Novel concept for the mass spectrometric determination of absolute isotopic abundances with improved measurement uncertainty: Part 3 - Molar mass of silicon highly enriched in 28Si

International Journal of Mass Spectrometry

Volumn 305, Issue 1, 2011, Pages 58-68

  Pramann, Axel ^a   Rienitz, Olaf ^a   Schiel, Detlef ^a   Güttler, Bernd ^a   Valkiers, Staf ^b  

^a PHYSIKALISCH TECHNISCHE BUNDESANSTALT   (Germany)

^b JOINT RESEARCH CENTRE   (Italy)

Author keywords

Avogadro constant; Isotope dilution mass spectrometry; MC ICP MS; Measurement uncertainty; Molar mass; Silicon

Indexed keywords

EID: 79960150693     PISSN: 13873806     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ijms.2011.05.017     Document Type: Article

References (32)

1. R. Gonfiantini, P. De Bivre, S. Valkiers, and P.D.P. Taylor Measuring the molar mass of silicon for a better Avogadro constant: reduced uncertainty IEEE Trans. Instrum. Meas. 40 1997 566 571 (Pubitemid 127769991)
2. P. Becker, H. Bettin, H.-U. Danzebrink, M. Gläser, U. Kuetgens, A. Nicolaus, D. Schiel, P. De Bivre, S. Valkiers, and P. Taylor Determination of the Avogadro constant via the silicon route Metrologia 40 2003 271 287
3. P. Becker Tracing the definition of the kilogram to the Avogadro constant using a silicon single crystal Metrologia 40 2003 366 375
4. 28Si for the precise determination of the Avogadro constant Meas. Sci. Technol. 17 2006 1854 1860 (Pubitemid 43958864)
5. P. De Bivre, G. Lenaers, T.J. Murphy, H.S. Peiser, and S. Valkiers The chemical preparation and characterization of specimens for "absolute" measurements of the molar mass of an element, exemplified by silicon, for redeterminations of the Avogadro constant Metrologia 32 1995 103 110
6. P. Becker, P. De Bivre, K. Fujii, M. Glaeser, B. Inglis, H. Luebbig, and G. Mana Considerations on future redefinitions of the kilogram, the mole and of other units Metrologia 44 2007 1 14 (Pubitemid 46620784)
7. O. Rienitz, A. Pramann, and D. Schiel Novel concept for the mass spectrometric determination of absolute isotopic abundances with improved measurement uncertainty: Part 1 - Theoretical derivation and feasibility study Int. J. Mass Spectrom. 289 2010 47 53
8. A. Pramann, O. Rienitz, D. Schiel, and B. Güttler Novel concept for the mass spectrometric determination of absolute isotopic abundances with improved measurement uncertainty: Part 2 - Development of an experimental procedure for the determination of the molar mass of silicon using MC-ICP-MS Int. J. Mass Spectrom. 299 2011 78 86
9. G. Mana, and O. Rienitz The calibration of Si isotope-ratio measurements Int. J. Mass Spectrom. 291 2010 55 60
10. P. De Bivre Isotope dilution mass spectrometry: What can it contribute to accuracy in trace analysis? Fresenius J. Anal. Chem. 337 1990 766 771
11. K.G. Heumann Isotope Dilution Mass Spectrometry F. Adams, R. Gijbels, R. van Grieken, Inorganic Mass Spectrometry 1988 John Wiley & Sons New York 301 376
12. K.G. Heumann Isotope dilution mass spectrometry Int. J. Mass Spectrom. Ion Processes T 118/119 1992 575 592
13. K.G. Heumann Isotope dilution mass spectrometry (IDMS) of the Elements Mass Spectrom. Rev. 11 1992 41 67
14. W. Riepe, and H. Kaiser Massenspektrometrische Spurenanalyse von Calcium, Strontium und Barium in Natriumazid durch Isotopenverdünnungstechnik Z. Anal. Chem. 223 1966 321 335
