GC-MS analysis of water-soluble organics in atmospheric aerosol: Response surface methodology for optimizing silyl-derivatization for simultaneous analysis of carboxylic acids and sugars

Analytica Chimica Acta

Volumn 689, Issue 2, 2011, Pages 257-264

  Pietrogrande, Maria Chiara ^a   Bacco, Dimitri ^a  

^a UNIVERSITY OF FERRARA   (Italy)

Author keywords

Atmospheric aerosol; Dicarboxylic acids and sugars; Experimental design; Response surface methodology; Silylation derivatization procedure

Indexed keywords

CENTRAL COMPOSITE DESIGNS; CHEMICAL MARKERS; DERIVATIZATION PROCEDURES; DERIVATIZATION REAGENT; DERIVATIZATIONS; DICARBOXYLIC ACID; ENVIRONMENTAL MATRIXES; EXPERIMENTAL DESIGN; EXPERIMENTAL EVIDENCE; GC-MS ANALYSIS; OPERATING CONDITION; OPTIMIZED PROTOCOL; REACTION TEMPERATURE; REAGENT CONCENTRATION; RESPONSE SURFACE METHODOLOGY; SAMPLING SITE; SILYLATION DERIVATIZATION PROCEDURE; SILYLATIONS; SIMULTANEOUS ANALYSIS; SIZE DIMENSIONS; SOLUTION VOLUME; TARGET ANALYTES; TRIFLUOROACETAMIDES; TRIMETHYLSILYL; WATER-SOLUBLE ORGANICS;

ATMOSPHERIC CHEMISTRY; ATMOSPHERIC THERMODYNAMICS; CARBOXYLIC ACIDS; CHEMICAL ANALYSIS; CHEMICAL REACTIONS; CONCENTRATION (PROCESS); DESIGN; OPTIMIZATION; PYRIDINE; STATISTICS; SUGARS; SURFACE PROPERTIES;

ATMOSPHERIC AEROSOLS;

4 HYDROXYBENZOIC ACID; ARABINOSE; AZELAIC ACID; CARBOHYDRATE; CARBOXYLIC ACID; GALACTOSE; GLUCOSE; GLUTARIC ACID; GLYCOLIC ACID; LEVOGLUCOSAN; MALEIC ACID; MALIC ACID; MALONIC ACID; MALTOSE; MANDELIC ACID; MANNOSE; PHTHALIC ACID; PIMELIC ACID; PYRIDINE; SALICYLIC ACID; SUCCINIC ACID; TREHALOSE; TRIFLUOROACETAMIDE DERIVATIVE;

AEROSOL; AIR ANALYSIS; ARTICLE; CHEMICAL REACTION; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DERIVATIZATION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; PARTICLE SIZE; PARTICULATE MATTER; PRIORITY JOURNAL; PROCESS OPTIMIZATION; RESPONSE SURFACE METHOD; SEASONAL VARIATION; SUMMER; TEMPERATURE; URBAN RURAL DIFFERENCE; WINTER;

EID: 79952489286     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2011.01.047     Document Type: Article

References (34)

