Optimization of the derivatization reaction and the solid-phase microextraction conditions using a D-optimal design and three-way calibration in the determination of non-steroidal anti-inflammatory drugs in bovine milk by gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1218, Issue 28, 2011, Pages 4487-4497

  Arroyo, David ^a   Ortiz, M Cruz ^a   Sarabia, Luis A ^a  

^a UNIVERSITY OF BURGOS   (Spain)

Author keywords

European Commission Decision 2002 657 EC; GC MS; Milk; NSAIDs; PARAFAC; SPME

Indexed keywords

EUROPEAN COMMISSION; GC/MS; MILK; NSAIDS; PARAFAC; SPME;

CALIBRATION; CHEMICAL ANALYSIS; DESIGN; DESIGN OF EXPERIMENTS; EXPERIMENTS; EXTRACTION; FIBERS; MASS SPECTROMETRY; MEASUREMENT THEORY; MICROCHANNELS; OPTIMAL SYSTEMS; OPTIMIZATION; SILICONES;

GAS CHROMATOGRAPHY;

DICLOFENAC; DIMETICONE; DIVINYLBENZENE; FLUFENAMIC ACID; IBUPROFEN; KETOPROFEN; MECLOFENAMIC ACID; NAPROXEN; NONSTEROID ANTIINFLAMMATORY AGENT; POLYACRYLIC ACID; TOLFENAMIC ACID;

ARTICLE; CALIBRATION; CONTROLLED STUDY; COW; DECOMPOSITION; DERIVATIZATION; DRUG DETERMINATION; FACTORIAL DESIGN; FOOD ANALYSIS; MASS FRAGMENTOGRAPHY; MILK; NONHUMAN; PRIORITY JOURNAL; REACTION OPTIMIZATION; SOLID PHASE MICROEXTRACTION;

ADSORPTION; ANIMALS; ANTI-INFLAMMATORY AGENTS, NON-STEROIDAL; CALIBRATION; CATTLE; DRUG RESIDUES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; MILK; REGRESSION ANALYSIS; SENSITIVITY AND SPECIFICITY; SOLID PHASE MICROEXTRACTION;

BOVINAE;

EID: 79959365707     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.05.010     Document Type: Article

References (47)

