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The electrochemical measurements were done in a threeelectrode experimental setup. Hg/HgO electrode was used as reference electrode, and nickel foil as the counter electrode. The working electrode was prepared as follows: V-MCFs or MCFs were mixed with poly(tetrafluoroethylene) and graphite with a mass ratio of 8.5:1:0.5. The mixture was pressed between two pieces of nickel foam under 30 MPa. Thereafter, the 0.45-mm-thick electrode was dried overnight at 100°C. Cyclic voltammograms and galvanostatic chargedischarge behavior were tested in electrolyte of 6mol L1 KOH using a CHI 660D system.
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