Combinative application of pH-zone-refining and conventional high-speed counter-current chromatography for preparative separation of alkaloids from Stephania kwangsiensis

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 879, Issue 13-14, 2011, Pages 945-949

  Dong, Hongjing ^a,b   Zhang, Yongqing ^b   Fang, Lei ^a   Duan, Wenjuan ^a   Wang, Xiao ^a   Huang, Luqi ^c  

^a QILU UNIVERSITY OF TECHNOLOGY   (China)

^b SHANDONG UNIVERSITY OF TRADITIONAL CHINESE MEDICINE   (China)

^c INSTITUTE OF CHINESE MATERIA MEDICA   (China)

Author keywords

Alkaloids; Conventional HSCCC; PH zone refining CCC; Preparative chromatography; Stephania kwangsiensis

Indexed keywords

ALKALOIDS; AQUEOUS MOBILE PHASE; CHEMICAL STRUCTURE; CONVENTIONAL HSCCC; CRUDE EXTRACT; ETHYL ACETATES; HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY; METHANOL-WATER; N-HEXANE; NATURAL PLANTS; NMR DATA; PH-ZONE-REFINING COUNTER-CURRENT CHROMATOGRAPHY; PREPARATIVE CHROMATOGRAPHY; PREPARATIVE SEPARATION; SOLVENT SYSTEM; STATIONARY PHASE; STEPHANIA KWANGSIENSIS; TRIETHYLAMINES;

ESTERS; HEXANE; HYDROCHLORIC ACID; METABOLITES; METHANOL; MIXTURES; NITROGEN COMPOUNDS; ORGANIC SOLVENTS; REFINING; VOLATILE FATTY ACIDS;

CHROMATOGRAPHY;

ALKALOID; CREBANINE; HYDROCHLORIC ACID; LEVO ROMERINE; PLANT EXTRACT; SINOACUTINE; STEPHANIA KWANGSIENSIS EXTRACT; STEPHANINE; UNCLASSIFIED DRUG;

AQUEOUS SOLUTION; ARTICLE; COUNTER CURRENT CHROMATOGRAPHY; DRUG PURITY; DRUG STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH SPEED COUNTER CURRENT CHROMATOGRAPHY; MASS SPECTROMETRY; NONHUMAN; PRIORITY JOURNAL; PROCESS OPTIMIZATION; PROTON NUCLEAR MAGNETIC RESONANCE;

ACETATES; APORPHINES; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; COUNTERCURRENT DISTRIBUTION; HEXANES; HYDROGEN-ION CONCENTRATION; METHANOL; MORPHINANS; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PLANT EXTRACTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; STEPHANIA; WATER;

EID: 79953315417     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2011.02.051     Document Type: Article

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