Application of new methodologies based on design of experiments, independent component analysis and design space for robust optimization in liquid chromatography

Analytica Chimica Acta

Volumn 691, Issue 1-2, 2011, Pages 33-42

  Debrus, Benjamin ^a   Lebrun, Pierre ^a   Ceccato, Attilio ^b   Caliaro, Gabriel ^c   Rozet, Eric ^a   Nistor, Iolanda ^a,d   Oprean, Radu ^d   Rupérez, Francisco J ^e   Barbas, Coral ^e   Boulanger, Bruno ^f   Hubert, Philippe ^a  

^a UNIVERSITY OF LIÈGE   (Belgium)

^b Odyssea Pharma   (Belgium)

^c Orailac Quality Solutions   (Belgium)

^d IULIU HATIEGANU UNIVERSITY OF MEDICINE AND PHARMACY   (Romania)

^e UNIVERSIDAD SAN PABLO CEU   (Spain)

^f Arlenda   (Belgium)

Author keywords

Design space; Experimental design; High performance liquid chromatography; Independent component analysis; Method development; Separation optimization

Indexed keywords

CHROMATOGRAPHIC ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INDEPENDENT COMPONENT ANALYSIS; OPTIMIZATION; SEPARATION; STATISTICS;

CHROMATOGRAPHIC METHODS; DESIGN SPACES; METHOD DEVELOPMENT; PHARMACEUTICAL FORMULATION; PREDICTION ACCURACY; ROBUST OPTIMIZATION; SEPARATION OPTIMIZATIONS; UNCERTAINTY STUDIES;

DESIGN OF EXPERIMENTS;

ARTICLE; CHEMOMETRIC ANALYSIS; CONTROLLED STUDY; CRITERION VARIABLE; EXPERIMENTAL DESIGN; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INDEPENDENT COMPONENT ANALYSIS; MATHEMATICAL ANALYSIS; PREDICTION; PRIORITY JOURNAL; PROBABILITY; PROCESS DESIGN; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; SEPARATION TECHNIQUE; UNCERTAINTY;

EID: 79953208584     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2011.02.035     Document Type: Article

References (26)

1. Snyder L.R., Kirkland J.J., Glajch: J.L. Practical HPLC Method Development 1997, Wiley & Sons, New York. 2nd ed.
2. Schoenmakers P., Abbott R.W. Anal. Chim. Acta 1988, 208:357-358.
3. Dewé W., Marini R., Chiap P., Hubert P., Crommen J., Boulanger B. Chemom. Intell. Lab. Syst. 2004, 74:263-268. http://hdl.handle.net/2268/6036.
4. International Conference on Harmonization (ICH) of Technical Requirements for registration of Pharmaceuticals for Human Use, Topic Q8(R2): Pharmaceutical Development, Geneva, 2005.
5. Peterson J.J. J. Qual. Tech. 2004, 36:139-153.
6. De Backer B., Debrus B., Lebrun P., Theunis L., Dubois N., Decock L., Verstraete A., Hubert Ph., Charlier C. J. Chromatogr. B 2009, 877:4115-4124. http://hdl.handle.net/2268/4442.
7. Lebrun P., Govaerts B., Debrus B., Ceccato A., Caliaro G., Hubert Ph., Boulanger B. Chemom. Intell. Lab. Syst. 2008, 91:4-16. http://hdl.handle.net/2268/1640.
8. Debrus B., Lebrun P., Ceccato A., Caliaro G., Govaerts B., Olsen B.A., Rozet E., Boulanger B., Hubert Ph. Talanta 2009, 79:77-85. http://hdl.handle.net/2268/13236.
9. Biswas K.M., Castle B.C., Olsen B.A., Risley D.S., Skibic M.J., Wright P.B. J. Pharm. Biomed. Anal. 2009, 49:692-701.
10. García A., Rupérez F.J., Marín A., de la Maza A., Barbas C. J. Chromatogr. B 2003, 785:237-243.
11. Olmo B., García A., Marín A., Barbas C. J. Chromatogr. B 2005, 817:159-165.
12. Marín A., Barbas C. J. Pharm. Biomed. Anal. 2006, 40:262-270.
13. Marín A., Barbas C. J. Pharm. Biomed. Anal. 2004, 35:769-777.
14. Marín A., García E., García A., Barbas C. J. Pharm. Biomed. Anal. 2002, 29:701-714.
15. Vander Heyden Y., Nijhuis A., Smeyers-Verbeke J., Vandeginste B.G.M., Massart D.L. J. Pharm. Biomed. Anal. 2001, 24:723-753.
16. Dejaegher B., Vander Heyden Y. J. Chromatogr. A 2007, 1158:138-157.
17. Dejaegher B., Dumarey M., Capron X., Bloomfield M.S., Vander Heyden Y. Anal. Chim. Acta 2007, 595:59-71.
18. Dejaegher B., Capron X., Smeyers-Verbeke J., Vander Heyden Y. Anal. Chim. Acta 2006, 564:184-200.
19. Dejaegher B., Smeyers-Verbeke J., Vander Heyden Y. Anal. Chim. Acta 2005, 544:268-279.
20. Atkinson A.C., Donev A.N. Optimum Experimental Designs 1992, Clarendon Press, Oxford.
21. Martens H., Martens M. Multivariate Analysis of Quality. An Introduction 2001, Wiley, Chichester.
22. International Conference on Harmonization (ICH) of Technical Requirements for registration of Pharmaceuticals for Human Use, Topic Q2(R1): Validation of Analytical Procedures: Text and Methodology, Geneva, 1996.
23. Herrador M.A., Asuero A.G., Gonzalez A.G. Chemom. Intell. Lab. Syst. 2005, 79:115-122.
24. Hyvärinen A., Karhunen J., Oja E. Independent Component Analysis 2001, Wiley, New York.
25. Hyvärinen A., Oja E. Neural Networks 2000, 13:411-430.
26. Moffat A.C., Osselton M.D., Widdop B. Clarke's Analysis of Drugs and Poisons 2004, Pharmaceutical Press, Electronic version.