1. The Merck Veterinary Manual 2010, Merck & Co. Inc., NJ, USA. 10th ed. C.M. Kahn, S. Line (Eds.).
2. Morin D.E., Shanks R.D., McCoy G.C. J. Am. Vet. Med. Assoc. 1998, 123:676.
3. Lockwood P.W., Johnson J.C., Katz T.L. Vet. Rec. 2003, 152:392.
4. Gallo P., Fabbrocino S., Vinci F., Fiori M., Danese V., Serpe L. Rapid Commun. Mass Spectrom. 2008, 22:841.
5. Reference Laboratory for Residues of Veterinary Drugs Workshop NSAIDs and Validation According to the SANCO/1805/2000 2001.
6. Goodman & Gilman's The Pharmacological Basis of Therapeutics 2005, Mc Graw-Hill, USA. 11th ed. L.L. Brunton, J.S. Lazo, K.L. Parker (Eds.).
7. 1990/2377/EEC Council Regulation of 26 June 1990, Brussels, Off. J. Eur. Union OJ L224 (August) (1990) 1.
8. CRL Guidance Paper, CRLs view on state of the art analytical methods for national residue control plans, 7 December 2007.
9. 2010/37/EC Council Regulation of 22 December 2009, Brussels, Off. J. Eur. Union L15 (January) (2010) 1.
10. Gallo P., Fabbrocino S., Dowling G., Salini M., Fiori M., Perretta G., Serpe L. J. Chromatogr. A 2010, 1217:2832.
11. Daeseleire E., Mortier L., De Ruyck H., Geerts N. Anal. Chim. Acta 2003, 488:25.
12. Gentili A. Trends Anal. Chem. 2007, 26:595.
13. Malone E.M., Dowling G., Elliot C.T., Kennedy D.G., Regan L. J. Chromatogr. A 2009, 1216:8132.
14. Dowling G., Gallo P., Malone E., Regan L. J. Chromatogr. A 2009, 1216:8117.
15. Dowling G., Gallo P., Fabbrocino S., Serpe L., Regan L. Food Addit. Contam. A 2008, 25:1497.
16. Rodríguez I., Quintana J.B., Carpinteiro J., Carro A.M., Lorenzo R.A., Cela R. J. Cromatogr. A 2003, 985:265.
17. Kosjek T., Heath E., Krbavcic A. Environ. Int. 2005, 31:679.
18. Lee H.B., Peart T.E., Svoboda M.L. J. Chromatogr. A 2005, 1094:122.
19. Lin W.C., Chen H.C., Ding W.H. J. Chromatogr. A 2005, 1065:279.
20. Moeder M., Schrader S., Winkler M., Popp P. J. Chromatogr. A 2000, 873:95.
21. Rodríguez I., Carpinteiro J., Quintana J.B., Carro A.M., Lorenzo R.A., Cela R. J. Chromatogr. A 2004, 1024:1.
22. Carpinteiro J., Quintana J.B., Martínez E., Rodríguez I., Carro A.M., Lorenzo R.A., Cela R. Anal. Chim. Acta 2004, 524:63.
23. Araujo L., Wild J., Villa N., Camargo N., Cubillan D., Prieto A. Talanta 2008, 75:111.
24. Farré M., Petrovic M., Barceló D. Anal. Bioanal. Chem. 2007, 387:1203.
25. 2002/657/EC Commission Decision of 12 August 2002, Brussels, Off. J. Eur. Commun. L221 (August) (2002) 8.
26. Sobolevsky T.G., Revelsky A.I., Revelsky I.A., Miller B., Oriedo V. J. Chromatogr. B 2004, 800:101.
27. Díez R., Sarabia L.A., Ortiz M.C. Anal. Bioanal. Chem. 2010, 396:923.
28. NIST/EPA/NIH Mass Spectral Library, Version 2.0 2002, National Institute of Standards and Technology, USA.
29. Mathieu D., Nony J., Phan-Tan-Luu R. NemrodW Version 2000 2000, L.P.R.A.I., Marseille.
30. Wise B.M., Gallagher N.B., Bro R., Shaver J.M. PLS_Toolbox 4.1.1 2007, Eigenvector Research, Manson, WA.
31. Rousseeuw P.J., Leroy A.M. Robust Regression and Outliers Detection 2001, John Wiley and Sons, Hoboken, NJ.
32. STATGRAPHICS Plus 5.1 2001, Statistical Graphics, Herndon, VA.
33. International Standard Organization, ISO 11843-2 Capability of Detection: Methodology in the Linear Calibration Case 2000, ISO, Geneva.
34. Arroyo D., Ortiz M.C., Sarabia L.A., Palacios F. J. Chromatogr. A 2009, 1216:5472.
35. Ortiz M.C., Sarabia L.A. J. Chromatogr. A 2007, 1158:94.
36. Anderson C.A., Bro R. Chemometr. Intell. Lab. Syst. 2000, 52:1.
37. Bro R. Chemometr. Intell. Lab. Syst. 1999, 46:133.
38. Kiers H.A.L., Ten Berge J.M.F., Bro R. J. Chemometr. 1999, 13:275.
39. I. García, R. Bro, G. Tomasi, L. Sarabia, M.C. Ortiz, in: G. Tomasi, Ph.D. Thesis, The Royal Veterinary and Agricultural University, Frederiksberg, 2006, pp. 247-262, http://www.models.kvl.dk/research/theses/.
40. García I., Ortiz M.C., Sarabia L., Aldama J.M. Anal. Chim. Acta 2007, 587:222.
41. Amigo J.M., Skov T., Bro R., Coello J., Maspoch S. Trends Anal. Chem. 2008, 27:714.
42. Ortiz M.C., Sarabia L.A., García I., Giménez D., Meléndez E. Anal. Chim. Acta 2006, 559:124.
43. Arroyo D., Ortiz M.C., Sarabia L.A., Palacios F. J. Chromatogr. A 2008, 1187:1.
44. Sanz M.B., Sarabia L.A., Herrero A., Ortiz M.C. Anal. Chim. Acta 2003, 489:85.
45. Ortiz M.C., Sarabia L.A., Sánchez M.S. Anal. Chim. Acta 2010, 674:123.
46. Lewis G.A., Mathieu D., Phan-Tan-Luu R. Pharmaceutical and Experimental Designs 1999, Marcel Dekker, New York.
47. Real B.D., Ortiz M.C., Sarabia L.A. D-Optimal Designs and the Second Order Property to Optimize a SPE Procedure to Analyze Triazines in Infusions by GC-MS VII Colloquium Chemiometricum Mediterraneum June 2010.