15. P. Klingbeil, J. Vogl, W. Pritzkow, G. Riebe, and J. Müller Comparative studies on the certification of reference materials by ICPMS and TIMS using isotope dilution procedures Anal. Chem. 73 2001 1881 1888 (Pubitemid 32862457)
16. M.J.T. Milton, and J. Wang High accuracy method for isotope dilution mass spectrometry with application to the measurement of carbon dioxide Int. J. Mass Spectrom. 218 2002 63 73
17. J.R. de Laeter, J.K. Böhlke, P. De Bivre, H. Hidaka, H.S. Peiser, K.J.R. Rosman, and P.D.P. Taylor Atomic weights of the elements: review 2000 (IUPAC Technical Report) Pure Appl. Chem. 75 2003 683 800
18. G. Audi, A.H. Wapstra, and C. Thibault The AME2003 atomic mass evaluation (II): Tables, graphs and references Nucl. Phys. A 729 2003 337 676 (Pubitemid 37495859)
19. G. Mana, O. Rienitz, and A. Pramann Measurement equations for the determination of the Si molar mass by isotope dilution mass spectrometry Metrologia 47 2010 460 463
20. A. Montaser Inductively Coupled Plasma Mass Spectrometry 1998 Wiley-VCH New York
21. J. Vogl Calibration Strategies and Quality Assurance S.M. Nelms, Inductively Coupled Plasma Mass Spectrometry Handbook 2005 Blackwell Publishing Ltd. Oxford 146 181
22. E. Ponzevera, C.R. Quétel, M. Berglund, P.D.P. Taylor, P. Evans, R.D. Loss, and G. Fortunato Mass Discrimination during MC-ICP-MS isotopic ratio measurements: investigation by means of synthetic isotopic mixtures (IRMM-007 series) and application to the calibration of natural-like zinc materials (including IRMM-3702 and IRMM-651) J. Am. Soc. Mass Spectrom. 17 2006 1412 1427 (Pubitemid 44441924)
23. M.E. Wieser, and J.B. Schwieters The development of multiple collector mass spectrometry for isotope ratio measurements Int. J. Mass. Spectrom. 242 2005 97 115 (Pubitemid 40353736)
24. S. Weyer, and J.B. Schwieters High precision Fe measurements with high mass resolution MC-ICPMS Int. J. Mass. Spectrom. 226 2003 355 368
25. E. Engström, I. Rodushkin, D.C. Baxter, and B. Öhlander Chromatographic purification for the determination of dissolved silicon isotopic compositions in natural waters by high-resolution multicollector inductively coupled plasma mass spectrometry Anal. Chem. 78 2006 250 257 (Pubitemid 43050161)
26. S.H.J.M. van den Boorn, P.Z. Vroon, C.C. van Belle, B. van der Waagt, J. Schwieters, and M.J. van Bergen Determination of silicon isotope ratios in silicate materials by high-resolution MC-ICP-MS using a sodium hydroxide sample digestion method J. Anal. Atom. Spectrom. 21 2006 734 742 (Pubitemid 44147655)
27. BIPM, Evaluation of measurement data - guide to the expression of uncertainty in measurement, JCGM 100:2008.
28. GUM-Workbench ™, Version 1.2.11.56 Win32© '96-'99 by Metrodata GmbH.
29. I. Mills, T. Cvitaš, K. Homann, N. Kallay, and K. Kuchitsu International Union of Pure and Applied Chemistry: Quantities, Units and Symbols in Physical Chemistry 1993 Blackwell Science Ltd Oxford
30. K. Fujii, A. Waseda, N. Kuramoto, S. Mizushima, P. Becker, H. Bettin, A. Nicolaus, U. Kuetgens, S. Valkiers, P. Taylor, P. De Bivre, G. Mana, E. Massa, R. Matyi, E.G. Kessler, and M. Hanke Jr. Present state of the Avogadro constant determination from silicon crystals with natural isotopic compositions IEEE Trans. Instrum. Meas. 54 2005 854 859 (Pubitemid 40535842)
31. P. Becker, H. Friedrich, K. Fujii, W. Giardini, G. Mana, A. Picard, H.-J. Pohl, H. Riemann, and S. Valkiers The Avogadro constant determination via enriched silicon-28 Meas. Sci. Technol. 20 2009 092002
32. 28Si crystal Phys. Rev. Lett. 106 2011 030801-1 0308014-0308014