Optimization of the synthesis of a hyper-crosslinked stationary phases: A new generation of highly efficient, acid-stable hyper-crosslinked materials for HPLC

Journal of Separation Science

Volumn 34, Issue 12, 2011, Pages 1407-1422

  Zhang, Yu ^a   Huang, Yuming ^b   Carr, Peter W ^a  

^a UNIVERSITY OF MINNESOTA   (United States)

^b SOUTHWEST UNIVERSITY   (China)

Author keywords

Acid stable; LC; RPLC; Stationary phase; Two dimensional

Indexed keywords

ACID STABILITY; ACIDIC MEDIA; BIOLOGICAL ANALYTES; CHROMATOGRAPHIC PROPERTIES; CROSS-LINKING REAGENTS; ELEVATED TEMPERATURE; FRIEDEL-CRAFTS; HIGH TEMPERATURE; KINETIC STUDY; LC; RPLC; SEPARATION PERFORMANCE; STATIONARY PHASE; STATIONARY PHASIS; TWO-DIMENSIONAL LIQUID CHROMATOGRAPHY; ULTRA-FAST;

CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; OPTIMIZATION; SYNTHESIS (CHEMICAL); TWO DIMENSIONAL;

CROSSLINKING;

ACID;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; FRIEDEL CRAFTS REACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYPERCROSSLINKED STATIONARY PHASE; KINETICS; LIQUID CHROMATOGRAPHY; PHASE SEPARATION; PRIORITY JOURNAL; REACTION OPTIMIZATION; REACTION TIME; REVERSED PHASE LIQUID CHROMATOGRAPHY; SYNTHESIS; TWO DIMENSIONAL LIQUID CHROMATOGRAPHY;

ACIDS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CROSS-LINKING REAGENTS; KINETICS; RESINS, SYNTHETIC;

EID: 79959211242     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201100252     Document Type: Article

References (76)

