Two photoluminescent one-dimensional copper(I) iodide coordination polymers incorporating Cu2I2 double-stranded stair and Cu 6I6 hexagonal cage chain units

Inorganic Chemistry Communications

Volumn 14, Issue 5, 2011, Pages 622-625

  Hu, Sheng ^a   Yu, Fang Yong ^a   Yan, Yan ^a   Hao, Zhi Feng ^a   Yu, Lin ^a   Tong, Ming Liang ^b  

^a GUANGDONG UNIVERSITY OF TECHNOLOGY   (China)

^b SUN YAT SEN UNIVERSITY   (China)

Author keywords

Copper iodide; Crystal structure; Hexagonal cage chain; Photoluminescence

Indexed keywords

EID: 79954419908     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2011.01.032     Document Type: Article

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41. Synthesis of compound 1: Phenanthrene-9-carbonitrile (0.203 g, 1.0 mmol) in acetonitrile (20 ml) was slowly added to the pale-yellow solution of CuI (0.190 g, 1.0 mmol) in acetonitrile (20 ml) with magnetic stirring. The reaction mixture was stirred 4 hour at room temperature. The resulting yellow solution was allowed to stand in air at room temperature for 5 days, yielding pale yellow crystals (56% yield). Element analysis for 1 C15H9CuIN, calcd: C, 45.76; H, 2.30, N, 3.56%. Found: C, 45.84; H, 2.36; N, 3.49%. IR data (KBr, cm-1): 425w, 3055w, 3013w, 2230 m, 1930w, 1809w, 1708w, 1611 m, 1523w, 1492w, 1446 s, 1385w, 1385w, 1244w, 1219w, 1162w, 1055w, 950w, 884 m, 858w, 785w, 753 s, 719 s, 618w, 510w, 470w, 442w.
42. Crystal data for 1 (293 K): monoclinic, space group P21/n, a = 15.160(3), b = 4.146(1), c = 20.238(5) Å, β = 98.177(4)o, V = 1259.1(5) Å3, Z = 4, ρcalcd = 2.077 g cm-3, μ(MoKα) = 4.164 mm-1. Rint = 0.0279, S = 1.020, R1 (I > 2σ(I)) = 0.0435, wR2 (all data) = 0.1055. Data were collected on a Bruker Apex CCD diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å). The relevant crystallographic data are presented in Table S1, while the selected bond lengths and angles are given in Table S2, ESI.
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47. Crystal data for 2 (123 K): orthorhombic, space group Fdd2, a = 33.692(3), b = 41.859(4), c = 4.144(1) Å, V = 5844.5(9) Å3, Z = 16, ρcalcd = 2.655 g cm-3, μ(MoKα) = 7.123 mm-1. Rint = 0.0414, S = 1.040, R1 (I > 2σ(I)) = 0.0363, wR2 (all data) = 0.0841. Data were collected on a Bruker Apex CCD diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å). The relevant crystallographic data are presented in Table S1, while the selected bond lengths and angles are given in Table S2, ESI.
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