Bubbling reactor technology for rapid synthesis of uniform, small MFI-type zeolite crystals

Industrial and Engineering Chemistry Research

Volumn 50, Issue 12, 2011, Pages 7241-7250

  Liu, Wei ^a   Rao, Yuxiang ^a   Wan, Haiying ^a   Karkamkar, Abhijeet ^a   Liu, Jun ^a   Wang, Li Qiong ^b  

^a PACIFIC NORTHWEST NATIONAL LABORATORY   (United States)

^b BROWN UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ADSORPTION PROCESS; ADSORPTION/DESORPTION; CRYSTAL SIZE; FLOW REACTORS; GROWTH SOLUTIONS; HIGH THROUGHPUT; HYDROTHERMAL GROWTH; MESOPOROSITY; MFI-TYPE ZEOLITE; NEW APPLICATIONS; PURE CRYSTALS; RAPID SYNTHESIS; REACTION CONDITIONS; REACTOR TECHNOLOGY; SEM/EDS; SI/AL RATIO; SMALL CRYSTALS; SYNTHESIS PROCESS; XRD , TEM; ZEOLITE CRYSTALS; ZEOLITE MATERIALS; ZEOLITE SYNTHESIS;

ADSORBENTS; ADSORPTION; BUBBLE FORMATION; CARBON DIOXIDE; CHARACTERIZATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION KINETICS; SYNTHESIS (CHEMICAL);

CRYSTALS;

EID: 79958796596     PISSN: 08885885     EISSN: 15205045     Source Type: Journal    
DOI: 10.1021/ie102069z     Document Type: Article

References (31)

1. Bhatia, S. Zeolite Catalysis: Principles and Applications; CRC Press: Boca Raton, FL, 1990.
2. Chen, N. Y.; Degnan, T. F.; Smith, C. M. Molecular Transport and Reaction in Zeolites: Design and Application of Shape Selective Catalysis; Wiley-VCH: Weinheim, Germany, 1994.
3. x Reduction in the Presence of Water Vapor Catal. Today 1998, 42, 73
4. 2 Separation from Coal-Powered Plants J. Min., Met. Mater. Soc. 1997, 4, 36
5. Dong, J. H.; Lin, Y. S.; Liu, W. Multicomponent Hydrogen/Hydrocarbon Separation by MFI-type Zeolite Membranes AIChE J. 2000, 46, 1957
6. Frisch, S.; Roesken, L. M.; Caro, J.; Wark, M. Ion Conductivity of Nano-scaled Al-rich ZSM-5 Synthesized in the Pores of Carbon Black Microporous Mesoporous Mater. 2009, 120, 47
7. Xi, J. Y.; Miao, S. J.; Tang, X. Z. Selective Transporting of Lithium Ion by Shape Selective Molecular Sieves ZSM-5 in PEO-Based Composite Polymer Electrolyte Macromolecules 2004, 37, 8592
8. Kokotailo, G. T.; Lawton, S. L.; Olson, D. H.; Meier, W. M. Structure of Synthetic Zeolite ZSM-5 Nature 1978, 272, 437
9. Olson, D. H.; Kokotailo, G. T.; Lawton, S. L.; Meier, W. M. Crystal Structure and Structure-Related Properties of ZSM-5 J. Phys. Chem. 1981, 85, 2238
10. Verduijn, J. P. Synthesis and stabilization of nanoscale zeolite particles. International Patent WO 93/08125, 1993.
11. Wang, R.; Guo, X.; Wang, X.; Hao, J. Propylene Epoxidation over Silver Supported on Titanium Silicalite Zeolite Catal. Lett. 2003, 90, 57
12. Persson, A. E.; Schoeman, B. J.; Sterte, J.; Ottesstedt, J. E. The Synthesis of Discrete Colloidal Particles of TPA-Silicalite-1 Zeolites 1994, 14, 557
13. Persson, A. E.; Schoeman, B. J.; Sterte, J.; Otterstedt, J. E. Synthesis of Stable Suspensions of Discrete Colloidal Zeolite (Na,TPA)ZSM-5 Crystals Zeolites 1995, 15, 611
14. Van Grieken, R.; Sotelo, J. L.; Menendez, J. M.; Melero, J. A. Anomalous Crystallization Mechanism in the Synthesis of Nanocrystalline ZSM-5 Microporous Mesoporous Mater. 2000, 39, 135
15. Reding, G.; Maurer, T.; Kraushaar-Czarnetzki, B. Comparing Synthesis Routes to Nano-Crystalline Zeolite ZSM-5 Microporous Mesoporous Mater. 2003, 57, 83
16. Aguado, J.; Serrano, D. P.; Escola, J. M.; Rodriguez, J. M. Low Temperature Synthesis and Properties of ZSM-5 Aggregates Formed by Ultra-Small Nanocrystals Microporous Mesoporous Mater. 2004, 75, 41
17. Cheng, Y.; Wang, L. J.; Li, J. S.; Yang, Y. C.; Sun, X. Y. Preparation and Characterization of Nanosized ZSM-5 Zeolites in the Absence of Organic Template Mater. Lett. 2005, 59, 3427
18. Mohamed, R. M.; Fouad, O. A.; Ismail, A. A.; Ibrahim, I. A. Influence of Crystallization Times on the Synthesis of Nanosized ZSM-5 Mater. Lett. 2005, 59, 3441
19. Ismail, A. A.; Mohamed, R. M.; Fouad, O. A.; Ibrahim, I. A. Synthesis of Nanosized ZSM-5 Using Different Alumina Sources Cryst. Res. Technol. 2006, 41, 145
20. Madsen, C.; Jacobsen, C. J. H. Nanosized Zeolite Crystals-Convenient Control of Crystal Size Distribution by Confined Space Synthesis Chem. Commun. 1999, 8, 673
21. Kim, S. S.; Shah, J.; Pinnavaia, T. J. Colloid-Imprinted Carbons as Templates for the Nanocasting Synthesis of Mesoporous ZSM-5 zeolite Chem. Mater. 2003, 15, 1664
22. Wei, X. T.; Smirniotis, P. G. Synthesis and Characterization of Mesoporous ZSM-12 by Using Carbon Particles Microporous Mesoporous Mater. 2006, 89, 170
23. Wang, J.; Groen, J. C.; Yue, W.; Zhou, W.; Coppens, M.-O. Single-Template Synthesis of Zeolite ZSM-5 Composites with Tunable Mesoporosity Chem. Commun. 2007, 44, 4653
24. Schoeman, B. J.; Sterte, J.; Otterstedt, J. E. Analysis of the Crystal-Growth Mechanism of TPA-Silicalite-1 Zeolites 1994, 14, 568
25. Zhang, W. P.; Bao, X. H.; Guo, X. W.; Wang, X. S. A High-Resolution Solid-State NMR Study on Nano-Structured HZSM-5 Zeolite Catal. Lett. 1999, 60, 89
26. 29Si-MAS NMR Spectroscopy Microporous Mesoporous Mater. 2000, 39, 393
27. 27Al NMR and DFT/MM Study J. Phys. Chem. C. 2009, 113, 1447
28. 1H-MAS NMR Studies of ZSM-5 Type Zeolites Zeolites 1987, 7, 108
29. 1H MAS NMR J. Phys. Chem. 1995, 99, 13763
30. 1H MAS NMR J. Phys. Chem. B. 1998, 102, 804
31. 1H Nuclear Magnetic Resonance Spectroscopy Appl. Phys. Lett. 2007, 91, 173107