Chiral separation of metalaxyl and benalaxyl fungicides by electrokinetic chromatography and determination of enantiomeric impurities

Journal of Chromatography A

Volumn 1218, Issue 30, 2011, Pages 4877-4885

  Pérez Fernández, Virginia ^a   García, Maria Ángeles ^a   Marina, Maria Luisa ^a  

^a UNIVERSITY OF ALCALÁ   (Spain)

Author keywords

Benalaxyl; Chiral separation; Commercial formulations; EKC; Enantiomeric impurity; Folpet; Metalaxyl

Indexed keywords

BENALAXYL; CHIRAL SEPARATIONS; COMMERCIAL FORMULATIONS; EKC; ENANTIOMERIC IMPURITY; FOLPET; METALAXYL;

CHIRALITY; CHROMATOGRAPHY; FUNGICIDES; IMPURITIES;

ENANTIOMERS;

CYCLODEXTRIN DERIVATIVE; FUNGICIDE; METALAXYL; METHYL N PHENYLACETYL N 2,6 XYLYLALANINATE; SUCCINYL BETA CYCLODEXTRIN; SUCCINYL GAMMA CYCLODEXTRIN; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; ENANTIOMER; ENANTIOMERIC IMPURITY; ENANTIOSELECTIVITY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MICELLAR ELECTROKINETIC CHROMATOGRAPHY; PRIORITY JOURNAL; PURIFICATION; SEPARATION TECHNIQUE;

ALANINE; ANALYSIS OF VARIANCE; CHROMATOGRAPHY, MICELLAR ELECTROKINETIC CAPILLARY; DRUG CONTAMINATION; FUNGICIDES, INDUSTRIAL; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; STEREOISOMERISM;

EID: 79959922927     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.12.116     Document Type: Article

References (41)

1. Sekhon B.S. J. Pestic. Sci. 2009, 34:1.
2. Armstrong D.W., Reid G.L., Hilton M.L., Chang C.D. Environ. Pollut. 1992, 79:51.
3. A.W. Garrison, Environ. Sci. Technol. (2006) 16.
4. Wong C.S. Anal. Bioanal. Chem. 2006, 286:544.
5. Kohler H.P.E., Nickel K., Zipper C. Adv. Microb. Ecol. 2000, 16:201.
6. Ali I., Gupta V.K., Aboul-Enein H.Y. Curr. Sci. 2003, 84:152.
7. Williams A. Pestic. Sci. 1996, 46:3.
8. http://www.marm.es/.
9. Marucchini C., Zadra C. Chirality 2002, 14:32.
10. Fischer D.J., Hayes A.L. Pestic. Sci. 1982, 13:330.
11. Vishunavat K., Nashaat N.I., Heran A., Kolte S.J. Crop Prot. 1998, 17:543.
12. Kurihara N., Miyamoto J., Paulson G.D., Zeeh B., Skidmore M.W., Hollingworht R.M., Kuiper H.A. Pure Appl. Chem. 1997, 69:2007.
13. Zadra C., Marucchini C., Zazzeini A. J. Agric. Food. Chem. 2002, 50:5373.
14. Chen S., Liu W. Bull. Environ. Contam. Toxicol. 2008, 81:531.
15. Müller M.D., Buser H.R. Environ. Sci. Technol. 1995, 29:2031.
16. Jarman J.L., Jones W.L., Howell L.A., Garrison A.W. J. Agric. Food Chem. 2005, 53:6175.
17. Buser H.R., Müller M.D., Poiger T., Balmer M.E. Environ. Sci. Technol. 2002, 36:221.
18. Buerge I.J., Poiger T., Müller M., Buser A.R. Environ. Sci. Technol. 2003, 37:2668.
19. Sukul P., Spiteller M. Rev. Environ. Contam. Toxicol. 2000, 164:1.
20. Qiu J., Wang Q., Wang P., Jia G., Li J., Zhou Z. Pestic. Biochem. Physiol. 2005, 83:1.
21. Liu D., Wang P., Zhou W., Gu X., Chen Z., Zhou Z. Anal. Chim. Acta 2006, 555:210.
22. Qiu J., Wang Q., Zhu W., Jia G., Wang X., Zhou Z. Chirality 2007, 19:51.
23. Gozzo F., Garavaglia G., Zagni A. Proc. Br. Crop Prot. Conf. Pests Dis. 1984, 3:923.
24. Gu X., Wang P., Liu D., Lv C., Lu Y., Zhou Z. Chirality 2008, 20:125.
25. Wang X., Jia G., Qiu J., Diao J., Zhu W., Lv C., Zhou Z. Chirality 2007, 19:300.
26. Xu P., Liu D., Diao J., Lu D., Zhou Z. J. Agric. Food Chem. 2009, 57:8545.
27. Monkiedje A., Spiteller M., Bester K. Environ. Sci. Technol. 2003, 37:707.
28. http://www.codexalimentarius.net/.
29. Santilio A., Dommarco R. J. Capillary Electrop. Microchip. Technol. 2006, 9:79.
30. Fanali S. J. Chromatogr. A 2000, 875:89.
31. Fanali S. J. Chromatogr. A 1997, 792:227.
32. Fanali S. Electrophoresis 2009, 30:S203.
33. Scriba G.K.E. J. Sep. Sci. 2008, 31:1991.
34. Chankvetadze B. J. Chromatogr. A 2007, 1168:45.
35. Scaheper J.P., Sepaniak K.J. Electrophoresis 2000, 21:1421.
36. Q2: Validation of Analytical Procedures: Text and Methodology. International Conference on Harmonization. ICH Harmonized Tripartite Guidelines. Published in the Federal Register 62, 1997, p. 27463.
37. Blanco M., Gonzalez J., Torras E., Valverde I. Anal. Bioanal. Chem. 2003, 375:157.
38. Chankvetadze B. Capillary Electrophoresis in Chiral Analysis 1997, John Wiley & Sons, Chichester, England.
39. Juvancz Z., Kendrovics R.B., Iványi R., Szente L. Electrophoresis 2008, 29:1701.
40. Marina M.L., Rios A., Valcarcel M. Analysis and Detection by Capillary Electrophoresis in Comprehensive Analytical Chemistry 2005, Elsevier, Amsterdam.
41. Quirino J.P., Terabe S. J. Chromatogr. A 1999, 856:465.