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note
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12: C, 20.05; H, 2.62; found: C, 20.15; H, 2.42; IR (KBr, cm-1; 3415.68(vs), 1604.02(s), 1421.33(s), 1350.46(m), 1310.22(w), 1292.39(w), 1233.84(w), 720.51(m), 576.70(m), 540.29(w).
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18
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19
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79957597834
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note
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2 using the SHELXTL program [17]. The CCDC reference numbers 791532 for 1.
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20
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32644443644
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