Quantitative analysis of simulated illicit street-drug samples using raman spectroscopy and partial least squares regression

Spectroscopy Letters

Volumn 44, Issue 4, 2011, Pages 229-234

  Fenton, Owen S ^a   Tonge, Lindsey A ^a   Moot, Taylor H ^b   Frederick, Kimberley A ^b  

^a Department of Biology   (United States)

^b SKIDMORE COLLEGE   (United States)

Author keywords

chemometrics; drugs; forensics; Raman

Indexed keywords

EID: 79954508553     PISSN: 00387010     EISSN: 15322289     Source Type: Journal    
DOI: 10.1080/00387010.2010.525285     Document Type: Article

References (25)

1. Noonan, K. Y.; Tonge, L. A.; Fenton, O. S.; Damiano, D. B.; Frederick, K. A. Rapid classification of simulated street drug mixtures using Raman spectroscopy and principal component analysis. Appl. Spectrosc. 2009, 63(7), 742-747.
2. Strachan, C. J.; Rades, T.; Gordon, K. C.; Rantanen, J. Raman spectroscopy for quantitative analysis of pharmaceutical solids. J. Pharm. Pharmacol. 2007, 59(2), 179-192. (Pubitemid 46203057)
3. Macleod, N. A.; Matousek, P. Emerging non-invasive Raman Methods in process control and forensic applications. Pharm. Res. 2008, 25(10), 2205-2215.
4. LaPlant, F.; Zhang, X. Quantitation of polymorphs in drug product by Raman Spectroscopy. Am. Pharm. Rev. 2005, 8(5), 88-95. (Pubitemid 44490899)
5. Strachan, C. J.; Pratiwi, D.; Gordon, K. C.; Rades, T. Quantitative analysis of polymorphic mixtures of carbamazepine by Raman spectroscopy and principal components analysis. J. Raman Spectrosc. 2004, 35(5), 347-352.
6. Wang, H.; Mann, C. K.; Vickers, T. J. Effect of powder properties on the intensity of Raman scattering by crystalline solids. Appl. Spectrosc. 2002, 56(12), 1538-1544.
7. Rantanen, J.; Wikstroem, H.; Rhea, F. E.; Taylor, L. S. Improved understanding of factors contributing to quantification of anhydrate= hydrate powder mixtures. Appl. Spectrosc. 2005, 59(7), 942-951. (Pubitemid 41028073)
8. Braun, D. E.; Maas, S. G.; Zencirci, N.; Langes, C.; Urbanetz, N. A.; Griesser, U. J. Simultaneous quantitative analysis of ternary mixtures of D-mannitol polymorphs by FT-Raman spectroscopy and multivariate calibration models. Int. J. Pharm. 2010, 385(1-2), 29-36.
9. Xie, Y.; Tao, W.; Morrison, H.; Chiu, R.; Jona, J.; Fang, J.; Cauchon, N. Quantitative determination of solid-state forms of a pharmaceutical development compound in drug substance and tablets. Int. J. Pharm. 2008, 362(1-2), 29-36.
10. Eliasson, C.; Macleod, N. A.; Jayes, L. C.; Clarke, F. C.; Hammond, S. V.; Smith, M. R.; Matousek, P. Non-invasive quantitative assessment of the content of pharmaceutical capsules using transmission Raman spectroscopy. J. Pharm. Biomed. Anal. 2008, 47(2), 221-229.
11. Johansson, J.; Sparen, A.; Svensson, O.; Folestad, S.; Claybourn, M. Quantitative transmission Raman spectroscopy of pharmaceutical tablets and capsules. Appl. Spectrosc. 2007, 61(11), 1211-1218. (Pubitemid 350096643)
12. Kim, M.; Chung, H.; Woo, Y.; Kemper, M. S. A new non-invasive, quantitative Raman technique for the determination of an active ingredient in pharmaceutical liquids by direct measurement through a plastic bottle. Anal. Chim. Acta 2007, 587(2), 200-207. (Pubitemid 46356286)
13. Park, S. C.; Kim, M.; Noh, J.; Chung, H.; Woo, Y.; Lee, J.; Kemper, M. S. Reliable and fast quantitative analysis of active ingredient in pharmaceutical suspension using Raman spectroscopy. Anal. Chim. Acta 2007, 593(1), 46-53. (Pubitemid 46776630)
14. Tsuchihashi, H.; Katagi, M.; Nishikawa, M.; Tatsuno, M.; Nishioka, H.; Nara, A.; Nishio, E.; Petty, C. Determination of methamphetamine and its related compounds using Fourier transform Raman spectroscopy. Appl. Spectrosc. 1997, 51(12), 1796-1799. (Pubitemid 127643750)
15. Bell, S. E. J.; Beattie, J. R.; McGarvey, J. J.; Peters, K. L.; Sirimuthu, N. M. S.; Speers, S. J. Development of sampling methods for Raman analysis of solid dosage forms of therapeutic and illicit drugs. J. Raman Spectrosc. 2004, 35(5), 409-417.
16. Katainen, E.; Elomaa, M.; Laakkonen, U.-M.; Sippola, E.; Niemela, P.; Suhonen, J.; Jarvinen, K. Quantification of the amphetamine content in seized street samples by Raman spectroscopy. J. Forensic Sci. 2007, 52(1), 88-92. (Pubitemid 46018426)
17. Ryder, A. G.; O'Connor, G. M.; Glynn, T. J. Identifications and quantitative measurements of narcotics in solid mixtures using near-IR Raman spectroscopy and multivariate analysis. J. Forensic Sci. 1999, 44(5), 1013-1019. (Pubitemid 29420387)
18. Ryder, A. G.; O'Connor, G. M.; Glynn, T. J. Quantitative analysis of cocaine in solid mixtures using Raman spectroscopy and chemometric methods. J. Raman Spectrosc. 2000, 31(3), 221-227.
19. Leger, M. N.; Ryder, A. G. Comparison of derivative preprocessing and automated polynomial baseline correction method for classification and quantification of narcotics in solid mixtures. Appl. Spectrosc. 2006, 60(2), 182-193. (Pubitemid 43341859)
20. Eliasson, C.; Matousek, P. Noninvasive authentication of pharmaceutical products through packaging using spatially offset Raman spectroscopy. Anal. Chem. 2007, 79(4), 1696-1701.
21. Johansson, J.; Pettersson, S.; Folestad, S. Characterization of different laser irradiation methods for quantitative Raman tablet assessment. J. Pharm. Biomed. Anal. 2005, 39(3-4), 510-516. (Pubitemid 41196056)
22. Beebe, K. R. Chemometrics: A Practical Guide; Wiley Interscience: New York, 1998; 360.
23. Moros, J.; Galipienso, N.; Vilches, R.; Garrigues, S.; de la Guardia, M. Nondestructive direct determination of heroin in seized illicit street drugs by diffuse reflectance near-infrared spectroscopy. Anal. Chem. 2008, 80(19), 7257-7265.
24. Zhang, D.; Ben-Amotz, D. Enhanced chemical classification of Raman images in the presence of strong fluorescence interference. Appl. Spectrosc. 2000, 54(9), 1379-1383.
25. Wise, B. M.; Shaver, J. M.; Gallagher, N. B.; Windig, W.; Bro, R.; Koch, R. S. Chemometrics Tutorial for PLS-Toolbox and Solo; Eigenvector Research, Inc.: Wenatchee, WA, 2006; 414.