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note
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-1): 3226s, 1579s, 1529m, 1475w, 1446s, 1414w, 1385m, 1362w, 1270m, 1220w, 1118s, 1001w, 979w, 833w, 804w, 787w, 708m, 545m.
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18
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79955862326
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note
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2=0.1781 (all data), and the GOOF=1.092. The data were collected at a temperature of 293± 2 K on a Bruker Smart APEX a X-diffractometer equipped with graphite monochromated Mo Ka radiation (λ=0.71073 Å). The structure was solved by direct methods with the SHELXTL-97 program [22].
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