1. Majors, R. E., LC-GC North Am. 2008, 26, 16-28.
2. MacNair, J. E., Lewis, K. C., Jorgenson, J. W., Anal. Chem. 1997, 69, 983-989.
3. Mazzeo, J. R., Neue, U. D., Kele, M., Plumb, R. S., Anal. Chem. 2005, 77, 460a-467a.
4. Wu, N. J., Thompson, R., J. Liq. Chrom. Rel. Technol. 2006, 29, 949-988.
5. DeStefano, J. J., Langlois, T. J., Kirkland, J. J., J. Chromatogr. Sci. 2008, 46, 254-260.
6. Zhang, Y., Wang, X. L., Mukherjee, P., Petersson, P., J. Chromatogr. A 2009, 1216, 4597-4605.
7. Thompson, J. D., Carr, P. W., Anal. Chem. 2002, 74, 4150-4159.
8. Yan, B. W., Zhao, J. H., Brown, J. S., Blackwell, J., Carr, P. W., Anal. Chem. 2000, 72, 1253-1262.
9. Heinisch, S., Rocca, J. L., J. Chromatogr. A 2009, 1216, 642-658.
10. Antia, F. D., Horvath, C., J. Chromatogr. 1988, 435, 1-15.
11. Li, J. W., Carr, P. W., Anal. Chem. 1997, 69, 2550-2553.
12. Chen, H., Horvath, C., Anal. Method Instrum. 1994, 1, 213-222.
13. Wilke, C. R., Chang, P., Am. Inst. Chem. Eng. J. 1955, 1, 264-270.
14. Yang, Y., J. Sep. Sci. 2007, 30, 1131-1140.
15. Smith, R. M., J. Chromatogr. A 2008, 1184, 441-455.
16. Hartonen, K., Riekkola, M. L., Trac. Trend Anal. Chem. 2008, 27, 1-14.
17. Mao, Y., Carr, P. W., Anal. Chem. 2000, 72, 110-118.
18. Vanhoenacker, G., Sandra, P., J. Sep. Sci. 2006, 29, 1822-1835.
19. McCalley, D. V., J. Sep. Sci. 2003, 26, 187-200.
20. McCalley, D. V., J. Chromatogr. A 2002, 965, 51-64.
21. Mao, Y., Carr, P. W., Anal. Chem. 2000, 72, 2788-2796.
22. Hetem, M. J. J., De Haan, J. W., Claessens, H. A., Van de Ven, L. J. M., Cramers, C. A., Kinkel, J. N., Anal. Chem. 1990, 62, 2288-2296.
23. Glajch, J. L., Kirkland, J. J., US Patent # 4,705,725 1987.
24. Kirkland, J. J., Glajch, J. L., Farlee, R. D., Anal. Chem. 1989, 61, 2-11.
25. Wirth, M. J., Fairbank, R. W. P., Fatunmbi, H. O., Science 1997, 275, 44-47.
26. Wirth, M. J., Fatunmbi, H. O., Anal. Chem. 1992, 64, 2783-2786.
27. Wirth, M. J., Fatunmbi, H. O., Anal. Chem. 1993, 65, 822-826.
28. Wirth, M. J., Fatunmbi, H. O., US Patent # 5,599,625 1997.
29. Wirth, M. J., Fatunmbi, H. O., US Patent # 5,716,705 1998.
30. Neue, U. D., in:, Meyers, R. A., (Ed.), Encyclopedia of Analytical Chemistry, Wiley, New York 2000.
31. Trammell, B. C., Ma, L., Luo, H., Jin, D., Hillmyer, M. A, Carr, P. W., Anal. Chem. 2002, 74, 4634-4639.
32. Fatunmbi, H. O., Bruch, M. D., Wirth, M. J., Anal. Chem. 1993, 65, 2048-2054.
33. Pesek, J. J., Rashet, W., Chromatographia 1990, 30, 442-446.
34. Buchmeiser, M. R., J. Chromatogr. A 2001, 918, 233-266.
35. Henry, R. A., Am. Lab. 2002, 34, 18, 20-22, 24-25.
36. Pesek, J. J., Matyska, M. T., J. Chromatogr. A 2002, 952, 1-11.
37. Kirkland, J. J., LC-GC 1996, 14, 486-500.
38. Majors, R. E., LC-GC 1986, 4, 872, 874, 876.
39. Nawrocki, J., Dunlap, C., McCormick, A., Carr, P. W., J. Chromatogr. A 2004, 1028, 1-30.
40. Snyder, L. R., Glajch, J. L., Kirkland, J. J., Practical HPLC Method Development, Wiley-Interscience, New York 1996.
41. Unger, K. K., Packings and Stationary Phases in Chromatographic Techniques, M. Dekker, New York 1989.
42. Luo, H., Carr, P. W., Anal. Bioanal. Chem. 2008, 391, 919-923.
43. Luo, H., Ma, L. J., Zhang, Y., Carr, P. W., J. Chromatogr. A 2008, 1182, 41-55.
44. Ma, L. J., Luo, H., Dai, J., Carr, P. W., J. Chromatogr. A 2006, 1114, 21-28.