1. Oliveira C., Pio C., Alves C., Evtyugina M., Santos P., Gonc-alves V., Nunes T., Silvestre A.J.D., Palmgren F., Wahlin P., Harrad S. Atmos. Environ. 2007, 41:5555.
2. Alves C., Pio C., Carvalho A., Santos C. Chemosphere 2006, 63:153.
3. Bi X., Simoneit B.R.T., Sheng G., Ma S., Fu J. Atmos. Res. 2008, 88:256.
4. Kourtchev I., Warnke J., Meanhaut W., Hoffmann T., Claeys M. Chemosphere 2008, 73:1308.
5. von Schneidemesser E., Schauer J.J., Hagler G.S.W., Bergin M.H. Atmos. Environ. 2009, 43:4155.
6. Lewandowski M., Jaoui M., Offenberg J.N., Kleindiest T.E., Edney E.O., Sheesley R.J., Schauer J.J. Environ. Sci. Technol. 2008, 42:3303.
7. Collet J.L., Herckes P., Youngster S., Lee T. Atmos. Res. 2008, 87:232.
8. Fisseha R., Dommen M., Paulsen D., Kalberer M., Maurer R., Hofler F., Weingartner E., Baltensperger U. Anal. Chem. 2004, 76:6535.
9. Ho K.F., Lee S.C., Cao J.J., Kawamura K., Watanabe T., Cheng Y., Chow J.C. Atmos. Environ. 2006, 40:3030.
10. Wang H., Kawamura K., Ho K.F., Lee S.C. Environ. Sci. Technol. 2006, 40:6255.
11. Yang L., Ray M.B., Yu L.E. Atmos. Environ. 2008, 42:868.
12. Wang W., Wu M.H., Li L., Zhang T., Liu X.D., Feng J.L., Li H.J., Wang Y.J., Sheng G.Y., Claeys M., Fu J. Atmos. Chem. Phys. 2008, 8:7507.
13. Graham B., Mayol-Bracero O., Guyon P., Roberts G.C., Decesari S., Facchini M.C., Artaxo P., Maenhaut W., Koll P., Andreae M.O. J. Geophys. Res. 2002, 107:8047.
14. Simoneit B.R.T., Elias V.O., Kobayashi M., Kawamura K., Rushdi A.I., Medeiros P.M., Rogge W.F., Didyk B.M. Environ. Sci. Technol. 2004, 38:5939.
15. Medeiros P., Conte M.H., Weber J.C., Simoneit B.R.T. Atmos. Environ. 2006, 40:1694.
16. Bauer H., Claeys M., Vermeylenb R., Schueller E., Weinke G., Berger A., Puxbaum H. Atmos. Environ. 2008, 42:588.
17. Schmidl C., Bauer H., Dattler A., Hitzenberger R., Weissenboeck G., Marr I.L., Puxbaum H. Atmos. Environ. 2008, 42:9070.
18. Zhang T., Claeys M., Cachier H., Dong S., Wang W., Maenhaut W., Liu X. Atmos. Environ. 2008, 42:7013.
19. Tsai Y.I., Wu P.L., Hsu Y.T., Yang C.R. Atmos. Environ. 2010, 44:3708.
20. Mochida M., Kawamura K., Fu P.Q., Takemura T. Atmos. Environ. 2010, 44:3511.
21. Wan E.C.H., Yu J.Z. J. Chromatogr. A 2006, 1107:175.
22. Iinuma Y., Engling G., Puxbaum H., Herrmann H. Atmos. Environ. 2009, 43:1367.
23. Jaoui M., Kleindienst T.E., Lewandowski M., Edney E.O. Anal. Chem. 2004, 76:4765.
24. Schkolnik G., Rudich Y. Anal. Bioanal. Chem. 2006, 385:26.
25. Medeiros P.M., Simonet B.R.T. J. Chromatogr. A 2007, 1141:271.
26. Schummer C., Delhomme O., Appenzeller B.M.R., Wennig R., Millet M. Talanta 2009, 77:1473.
27. Pietrogrande M.C., Bacco D., Mercuriali M. Anal. Bioanal. Chem. 2010, 396:877.
28. Hoffer A., Gelencser A., Blazso M., Guyon P., Artaxo P., Andreae M.O. Atmos. Chem. Phys. 2006, 8:3505.
29. Fuzfai Z., Boldizsar I., Molnar-Perl I. J. Chromatogr. A 2008, 1177:183.
30. Ding X., Zheng M., Yu L., Zhang X., Weber R.J., Yan B., Russel A.G., Edgerton E.S., Wang Z. Environ. Sci. Technol. 2008, 42:5171.
31. Fu P., Kawamura K., Barrie L.A. Environ. Sci. Technol. 2009, 43:286.
32. Massart D.L., Vandeginste B.G.M., Buydens L.M.C., De Song S., Lewi P.J., Smeyers-Verbeke J. Handbook of Chemometrics Qualimetrics (Part A) 1997, Elsevier Science, Amsterdam, Netherlands.
33. Ranz A., Korpecka J., Lankmayr E. J. Sep. Sci. 2008, 31:746.
34. Rontanil J.F., Aubert C. Rapid Commun. Mass Spectrom. 2004, 18:1889.