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79955853970
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note
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2): δ=9.97 (s, 2 H, N=CH); 8,78 (s, 2 H, OH); 8.41-7.14 (m, 18 C-H, Ar); 4.04 (s, 2 H, CH2) ppm.
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42
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79955869691
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note
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+.
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43
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79955835330
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note
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Elemental analyses were carried out at the REQUIMTE DQ Service (Universidade Nova de Lisboa), on a Thermo Finnigan-CE Flash-EA 1112- CHNS instrument. Infrared spectra were recorded as KBr discs using Bio-Rad FTS 175-C spectrophotometer. Proton NMR spectra were recorded using a BrukerWM-400 spectrometer.
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44
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0642282599
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46
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79955864289
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note
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-5 M) were prepared by appropriate dilution of the stock solutions. Titrations of the ligand were carried out by addition of microliter amounts of standard solutions of the ions in acetonitrile or dichloromethane.
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47
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7044235741
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Savage, P.B.9
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