45. Trammell, B. C., Ma, L. J., Luo, H., Hillmyer, M. A., Carr, P. W., J. Chromatogr. A 2004, 1060, 61-76.
46. Davankov, V. A., Sychov, C. S., Ilyin, M. M., Sochilina, K. O., J. Chromatogr. A 2003, 987, 67-75.
47. Penner, N. A., Nesterenko, P. N., Rybalko, M. A., J. Anal. Chem. 2001, 56, 934-939.
48. Rosenberg, G. I., Shabaeva, A. S., Moryakov, V. S., Musin, T. G., Tsyurupa, M. P., Davankov, V. A., Reactive Polymers, Ion Exchangers, Sorbents 1983, 1, 175-182.
49. Ma, L., Acid Stable Hyper Crosslinked Stationary Phases for the Reversed Phase High Performance Liquid Chromatographic Separation of Basic and Biological Analytes. Ph.D. Thesis, University of Minnesota University of Minnesota, Minneapolis, 2005.
50. Luo, H., A Silica-Based Hydrophobic Cation Exchange Phase for Water Soluble Pharmaceuticals and Bioactive Analytes. Ph.D. Thesis, University of Minnesota 2006.
51. Halasz, I., Martin, K., Ber. Bunsen-Ges. Phys. Chem. 1975, 79, 731-732.
52. Olah, G. A., Kobayashi, S., Tashiro, M., J. Am. Chem. Soc. 1972, 94, 7448-7461.
53. Olah, G. A., Kuhn, S. J., J. Org. Chem. 1964, 29, 2317-2320.
54. Hanson, M., Eray, B., Unger, K., Neimark, A. V., Schmid, J., Albert, K., Bayer, E., Chromatographia 1993, 35, 403-409.
55. Hanson, M., Unger, K. K., Trac. Trend Anal. Chem. 1992, 11, 368-373.
56. Li, J., Carr, P. W., Anal. Chem. 1997, 69, 2193-2201.
57. Li, J., Reeder, D. H., McCormick, A. V., Carr, P. W., J. Chromatogr. A 1997, 791, 45-52.
58. Dai, J., Carr, P. W., McCalley, D. V., J. Chromatogr. A 2009, 1216, 2474-2482.
59. McCalley, D. V., Anal. Chem. 2003, 75, 3404-3410.
60. Dai, J., Carr, P. W., J. Chromatogr. A 2005, 1072, 169-184.
61. Dai, J., Mendonsa, S. D., Bowser, M. T., Lucy, C. A., Carr, P. W., J. Chromatogr. A 2005, 1069, 225-234.
62. Snyder, L. R., Dolan, J. W., Carr, P. W., J. Chromatogr. A 2004, 1060, 77-116.
63. Gilroy, J. J., Dolan, J. W., Snyder, L. R., J. Chromatogr. A 2003, 1000, 757-778.
64. Gilroy, J. J., Dolan, J. W., Carr, P. W., Snyder, L. R., J. Chromatogr. A 2004, 1026, 77-89.
65. Wilson, N. S., Gilroy, J., Dolan, J. W., Snyder, L. R., J. Chromatogr. A 2004, 1026, 91-100.
66. Marchand, D. H., Croes, K., Dolan, J. W., Snyder, L. R., J. Chromatogr. A 2005, 1062, 57-64.
67. Marchand, D. H., Croes, K., Dolan, J. W., Snyder, L. R., Henry, R. A., Kallury, K. M. R., Waite, S., Carr, P. W., J. Chromatogr. A 2005, 1062, 65-78.
68. Wilson, N. S., Nelson, M. D., Dolan, J. W., Snyder, L. R., Wolcott, R. G., Carr, P. W., J. Chromatogr. A 2002, 961, 171-193.
69. Wilson, N. S., Nelson, M. D., Dolan, J. W., Snyder, L. R., Carr, P. W., J. Chromatogr. A 2002, 961, 195-215.
70. Wilson, N. S., Dolan, J. W., Snyder, L. R., Carr, P. W., Sander, L. C., J. Chromatogr. A 2002, 961, 217-236.
71. Zhang, Y., Carr, P. W., J. Chromatogr. A 2011, 1218, 763-777.
72. Melander, W., Stoveken, J., Horvath, C., J. Chromatogr. 1980, 199, 35-56.
73. Hanai, T., Hubert, J., J. Chromatogr. 1984, 291, 81-89.
74. Tanaka, N., Tokuda, Y., Iwaguchi, K., Araki, M., J. Chromatogr. 1982, 239, 761-772.
75. Yang, X., Ma, L., Carr, P. W., J. Chromatogr. A 2005, 1079, 213-220.
76. Stoll, D. R., Li, X., Wang, X., Carr, P. W., Porter, S. E. G., Rutan, S. C., J. Chromatogr. A 2007, 1168, 3-43.