Development and validation of a solid-phase extraction method coupled to high-performance liquid chromatography with ultraviolet-diode array detection for the determination of sulfonylurea herbicide residues in bovine milk samples

Journal of Chromatography A

Volumn 1218, Issue 9, 2011, Pages 1253-1259

  Seccia, Serenella ^a   Albrizio, Stefania ^a   Fidente, Paola ^b   Montesano, Domenico ^a  

^a UNIVERSITY OF NAPLES FEDERICO II   (Italy)

^b UNIVERSITY OF MILAN   (Italy)

Author keywords

Food; HPLC DAD analysis; SPE extraction; Sulfonylurea herbicides

Indexed keywords

ANALYTES; BENSULFURON-METHYL; BOVINE MILK; CHLORSULFURON; CLEAN UP; DECISION LIMIT; DETECTION CAPABILITY; DIODE ARRAY DETECTION; DIODE ARRAY DETECTORS; EUROPEAN COMMISSION; FOOD; HPLC-DAD ANALYSIS; MATRIX EFFECTS; MAXIMUM RESIDUE LIMITS; METHOD VALIDATIONS; METSULFURON METHYL; RELATIVE STANDARD DEVIATIONS; SIMULTANEOUS DETERMINATIONS; SOLID PHASE EXTRACTION METHOD; SOLID-PHASE EXTRACTION; SPE EXTRACTION; SULFONYLUREA HERBICIDES; THIFENSULFURON METHYL; TRIASULFURON; WATER GRADIENT; WHOLE MILK;

ACETONITRILE; DETECTORS; EXTRACTION; LAWS AND LEGISLATION; LIQUID CHROMATOGRAPHY; LIQUIDS; RECOVERY; WEED CONTROL;

HERBICIDES;

ACETONITRILE; BENSULFURON METHYL; CHLORSULFURON; HERBICIDE RESIDUE; METSULFURON METHYL; PRIMISULFURON METHYL; RIMSULFURON; SULFONYLUREA; THIFENSULFURON; TRIASULFURON; TRIBENURON METHYL; UNCLASSIFIED DRUG; WATER;

ACCURACY; ARTICLE; CHEMICAL STRUCTURE; CONCENTRATION (PARAMETERS); ELUTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MILK; PRIORITY JOURNAL; RESIDUE ANALYSIS; SENSITIVITY AND SPECIFICITY; SEPARATION TECHNIQUE; SOLID PHASE EXTRACTION;

ANIMALS; CATTLE; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DRUG RESIDUES; HERBICIDES; LEAST-SQUARES ANALYSIS; MILK; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; SPECTROPHOTOMETRY, ULTRAVIOLET; SULFONYLUREA COMPOUNDS;

BOVINAE;

EID: 79551610460     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.01.006     Document Type: Article

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