura N., Yashiki M., Kojima M.T. J. Chromatogr. B: Biomed. Sci. Appl. 2001, 758(1):123-128.
33. Takamoto S., Sakura N., Namera A., Yashiki M. J. Chromatogr. B: Analyt. Technol. Biomed. Life Sci. 2004, 806(1):59-63.
34. Mills G.A., Walker V. J. Chromatogr. B: Biomed. Sci. Appl. 2001, 753(2):259-268.
35. Walker V., Mills G.A., Stansbridge E.M. J. Chromatogr. B: Analyt. Biomed. Life Sci. 2009, 877(8-9):784-790.
36. US FDA, Food and Drug Administration: Center for Drug Evaluation Research, 2001. Guidance for Industry: Bioanalytical Method Validation. Available from: http://www.fda.gov/downloads/Drugs/GuidanceComplianceRegulatorInformation/Guidances/ucm070107.pdf.
37. Eggink M., Charret S., Wijtmans M., Lingeman H., Kool J., Niessen W.M.A., Irth H. J. Chromatogr. B 2009, 877:3937-3945.
38. Simonelli A., Basilicata P., Miraglia N., Castiglia L., Guadagni R., Acampora A., Sannolo N. J. Chromatogr. B 2007, 860:26-33.
39. Pieri M., Castiglia L., Basilicata P., Sannolo N., Acampora A., Miraglia N. Ann. Occup. Hyg. 2010, 54:368-376.
40. EURACHEM Guide The Fitness for Purpose of Analytical Methods: A Laboratory Guide to Method Validation and Related Topics 1998.
41. Currie L.A. Anal. Chim. Acta 1999, 391:103.
42. Lee H.W., Park W.S., Kim Y.W., Cho S.H., Kim S.S., Seo J.H., Lee K.T. J. Mass Spectrom. 2006, 41:855-860.