Enrofloxacin-imprinted monolithic HPLC columns synthesized by in situ copolymerization for chromatographic separation

Journal of Liquid Chromatography and Related Technologies

Volumn 34, Issue 9, 2011, Pages 705-718

  Lv, Yun Kai ^a   Zhao, Mi Ge ^a   Zhang, Dong ^b   Yan, Hong Yuan ^a  

^a HEBEI UNIVERSITY   (China)

^b The National Police University for Criminal Justice   (China)

Author keywords

Copolymerization; Egg samples; Enrofloxacin imprinted polymer; Monolithic column

Indexed keywords

ACTIVE METABOLITES; AFFINITY BINDING; BACK PRESSURES; BINDING CAPACITIES; CHROMATOGRAPHIC COLUMN; CHROMATOGRAPHIC CONDITIONS; CHROMATOGRAPHIC SEPARATIONS; CIPROFLOXACIN; DISSOCIATION CONSTANT; EGG SAMPLES; ENROFLOXACIN; ENROFLOXACIN IMPRINTED POLYMER; FLOWTHROUGH; HIGH-AFFINITY BINDING SITES; IN-SITU; MACROPORES; MESO-PORES; METHYL METHACRYLATES; METHYLACRYLIC ACIDS; MOBILE PHASE; MOBILE-PHASE COMPOSITION; MOLECULARLY IMPRINTED MONOLITHIC COLUMNS; MOLECULARLY IMPRINTED POLYMER; MONOLITHIC COLUMNS; POLYMERIZATION CONDITIONS; RAPID SEPARATION; RETENTION TIME; SCATCHARD ANALYSIS; SEM; SPECIFIC RECOGNITION; STATIC ADSORPTION;

ACRYLIC MONOMERS; ADSORPTION; ANTIBIOTICS; CHROMATOGRAPHY; COPOLYMERIZATION; DISSOCIATION; ESTERS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; POLYMERS; STAINLESS STEEL;

COPOLYMERS;

CIPROFLOXACIN; ENROFLOXACIN; METHACRYLIC ACID; METHACRYLIC ACID METHYL ESTER; STAINLESS STEEL;

ARTICLE; DISSOCIATION CONSTANT; DRUG DETERMINATION; DRUG STRUCTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHOBICITY; POLYMERIZATION; SCANNING ELECTRON MICROSCOPY;

EID: 79956057827     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826076.2011.562592     Document Type: Article

References (38)

