A new open-framework indium phosphate-phosphite containing intersecting extra-large 16-ring channels

Inorganic Chemistry Communications

Volumn 14, Issue 5, 2011, Pages 727-730

  Dong, Zhaojun ^a   Yan, Yan ^a   Li, Yi ^a   Li, Jiyang ^a   Yu, Jihong ^a   Xu, Ruren ^a  

^a JILIN UNIVERSITY   (China)

Author keywords

Extra large 16 ring channel; Hydrothermal synthesis; Indium phosphate phosphite; NMR

Indexed keywords

EID: 79954429482     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2011.02.019     Document Type: Article

References (27)

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14. InHPO-CJ1 was prepared hydrothermally from a reaction mixture of InCl3•6H2O, H3PO3, 2-methyl-1,5-pentanediamine (MPMD) and H2O with a molar ratio of 1.0:4.0:3.0:277.7. The resulting mixture was heated at 180 °C for 7 days under static conditions. The colorless hexagonal prism shaped single crystals (39 wt.% yield based on Indium) were separated from the remainder of the product by sonication, washed with distilled water, and air-dried for characterization.
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