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Unpublished data
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Unpublished data.
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The 3-closed HBC contaminant was evident via NMR, but we were unable to obtain an analytically pure sample
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The 3-closed HBC contaminant was evident via NMR, but we were unable to obtain an analytically pure sample.
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Analogs of 1a, 2a, and 3a were synthesized with two alkyl chains in order to simplify analysis of the variable temperature 1H NMR data (see supplemental information)
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Analogs of 1a, 2a, and 3a were synthesized with two alkyl chains in order to simplify analysis of the variable temperature 1H NMR data (see supplemental information).
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