1. Wulff, G. Molecular Imprinting in Cross-Linked Materials with the Aid of Molecular Templates - A Way towards Artificial Antibodies. Angew. Chem. Int. Ed. Engl. 1995, 34, 1812-1832.
2. Lavignac, N.; Allender, C. J.; Brain, K. R. Current Status of Molecularly Imprinted Polymers as Alternatives to Antibodies in Sorbent Assays. Anal. Chim. Acta 2004, 510, 139-145. (Pubitemid 38510123)
3. Yang, H. H.; Zhang, S. Q.; Tan, F.; Zhuang, Z. X.; Wang, X. R. Surface Molecularly Imprinted Nanowires for Biorecognition. J. Am. Chem. Soc. 2005, 127, 1378-1379. (Pubitemid 40204505)
4. Vlatakis, G.; Andersson, L. I.; Miller, R.; Mosbach, K. Drug Assay Using Antibody Mimics Made by Molecular Imprinting. Nature 1993, 361, 645-647. (Pubitemid 23062398)
5. Díaz-Alvarez, M.; Turiel, E.; Martín-Esteban, A. Selective Sample Preparation for the ANALYSis of (Fluoro) Quinolones in Baby Food: Molecularly Imprinted Polymers Versus Anion-Exchange Resins. Anal. Bioanal. Chem. 2009, 393, 899-905.
6. Xiong, Y.; Zhou, H. J.; Zhang, Z. J.; He, D. Y.; He, C. Flow-injection Chemiluminescence Sensor for Determination of Isoniazid in Urine Sample Based on Molecularly Imprinted Polymer. Spectrochim. Acta, Part A 2007, 66, 341-346. (Pubitemid 46027683)
7. Lee, W. C.; Cheng, C. H.; Pan, H. H.; Chung, T. H.; Hwang, C. C. Chromatographic Characterization of Molecularly Imprinted Polymers. Anal. Bioanal. Chem. 2008, 390, 1101-1109.
8. Haginaka, J.; Futagami, A. Addition of N-carbobenzyloxy-l-tryptophan as a Co-Template Molecule to Molecularly Imprinted Polymer Monoliths for (+)-nilvadipine. J. chromatogr. A 2008, 1185, 258-262.
9. Huang, X. D.; Qin, F.; Chen, X. M.; Liu, Y. Q.; Zou, H. F. Short Columns with Molecularly Imprinted Monolithic Stationary Phases for Rapid Separation of Diastereomers and Enantiomers. J. Chromatogr. B 2004, 804, 13-18. (Pubitemid 38469867)
10. Huang, X. D.; Zou, H. F.; Chen, X. M.; Luo, Q. Z.; Kong, L. Molecularly Imprinted Monolithic Stationary Phases for Liquid Chromatographic Separation of Enantiomers and Diastereomers. J. Chromatogr. A 2003, 984, 273-282. (Pubitemid 35454093)
11. Yan, H. Y.; Tian, M. L.; Row, K. H. Determination of Enrofloxacin and Ciprofloxacin in Milk Using Molecularly Imprinted Solid-Phase Extraction. J. Sep. Sci. 2008, 31, 3015-3020.
12. Yin, J. F.; Yang, G. L.; Chen, Y. Rapid and Efficient Chiral Separation of Nateglinide and Its L-enantiomer on Monolithic Molecularly Imprinted Polymers. J. Chromatogr. A 2005, 1090, 68-75. (Pubitemid 41207665)
13. Tamayo, F. G.; Turiel, E.; Martin-Esteban, A. Molecularly Imprinted Polymers for Solid-Phase Extraction and Solid-Phase Microextraction: Recent Developments and Future Trends. J. Chromatogr. A 2007, 1152, 32-40. (Pubitemid 46753989)
14. Benito-Peña, E.; Martins, S.; Orellana, G.; Moreno-Bondi, M. C. Water-compatible Molecularly Imprinted Polymer for the Selective Recognition of Fluoroquinolone Antibiotics in Biological Samples. Anal. Bioanal. Chem. 2009, 393, 235-245. (Pubitemid 50294104)
15. Prasad, B. B.; Sharma, P. S.; Lakshmi, D. Molecularly Imprinted Polymer-Based Solid-Phase Extraction Combined with Molecularly Imprinted Polymer-Based Sensor for Detection of Uric Acid. J. Chromatogr. A 2007, 1173, 18-26. (Pubitemid 350046584)
16. Brüggemann, O.; Visnjevski, A.; Burch, R.; Patel, P. Selective Extraction of Antioxidants with Molecularly Imprinted Polymers. Anal. Chim. Acta 2004, 504, 81-88. (Pubitemid 38128326)
17. Hirayama, K.; Sakai, Y.; Kameoka, K.; Nodac, K.; Naganawa, R. Preparation of a Sensor Device with Specific Recognition Sites for Acetaldehyde by Molecular Imprinting Technique. Sens. Actuators B 2002, 86, 20-25.
18. Dickert, F. L.; Lieberzeit, P.; Tortschanoff, M. Molecular Imprints as Artificial Antibodies a New Generation of Chemical Sensors. Sens. Actuators B 2000, 65, 186-189.
19. Haginaka, J.; Sanbe, H. Uniformly Sized Molecularly Imprinted Polymer for (S)-naproxen: Retention and Molecular Recognition Properties in Aqueous Mobile Phase. J. Chromatogr. A 2001, 913, 141-146. (Pubitemid 32260977)
20. Liu, X. J.; Chen, Z. Y.; Zhao, R.; Shangguan, D. H.; Liu, G. Q.; Chen, Y. Uniform-Sized Molecularly Imprinted Polymer for Metsulfuron-Methyl by One-Step Swelling and Polymerization Method. Talanta 2007, 71, 1205-1210. (Pubitemid 46161641)
