Microextraction by packed sorbent in bioanalysis

Bioanalysis

Volumn 1, Issue 4, 2009, Pages 687-691

  Abdel Rehim, Mohamed ^a  

^a ASTRAZENECA   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

ANTINEOPLASTIC AGENT; LOCAL ANESTHETIC AGENT; STREET DRUG;

ADSORPTION; ANALYSIS; ARTICLE; BLOOD; HUMAN; ISOLATION AND PURIFICATION; METHODOLOGY; SOLID PHASE MICROEXTRACTION; URINE;

ADSORPTION; ANALYTIC SAMPLE PREPARATION METHODS; ANESTHETICS, LOCAL; ANTINEOPLASTIC AGENTS; HUMANS; SOLID PHASE MICROEXTRACTION; STREET DRUGS;

EID: 79952987515     PISSN: 17576180     EISSN: 17576199     Source Type: Journal    
DOI: 10.4155/bio.09.61     Document Type: Note

References (22)

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2. Abdel-Rehim M, Altun Z, Blomberg L. Microextraction in packed syringe (MEPS) for liquid and gas chromatographic applications: part II-determination of ropivacaine and its metabolites in human plasma samples using MEPS with liquid chromatography/tandem mass spectrometry. J. Mass Spectrom. 39, 1488-1493 (2004).
3. Altun Z, Abdel-Rehim M, Blomberg L. New trends in sample preparation: on-line microextraction in packed syringe (MEPS) for LC and GC applications Part III: determination and validation of local anaesthetics in human plasma samples using a cation-exchance sorbent, and MEPS-LC-MS/MS. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 813, 129-135 (2004).
4. Vita M, Skansen P, Hassan M, Abdel-Rehim M. Development and validation of a liquid chromatography and tandem mass spectrometry method for determination of roscovitine in plasma and urine samples utilizing on-line sample preparation. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 817, 303-307 (2005).
5. a and plasma protein binding of roscovitine. J. Chromatogr. B 821, 75-80 (2005).
6. Abdel-Rehim M, Skansen P, Vita M et al. Microextraction in packed syringe/liquid chromatography/electrospray tandem mass spectrometry for quantifcation of olomoucine in human plasma samples. Anal. Chim. Acta. 539, 35-39 (2005).
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10. Abdel-Rehim M, Dahlgren M, Claude S, Tabacchi R, Blomberg L. Microextraction in packed syringe (MEPS) utilizing methylcyanopropyl-silarylene as coating polymer for extraction of drugs in biological samples. J. Liq. Chromatogr. Relat. Technol. 29, 2537-2544 (2006).
11. Abdel-Rehim M, Askemark M, Norsten-Höög C, Pettersson KJ, Halldin M. Quantifcation of 4-OH-2, 6-xylidine and its conjugates in human urine samples utilising microextraction in packed syringe on-line with liquid chromatography and electrospray tandem mass spectrometry (MEPS-LC-MS/MS). J. Liq. Chromatogr. Relat. Technol. 29, 2413-2424 (2006).
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13. El-Beqqali A, Kussak A, Abdel-Rehim M. Determination of dopamine and serotonin in human urine samples utilizing microextraction online with liquid chromatography/electrospray tandem mass spectrometry. J. Sep. Sci. 30, 421-424 (2007).
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15. Abdel-Rehim M, Hassan Z, Skansen P, Hassan M. Simultaneous determination of busulphan in plasma samples by liquid chromatography-electrospray ionization mass spectrometry utilizing microextraction in packed syringe (MEPS) as on-line sample preparation method J. Liq. Chromatogr. Relat. Technol. 30, 3029-3041 (2007).
16. Said R, Hassan Z, Hassan M, Abdel-Rehim M. Rapid and sensitive method for determination of cyclophosphamide in patients plasma samples utilizing microextraction by packed sorbent online with liquid chromatography-tandem mass spectrometry (MEPS-LC-MS/MS) J. Liq. Chromatogr. Relat. Technol. 31, 683-694 (2008).
17. Abdel-Rehim M, Andersson A, Breitholtz-Emanuelsson A, Sandberg-Ställ M, Brunfelter K, Norsten-Höög C. MEPS as a rapid sample preparation method to handle unstable compounds in a complex matrix: determination of AZD3409 in plasma samples utilizing MEPS-LC-MS/MS. J. Chromatogr. Sci. 46, 518-523 (2008).
18. Kamel M, Said R, Elbiqali A, Abdel-Rehim M. Quantitative determination of lidocaine, ropivacaine and bupivacine in whole human blood samples utilizing microextraction by packed sorbent online with liquid chromatography-tandem mass spectrometry (MEPS-LC-MS/MS). Anal. Chim. Acta Submitted for publication (2009).
19. Kamel M, Said R, Elbiqali A, Bassyouni F, Abdel-Rehim M. On-line determination of cyclophosphamide in blood samples utilizing microextraction by packed sorbent and liquid chromatography tandem mass spectrometry (MEPS-LC-MS/MS). Open Spec. J. 3, 26-30 (2009).
20. Jagerdeo E, Abdel-Rehim M. Screening of cocaine and its metabolites in human urine samples by direct ana lysis in real-time source coupled to time-of-fight mass spectrometry after online preconcentration utilizing microextraction by packed sorbent. J. Am. Soc. Mass Spectrom. 20, 891-899 (2009).
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