21. Qu, G.; Wu, A.; Shi, X.; Niu, Z.; Xie, W.; Zhang, D. Improvement on Analyte Extraction by Molecularly Imprinted Polymer Microspheres Toward Enrofloxacin. Anal. Lett. 2008, 41, 1443-1458. (Pubitemid 351990080)
22. Ho, K. C.; Yeh, W. M.; Tung, T. S.; Liao, J. Y. Amperometric Detection of Morphine Based on Poly (3,4-ethylenedioxythiophene) Immobilized Molecularly Imprinted Polymer Particles Prepared by Precipitation Polymerization. Anal. Chim. Acta 2005, 542, 90-96.
23. Wang, J. F.; Cormack, P. A. G.; Sherrington, D. C.; Khoshdel, E. Monodisperse, Molecularly Imprinted Polymer Microspheres Prepared by Precipitation Polymerization for Affinity Separation Applications. Agnew. Chem. Inter. Ed. 2003, 42, 5336-5338. (Pubitemid 37462647)
24. Han, D. M.; Fang, G. Z.; Yan, X. P. Preparation and Evaluation of a Molecularly Imprinted Sol-Gel Material for On-Line Solid-Phase Extraction Coupled with High Performance Liquid Chromatography for the Determination of Trace Pentachlorophenol in Water Samples. J. Chromatogr. A 2005, 1100, 131-136.
25. Altmaier, S.; Cabrera, K. Structure and Performance of Silica-Based Monolithic HPLC Columns. J. Sep. Sci. 2008, 31, 2551-2559.
26. Matsui, J.; Kato, T.; Takeuchi, T.; Suzuki, M.; Yokoyama, K.; Tamiya, E.; Karube, I. Molecular Recognition in Continuous Polymer Rods Prepared by a Molecular Imprinting Technique. Anal. Chem. 1993, 65, 2223-2224.
27. Ou, J. J.; Kong, L.; Pan, C. S.; Su, X. Y.; Lei, X. Y.; Zou, H. F. Determination of DL-tetrahydropalmatine in Corydalis yanhusuo by L-tetrahydropalmatine Imprinted Monolithic Column Coupling with Reversed-Phase High Performance Liquid Chromatography. J. Chromatogr. A 2006, 1117, 163-169. (Pubitemid 44269290)
28. Franco, E. J.; Hofstetter, H.; Hofstetter, O. Enantiomer Separation of Alpha-Hydroxy Acids in High-Performsance Immunoaffinity Chromatography. J. Pharm. Biomed. Anal. 2008, 46, 907-913. (Pubitemid 351400614)
29. Matsui, J.; Miyoshi, Y.; Matsui, R.; Takeuchi, T. Rod-Type Affinity Media for Liquid Chromatography Prepared by In-Situ-Molecular Imprinting. Anal. Sci. 1995, 11, 1017-1019.
30. Schweitz, L.; Spégel, P.; Nilsson, S. Molecularly Imprinted Microparticles for Capillary Electrochromatographic Enantiomer Separation of Propranolol. Analyst 2000, 125, 1899-1901.
31. Schweitz, L.; Andersson, L. I.; Nilsson, S. Rapid Electrochromatographic Enantiomer Separations on Short Molecularly Imprinted Polymer Monoliths. Anal. Chim. Acta 2001, 435, 43-47. (Pubitemid 32727439)
32. Donoghue, D. J.; Schneider, M. J. Comparison Between a Bioassay and Liquid chromatography-Fluorescence-Mass Spectrometry for the Determination of Incurred Enrofloxacin in Whole Eggs. J. AOAC Int. 2003, 86, 669-674.
33. Hassouan, M. K.; Ballesteros, O.; Zafra, A.; Vílchez, J. L.; Navalón, A. Multiresidue Method for Simultaneous Determination of Quinolone Antibacterials in Pig Kidney Samples by Liquid Chromatography with Fluorescence Detection. J. Chromatogr. B 2007, 859, 282-288. (Pubitemid 350046454)
34. Hassouan, M.; Ballesteros, O.; Vlchez, J.; Zafra, A.; Navalon, A. Simple Multiresidue Determination of Fluoroquinolones in Bovine Milk by Liquid Chromatography with Fluorescence Detection. Anal. Lett. 2007, 40, 779-791. (Pubitemid 46395731)
35. Nilsson, K. G. I.; Sakaguchi, K.; Gemeiner, P.; Mosbach, K. Molecular Imprinting of Acetylated Carbohydrate Derivatives into Methacrylic Polymers. J. Chromatogr. A 1995, 707, 199-203.
36. Sun, H. W.; Qiao, F. X. Recognition Mechanism of Water-Compatible Molecularly Imprinted Solid-Phase Extraction and Determination of Nine Quinolones in Urine by High Performance Liquid Chromatography. J. Chromatogr. A 2008, 1212, 1-9.
37. Liu, H.; Zhuang, X.; Turson, M.; Zhang, M.; Dong, X. Enrofloxacin- Imprinted Monolithic Columns Synthesized Using Reversible Addition-Fragmentation Chain Transfer Polymerization. J. Sep. Sci. 2008, 31, 1694-1701. (Pubitemid 351911732)
38. Caro, E.; Marcé, R. M.; Cormack, P. A. G.; Sherrington, D. C.; Borrul, F. Direct Determination of Ciprofloxacin by Mass Spectrometry After a Two-Step Solid-Phase Extraction Using a Molecularly Imprinted Polymer. J. Sep. Sci. 2006, 29, 1230-1236. (Pubitemid 43950869)